HomeMy Public PortalAboutWQRC Packet 1-29-21Town of Brewster Water Quality Review Committee
2198 Main St., Brewster, MA 02631
wqrcmeeting@brewster-ma.gov
(508) 896-3701
MEETING AGENDA
Remote Participation Only
January 29, 2021 at 9 a.m.
This meeting will be conducted by remote participation pursuant to Governor Baker’s March 2020 orders suspending certain Open Meeting Law
provisions and imposing limits on public gatherings. No in-person meeting attendance will be permitted. If the Town is unable to live broadcast
this meeting, a record of the proceedings will be provided on the Town website as soon as possible. The Town has established specific email
addresses for each board and committee so the public can submit comments either before or during the meeting. To submit public comment
or questions to the Water Qulity Review Committee, please email: wqrcmeeting@brewster-ma.gov. To view the:
Live broadcast: Tune to Brewster Government TV Channel 18
Livestream: Go to www.livestream.brewster-ma.gov
Audio/video recording: Go to www.tv.brewster-ma.gov
Water Quality
Review
Committee
Cyndi Baran
Chair
Amy von Hone
Vice Chair
Roberta Barrett
Ned Chatelain
Penny Holeman
Chris Miller
Victor Staley
CPC Assistant
Beth Devine
1.Call to Order
2.Declaration of a Quorum
3.Meeting Participation Statement
4.Discussion and Vote on Site Assignment Closing and Reduction of Monitoring
5.Discussion and Possible Vote on Committee Signatures for Certificates
6.Approval of Minutes from 12/18/20
7.For Your Information
Cape Sand & Recycling Update 12 20
CS&R GW Monitoring and TPI Report (Nov 2020)
8.Matters Not Reasonably Anticipated by the Chair
9.Next Meeting: TBD
10.Adjournment
Date Posted:Date Revised:Received by Town Clerk:
Charles D. Baker
Governor
Karyn E. Polito
Lieutenant Governor
Kathleen Theoharides
Secretary
Martin Suuberg
Commissioner
This information is available in alternate format. Call Michelle Waters-Ekanem, Diversity Director, at 617-292-5751. TTY# MassRelay Service 1-800-439-2370
MassDEP Website: www.mass.gov/dep
Printed on Recycled Paper
January 12, 2021
Mr. Daniel Serber
Senior Director of Land Development
Next Grid NFF Marshfield LLC
P.O. Box 7755 #73069
San Francisco, CA 94120
RE: Approval with Conditions
Application for: BWP SW 37 Post-Closure Use - Minor
Solar Photovoltaic Array
Application No: 20-SW37-0003-APP
Permit Authorization No: SW37-0000015
AT: Daniels Antinarelli Stump Dump
443 Freemans Way
Brewster, MA 02631
Facility ID#: 337767, Regulated Object#: 337768
Dear Mr. Serber:
The Massachusetts Department of Environmental Protection, Solid Waste Management Section (the
"MassDEP"), has completed its Administrative Review and Technical Review of the referenced Post-
Closure Use permit application (the "Application") for the Daniels Antinarelli Stump Dump (the
“Site”). The Application was prepared and submitted on behalf of NextGrid NFF Marshfield LLC
(“NextGrid”) by Bennett Environmental Associates, LLC (the “Engineer”) of Brewster,
Massachusetts.
MassDEP has determined the Application is administratively and technically complete and hereby
approves the Post-Closure Use of the Landfill for a 3.2 megawatts ("MW") DC solar photovoltaic
("PV") array subject to conditions as specified herein.
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I. SUBMITTALS:
MassDEP has reviewed the Application pursuant to 310 CMR 19.000: Solid Waste Regulations,
310 CMR 19.143: Post-Closure Use of Landfills and MassDEP's Landfill Technical Guidance
Manual, May 1997 (the "Manual"). The Application consists of the following:
A completed BWP SW 37 application form for Post-Closure Use – Minor with assigned
application no: 20-SW37-0003-APP, an application form for Post-Closure Use - Minor
(BWP SW 37) signed by Daniel Serber of NextGrid;
A report narrative prepared by Bennett Environmental Associates, LLC dated September
17, 2020 describing the proposed use which includes erosion and sedimentation controls,
drainage plan and stormwater management, and Permit Criteria;
A set of eight engineering drawings dated August 10, 2020 prepared by BSC Group of
West Yarmouth, Massachusetts and signed by Brian G. Yergatian, Massachusetts
Registered Professional Engineer No. 46206;
The Application was submitted electronically via the Massachusetts Executive Office of Energy
and Environmental Affairs ePlace Portal at https://permitting.state.ma.us/CitizenAccess/ on
September 30, 2020.
The following supplemental information was submitted in response to MassDEP questions and
comments:
A copy of the Administrative Consent Order dated September 16, 2010 issued by MassDEP
to Daniels Landscaping & Construction, Inc. of Orleans, Massachusetts, a copy of Property
Card from the Town of Brewster Assessor for Parcel ID 119-6-0 and Parcel ID 119-8-0,
and a copy of the Town of Brewster Registry of Deeds Book 660 Page 9, submitted
electronically via email by the Engineer on December 3, 2020.
Variance approval from the Town of Brewster Zoning Board of Appeals dated October 19,
2020, Site Plan Review Approval Modification #2019-17 dated October 28, 2020 and
Special Permit and Site Plan Review Decision #2020-14 from the Town of Brewster
Planning Department, submitted electronically via email by the Engineer on December 3,
2020.
MassDEP’s review of application is limited to the submittals as listed above. Bearing capacity
and settlement analysis that would include a geotechnical evaluation were not required for
submittal and/or reviewed. The Application indicated that no settlement is anticipated since the
installation of the frame for the PV panels will be driven into the soils that have not been previously
disturbed to specifications for load bearing. The Applicant did not submit a stability analysis on
the proposed PV array project at this time (refer to Condition #3).
The Application may be reviewed online at https://eeaonline.eea.state.ma.us/EEA/PublicApp/
using the “Site Name” Daniels Antinarelli Stump Dump and the “Search” tab. Under “Record
Type”, select the “Application” file with the 09/30/2020 “Application Date” and the
“Authorization” file with the 05/01/2021 “Authorization Date”.
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II. SITE DESCRIPTION:
The Daniels Antinarelli Stump Dump is located immediately east of the intersection of Route 6
and north of Freeman’s way in Brewster, Massachusetts. The Site encompasses approximately a
total of 10.4 acres of land and consists of two lots: Lot 56 (i.e., Parcel ID 119-6) and Lot 58, each
consisting of approximately 5.2 acres of land. The Site abuts the Brewster Recreation Fields and
Watershed to the west, municipal golf course to the south, mostly land-locked undeveloped land
to the north, and industrial and commercial use properties and facilities to the east. There are no
buildings located on the Site. According to the letter from MassDEP addressed to Aaron Culig of
NextGrid, Inc. dated November 3, 2020 and the Existing Conditions Site Plan submitted to
MassDEP in April 2020, the following approximate volumes of woodwaste still remain at the Site:
Woodwaste Type Parcel ID 119-6 Parcel ID 119-8
Unprocessed Woodwaste None 15,681 cubic yards (CY)
Partially Processed Woodwaste None 5.190 CY
Totals 0 CY 20,871 CY
As a condition to this Approval, the Applicant shall conduct woodwaste recovery operations by
removing all the woodwaste including stockpiled woodwaste and any buried woodwaste that may
be discovered during project activities. Processed woodwaste (i.e. woodchips) may be used as
landscaping material (e.g. erosion control). Utilization of these processed woodwaste as fill
material for the PV array project is prohibited by MassDEP pursuant to the Solid Waste
Regulations (refer to Condition #2).
The Application indicated that approximately 2,000 CY of an estimated 4,400 CY of the screened
loam from recovery operations shall be re-used in the final groundcover to support revegetation.
Any unsuitable materials that do not qualify for reuse at the Site will be transported off-site to
Cape Sand and Recycling, a permitted and licensed solid waste facility (refer to Condition #2).
Erosion and Sedimentation Controls: The Applicant indicated that based on the topography of the
Site, all stormwater and any sediment generated were confined to the Site. Existing slopes were
graded and vegetated to prevent erosion. No history of flooding has ever recorded on site.
Post-Closure Maintenance and Environmental Monitoring: Pursuant to 310 CMR 19.006:
Definitions, the Site does not meet the definition for Landfill; therefore, post –closure maintenance
and environmental monitoring is not required. Post-Closure maintenance work at the Site will be
associated with the PV array project upon construction completion and during operation.
III. POST-CLOSURE USE PROPOSAL SUMMARY:
Upon purchase completion of the subject property (Parcel ID 119-6 and Parcel ID 119-8) from the
current owner, the Applicant will develop, build, own, and operate a PV array at the Site. The
Applicant shall be responsible in removing all buried woodwaste from the Site and submit a BWP
SW-43 Closure Completion permit application for MassDEP review and approval, documenting the
woodwaste recovery and removal operation (refer to Condition #3).
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The Applicant is proposing to construct and maintain a PV array on an approximate 5.86-acre portion
of the 10.4-acre Site, tentatively consisting of the following components:
Approximately 7,056, 395-Watt (W) PV modules (manufacturer to be determined) that will
be mounted on pile-driven galvanized steel frame and support racks;
A total of 230 full racks and another 29 partial racks RBI Solar Fixed-Tilt Ground Mound
Solution Model GM-2, supporting 14 modules per rack;
The racking system will hold the modules at a fixed tilt of 20 degrees facing south. Approximately
3,423 modules will be installed within the area of Site Assignment. The supporting appurtenances
to the system will include inverters, DC converters, neutral grounding reactors, transformers, a
Data Acquisition System (DAS), and several pile-driven utility poles.
The Applicant is proposing to install a battery storage system (manufacturer and model are to be
determined). The system will be used to store energy generated by the PV array to inject into the
grid at times of need. Interconnection agreement with Eversource will be established to allow
electric power generated by the solar array to be distributed through the local distribution circuit.
The Applicant is proposing to stabilize construction entrance off Freeman’s Way by placing a
concrete pad. The concrete pad will be a minimum 50 inches long, 15 inches wide and raised 8
inch above grade with a 2 inch diameter coarse aggregate overlain by geotextile filter fabric.
Glare Analysis: The Town of Brewster Zoning Board of Appeals required NextGrid to identify
potential impacts resulting from the proposed project and to comply with the local zoning
regulations in the Town’s Bylaws. The zoning regulations include potential glare impact resulting
from the proposed project. The project was granted a variance from the Zoning Board of Appeals
on December 1, 2020. The Engineer has indicated that the elevation at the bottom of the pit is
approximately between 20- and 30-feet below the street level; therefore, the proposed project will
not have a direct visual sight that will impact the surrounding facilities and/or community. The
Application has also indicated that the panels will be coated in anti-glare material (refer to
Condition #5).
Stormwater: Temporary drainage will be provided during construction by constructed drainage
swales. Final grading will divert stormwater toward a central location where a permanent
stormwater drainage system will be constructed. The system will consist of six (6) precast leaching
catch basins in a 62- by 10-feet gallery configuration, located on Site beneath the proposed PV
array. A 12-inch thick layer of crushed stone, approximately 1-inch diameter, will be placed below
the leaching pit. Silt controls will be put in place until ground cover has been established through
revegetation, wherein a portion of stockpile topsoil will be used to support natural grasses planned
for ground stabilization. A silt barrier surrounding the leaching gallery will be constructed of
staked coir rolls or equivalent.
Site Security: For security purposes, the Applicants are proposing to enclose the PV array with a
chain link fence. The fence will be 7 feet high, and is fabricated with 2 inches mesh size, 9-gauge,
galvanized chain link fabric, top and bottom selvage knuckled. All the fence posts, including the
line posts and terminal posts will be constructed with 12 inches diameter concrete footing onto a
compacted subgrade to a depth of 4 feet below final grade. A double swing gate will be installed
at the entrance off Freeman’s Way (refer to Condition #9).
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Decommissioning Plan and Financial Assurance Mechanism: With the removal of the woodwaste
and submittal of a BWP SW-43 Closure Completion permit application to MassDEP (refer to
Conditions #2 and #3), there will be no solid waste on Site. The Applicant will purchase the
property where the proposed PV array will be constructed; therefore, as the owner of the Site, the
Applicant is not required to submit a decommissioning plan. The Application indicated that the
Site Assignment will be terminated. A copy of the Site Assignment termination shall be submitted
to MassDEP. Financial Assurance Mechanism shall be required if the Site Assignment is not
terminated accordingly.
IV. APPLICATION REVIEW AND DECISION PROCESS:
The Application was submitted and reviewed pursuant to the provisions of 310 CMR 19.029(2):
Applicable Permit Procedures and 310 CMR 19.033: Permit Procedure for an Application for a
Permit Modification or Other Approval. According to these review procedures, MassDEP’s
decision regarding the proposed activities shall be either: a “Provisional Decision” pursuant to 310
CMR 19.033(4)(a); or a non-provisional decision pursuant to 310 CMR 19.033(4). MassDEP has
determined that non-provisional decision is inappropriate for this Application.
MassDEP reviewed the Application pursuant to 310 CMR 19.000: Solid Waste Management and
MassDEP’s Landfill Technical Guidance Manual, May 1997 (the “Manual”).
V. PERMIT DECISION:
MassDEP, having determined the information in the Application is satisfactory and in accordance
with its authority granted pursuant to M.G.L. c.111, s. 150A, and 310 CMR 19.000, hereby
APPROVES the Post-Closure Use of the Daniels Antinarelli Stump Dump for a Solar Photovoltaic
Array subject to the conditions identified herein.
1. Permit Limitations: The issuance of this approval is limited to the proposed Solar Photovoltaic
Array at the Site Assigned parcels as detailed in the Application and does not relieve the
Applicants from the responsibility to comply with all other regulatory or permitting
requirements. Post-Closure Use construction shall proceed in complete compliance with the
approved plans, MassDEP's regulations and requirements, the Manual or as required by this
Approval. There shall be no deviation from this Approval without prior consent from MassDEP.
2. Pre-Construction Work: Prior to construction, the Applicant shall remove all remaining
woodwaste at the Site in a timely manner and document that all woodwaste has been handled
(i.e. means processing, storing, transferring or treating a material or solid waste) in accordance
with 310 CMR 16.02, consistent with MassDEP’s letter to NextGrid, Inc. dated November 3,
2020. Any processed woodwaste (i.e., woodchips) may be used as landscaping material (e.g.
erosion control) but MassDEP prohibits the use of these woodwaste as a fill material. Materials
that do not qualify for reuse at the Site must be transported off-site to a facility that is permitted
and licensed to accept the materials in accordance with the Solid Waste Regulations, where
applicable.
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3. Pre-Construction Submittals:
1) The Applicant is required to submit a BWP SW-43 Closure Completion permit application
documenting all the woodwaste recovery work for MassDEP review and approval.
2) At least 30 days prior to Construction, the Applicant shall submit to MassDEP for review
and approval the Final Design of the proposed PV array system, including, but not limited
to, any structural (stability) analysis of the PV array system and all associated
appurtenances, any manufacturer technical specifications of the PV array system, and any
revised site plan and/or civil design drawings that differ from the submittal in this
application.
4. Permit Modification: MassDEP reserves the right to ask for submittal of permit modification
(SW-37) from the Applicant should the Final Design of the proposed PV array system
constitutes a major modification from its initial design. The Applicant should consult with
MassDEP to determine whether a permit modification is required.
5. Solar Glare Analysis/Remediation: The Applicant shall monitor the solar glare from the solar
panels as they are installed to confirm that no off-site glare issues develop. No portion of the
array shall cause reflective glare to any motorist in any direction or impact the general public.
The Applicant shall take remedial actions if a problem develops during or after installation of
panels.
6. Notification of Construction: The Applicant shall notify MassDEP, Southeast Regional Office
Solid Waste Section Chief, in writing (email is acceptable, to mark.daker@mass.gov) when
the post-closure use construction commences, provided that Conditions #2 and #3 have been
completed, and again when the construction is completed.
7. Regulatory Compliance: The Applicants, Engineer and Applicants’ Contractors shall fully
comply with all applicable local, state and federal laws, regulations and policies, by-laws,
ordinances and agreements. This includes but is not limited to, 310 CMR 19.142: Post-Closure
Requirements, 310 CMR 19.143: Post-Closure Use of Landfills, and 310 CMR 19.043:
Standard Conditions. Applicable federal regulations include, but are not limited to, 29 CFR
Part 1910, OSHA standards governing employee health and safety in the workplace and all
applicable local, state and federal electrical codes and permits, including National Electrical
Code (NEC), 2011 Edition, Article 690-"Solar Photovoltaic (PV) Systems".
8. Health and Safety: The Applicants, Engineer and Applicants’ Contractors are responsible to
ensure all necessary precautions are taken to protect the health and safety of workers and the
general public during both the construction phase and during the operation and maintenance
phase of the post-closure use.
A site-specific Health and Safety Plan for the construction period shall be developed and
submitted to MassDEP (for its record) prior to any commencement of construction activity.
9. Site Security: Pursuant to 310 CMR 19.130(23) the Applicant is required to provide sufficient
fences or other barriers to prevent unauthorized access to the Site. The Applicant must continually
monitor and evaluate the potential for unauthorized access and institute all appropriate measures
to prevent unauthorized access during the closure and post-closure period.
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10. Certification Report: Within ninety (90) days of completing the installation of the solar
photovoltaic array, MassDEP shall be provided with a certification report for MassDEP’s
records. All construction work shall be completed under the supervision of a Massachusetts
Registered Professional Engineer who shall have sufficient staff on-site to provide quality
assurance/quality control (QA/QC) oversight for all construction work at the Site. The report
shall be signed and stamped by a Massachusetts-registered professional engineer and include, at
a minimum, written certification from the supervising engineer that the project was performed
in accordance with MassDEP regulations, requirements and the approved Post Closure Use
permit application. The report shall include a project narrative, as-built drawings depicting all
pertinent site features and photographs representative of the construction processes and
completed work. Should the Applicant desire a formal review and written approval of the
certification report, the Applicant must submit a formal BWP SW 43, Landfill Closure
Completion permit application.
11. Entries and Inspections: In accordance with 310 CMR 19.043: Standard Conditions, MassDEP
and its agents and employees shall have the right to inspect the Site and any equipment, structure
or land located thereon, take samples, recover materials or discharges, have access to and
photocopy records, to perform tests and to otherwise monitor compliance with this permit and
all environmental laws and regulations.
12. Permit Transfer: Pursuant to 310 CMR 19.044, no sale, assignment, or transfer of the rights or
privileges, or effective control of such rights or privileges, granted under a permit to establish,
expand, construct, operate or maintain a facility shall be valid until a responsible official of the
transferee submits a transfer certification, using a BWP SW 49 application form, in accordance
with 310 CMR 19.011(1) to MassDEP. Accordingly, the Applicant is jointly and severably
liable for maintaining the PV array as specified in this permit and for adhering to the permit
conditions, unless and until a properly completed BWP SW49 application is submitted to
MassDEP. The Applicant should refer to 310 CMR 19.044 and the BWP SW 49 application
form for the complete permit transfer requirements.
13. Reservation of Rights: MassDEP reserves the right to require additional assessment or action, as
deemed necessary to protect and maintain an environment free from objectionable nuisance
conditions, dangers or threats to public health, safety and the environment. MassDEP reserves
all rights to suspend, modify or rescind this permit if it determines the PV array results in a threat
to public health, safety or the environment.
This approval pertains only to the Solid Waste Management aspects of the proposal does not
negate the responsibility of the owners or operators to comply with any other local, state or
federal laws, statutes and regulations or enforcement actions, including orders issued by
another agency now or in the future. Nor does this approval limit the liability of the owners or
otherwise legally responsible parties from any other applicable laws, statutes or regulations
now or in the future.
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VI. REVIEW OF DECISION:
Review of Decision: Pursuant to 310 CMR 19.033(4)(b), if the Applicants are aggrieved by
MassDEP’s decision to issue this decision, it may within twenty-one days of the date of issuance
file a written request that the decision be deemed provisional, and a written statement of the basis
on which the Applicants believe it is aggrieved, together with any supporting materials. Upon
timely filing of such a request, the decision shall be deemed a provisional decision with an
effective date twenty-one days after MassDEP’s receipt of the request. Such a request shall
reopen the administrative record, and MassDEP may rescind, supplement, modify, or reaffirm its
decision. If MassDEP reaffirms its decision, the decision shall become final decision on the
effective date. Failure by the Applicants to exercise the right provided in 310 CMR 19.033(4)(b)
shall constitute waiver of the Applicants’ right to appeal.
VII. RIGHT TO APPEAL:
Right to Appeal: This approval has been issued pursuant to M.G.L. Chapter 111, Section 150A,
and 310 CMR 19.033: Permit Procedure for an Application for a Permit Modification or Other
Approval, of the “Solid Waste Management Regulations”. Pursuant to 310 CMR 19.033(5), any
person aggrieved by the final permit decision, except as provided for under 310 CMR
19.033(4)(b), may file an appeal for judicial review of said decision in accordance with the
provisions of M.G.L. Chapter 111, Section 150A and M.G.L. Chapter 30A no later than thirty
days following the date of issuance of the final permit decision to the Applicants. The standing
of a person to file an appeal and the procedures for filing such an appeal shall be governed by the
provisions of M.G.L. c. 30A. Unless the person requesting an appeal requests and is granted a
stay of the terms and conditions of the permit by a court of competent jurisdiction, the permit
decision shall be effective in accordance with the terms of 310 CMR 19.033(3).
Notice of Appeal: Any aggrieved person intending to appeal a final permit decision to the Superior
Court shall first provide notice of intention to commence such action. Said notices of intention
shall include MassDEP Authorization Number: SW37-0000015 and shall identify with
particularity the issues and reason why it is believed the final permit decision was not proper. Such
notice shall be provided to the Office of General Counsel of MassDEP and the Regional Director
for the regional office which processed the permit application, if applicable at least five days prior
to filing of an appeal. The appropriate addresses to send such notices are:
Office of General Counsel Regional Director
Department of Environmental Protection Department of Environmental Protection
One Winter Street 20 Riverside Drive
Boston, MA 02108 Lakeville, MA 02347
No allegation shall be made in any judicial appeal of a final permit decision unless the matter
complained of was raised at the appropriate point in the administrative review procedures
established in 310 CMR 19.000, provided that a matter may be raised upon showing that it is
material and that it was not reasonably possible with due diligence to have been raised during such
procedures or that matter sought to be raised is of critical importance to the environmental impact
of the permitted activity.
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If you have any questions or comments regarding this approval letter, please contact me at (508)
946-2847 or Elza Bystrom at (508) 946-2856 or write to the letterhead address.
Very truly yours,
Mark Dakers, Chief
Solid Waste Management Section
Bureau of Air and Waste
D/EB
Cc: Brewster Building Department
2198 Main St.
Brewster, MA 02631
Ec: Brewster Board of Health
brhealth@brewster-ma.gov
Michael Antinarelli
amaexec@gmail.com
Bennett Environmental Associates, LLC
David Bennett - dbennett@NSUWater.com
DEP-Boston
ATTN: G. Cooper
J. Fischer
DEP- SERO
ATTN: S. Pickering
M. Dakers
GROUNDWATER MONITORING AND
THIRD PARTY INSPECTION REPORT
November 2020
Cape Sand & Recycling, LLC
Wood Waste Reclamation Facility
Brewster, Massachusetts
K10740A
DECEMBER 23, 2020
GROUNDWATER MONITORING AND
THIRD PARTY INSPECTION REPORT
November 2020
Cape Sand & Recycling, LLC
Wood Waste Reclamation Facility
Brewster, Massachusetts
K10740A
DECEMBER 23, 2020
Prepared for:
MA Department of Environmental Protection
Southeast Regional Office, BAW/Solid Waste Section
20 Riverside Drive – Lakeville, MA 02347
and
Brewster Water Quality Review Committee
Brewster Town Hall
2198 Main Street – Brewster, MA 02631
On Behalf Of:
Cape Sand & Recycling, LLC
1515 Freemans Way
Brewster, MA 02631
Jay Merchant, Owner
Prepared by:
BENNETT ENVIRONMENTAL ASSOCIATES, LLC
1573 Main Street
Brewster, MA 02631
John Tadema-Wielandt, Manager of Environmental Services
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CAPE SAND & RECYCLING, LLC
WOOD WASTE RECLAMATION FACILITY
SEMI‐ANNUAL GROUNDWATER MONITORING REPORT
NOVEMBER 2020 SAMPLING EVENT
1.0 INTRODUCTION
This Groundwater Monitoring Report has been prepared to provide the Massachusetts Department of
Environmental Protection (MassDEP) and the Town of Brewster Water Quality Review Committee
(BWQRC) with results of the November 2020 groundwater sampling event, associated with the Wood
Waste Reclamation Facility (WWRF) located at 1515 Freemans Way in Brewster, Massachusetts,
currently operated by Cape Sand & Recycling, LLC (CS&R). Groundwater sampling was performed by
Bennett Environmental Associates, LLC (BEA) on November 17, 2020. The laboratory analyses were
performed by Alpha Analytical; the lab is appropriately certified to perform the requisite analyses. This
report, along with the six‐month Third‐Party Inspector’s report, is being filed with the Mass DEP and the
BWQRC as part of the conditional approvals for the small WWRF handling facility.
2.0 GROUNDWATER MONITORING PROGRAM
2.1 Background
On December 29, 2009, the MassDEP issued a Provisional Approval – Authorization to Operate (ATO) a
Small Handling Facility/Wood Waste Reclamation to CS&R. The ATO approval included requirements for
continuation of the groundwater monitoring program that had been previously developed to comply
with the MassDEP “Wood Waste Reclamation Facilities Siting and Permitting Requirements” Guidance
Document ‐ #BWP‐98‐006 (the WWRF Guidance Document), the Massachusetts Contingency Plan (MCP,
310 CMR 40.0000), and the requirements of the Brewster Water Quality Review Committee (BWQRC).
On October 19, 2010, MassDEP issued a Provisional Approval – Modification of a Small Handling
Facility/Wood Waste Reclamation Facility, which included a determination deeming the Site Adequately
Regulated, pursuant to the applicable provisions of both the MCP and the Solid Waste Regulations (310
CMR 19.00). The Modification Approval also included a reduction in the number of groundwater
sampling locations from six (6) to four (4) monitoring wells, eliminating former MCP‐related monitoring
locations. The groundwater monitoring wells included under the approved MassDEP program are MW‐1
(replaced by MW‐1R), MW‐3A, MW‐4A and MW‐5. These monitoring wells are routinely sampled for the
full list of parameters included in the Groundwater Monitoring Appendix of the WWRF Guidance
Document. Total Phosphorus was added as a parameter in November 2015, at the request of the
BWQRC.
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The BWQRC has also requested retaining two (2) additional down‐gradient monitoring wells (MW‐3B
and MW‐5B) within the monitoring program, to evaluate groundwater conditions up‐gradient of the
Timberlane Drive neighborhood, where private drinking‐water wells are currently in‐use. These
monitoring wells are also sampled for Manganese to evaluate concentrations in these downgradient
wells. MW‐3B and MW‐5B are also sampled for nitrogen‐related parameters when concentrations of
Nitrate/Total Nitrogen are reported above the MMCL of 10 mg/L, in any of the MW‐3A, MW‐4A or MW‐
5 monitoring wells. These down‐gradient wells were sampled for Nitrate/Total Nitrogen during the
November 2020 sampling event, as Nitrate and Total Nitrogen were reported above the MMCL of 10
mg/L in MW‐3A in May 2020. Each of the groundwater monitoring well locations are shown on the
enclosed Site Plan dated 12/2/20.
2.2 Groundwater Sample Collection
Groundwater samples were collected by BEA personnel on November 17, 2020, from monitoring wells
MW‐1R, MW‐3A, MW‐3B, MW‐4A, MW‐5, and MW‐5B. A Monitoring Well Sampling Log is attached for
reference. Prior to sampling, depth‐to‐groundwater measurements were taken at each monitoring well
location. The wells were then purged in accordance with MassDEP standard practices and BEA Quality
Assurance & Quality Control (QA/QC) methods. Field parameters measured during sampling activities
included temperature, pH, conductivity, dissolved oxygen (DO) and oxidation‐reduction potential (ORP).
The groundwater samples were collected using a variable‐speed 2” submersible pump, using low‐flow
sampling methodology. Samples were collected for all required parameters including total metals, as
well as dissolved metals, which were field‐filtered using an in‐line 0.45 Micron filter. The laboratory was
instructed to hold the dissolved metals samples pending results of the total metals samples. Sample
containers were prepared by Alpha Analytical and kept in a cooler or refrigerator pending pick up by a
lab courier and transported following chain of custody procedures.
2.3 Groundwater Gauging Data
Well gauging from the date of sampling reports groundwater elevations ranging from 22.43 to 23.17
feet (NGVD), as measured from the top of the well casings. The November 2020 gauging event shows
groundwater flows to the southeast towards Pleasant Bay, consistent with data from previous
monitoring events. Depth‐to‐groundwater measurements and corresponding elevations are presented
on the enclosed Monitoring Well Sampling Log. Groundwater contours are represented on the enclosed
Site Plan dated 12/2/20.
3.0 GROUNDWATER ANAYLTICAL RESULTS
Groundwater analytical results were compared to the Massachusetts Drinking Water Standards
(MDWS), published by MassDEP. These standards include Massachusetts Maximum Contaminant Levels
(MMCLs), Secondary Maximum Contaminant Levels (SMCLs) and Office of Research and Standards
Guideline (ORGS) concentrations. In addition, the results were compared to the MCP Method 1 Risk
Characterization Standards for the GW‐1 (ingestion) and GW‐3 (discharge to surface water)
groundwater categories. A tabulation of the laboratory data for the November 2020 sampling event,
along with a comparison to the above standards, is presented in Table 1: Results of Groundwater
3
Analyses Compared to Various Standards. The results of semi‐annual groundwater data over the past
three (3) years are presented in Table 2: Temporal Groundwater Analysis Summary – May 2018 through
November 2020.
3.1 Total Metals
Groundwater samples collected from MW‐1R, MW‐3A, MW‐4A, and MW‐5 were analyzed for Total
Arsenic, Barium, Cadmium, Chromium, Copper, Iron, Lead, Manganese, Mercury, Selenium, Silver and
Zinc. Monitoring wells MW‐3B and MW‐5B were sampled for Total Manganese only. Arsenic was
reported in monitoring well MW‐1R and MW‐3A at 0.0564 mg/L and 0.0166 mg/L, respectively, above
the Massachusetts Drinking Water Standard (0.01 mg/L), as well as the Method 1 GW‐1 Risk
Characterization Standard, pursuant to the Massachusetts Contingency Plan (MCP). BEA returned to the
property on December 11, 2020 and collected a sample from downgradient monitoring well MW‐3B for
arsenic analysis. Results of the analysis reported concentrations of arsenic in MW‐3B as Non‐Detect.
These results confirm that elevated concentrations of arsenic remain localized and are not migrating off
the subject property.
Release Notification was made to the DEP for the presence of similar concentrations of Arsenic in
groundwater in 2008. In 2009, the Site was listed as Adequately Regulated under the MCP, wherein
such localized impacts are confined to the property. Therefore, Release Notification to the MA DEP
pursuant to 310 CMR 40.0315, is not required.
Historically, similar concentrations of Arsenic, have been reported in monitoring wells MW‐1 (May 2014)
and MW‐3A (May/November 2012). Arsenic has consistently been reported above the MA Drinking
Water Standards and Method 1 GW‐1 Standards in monitoring well MW‐1R since November 2016, with
concentrations ranging from 0.058 mg/L to 0.018 mg/L. The elevated concentrations of total metals
reported in MW‐1R are attributed to naturally occurring metals being leached from native soils in a
reducing environment, which is a result of decaying organic matter, associated with previously buried
wood waste being in contact with groundwater. Concentrations of Arsenic, Iron and Manganese in MW‐
3A have been increasing over the past few years, as shown in Table 2. The elevated concentrations of
arsenic reported are most likely associated with the wood waste reclamation and processing activities
located directly upgradient of MW‐3A. Future sampling events will include MW‐3B and MW‐5B for
Arsenic analysis.
Total Iron was reported at concentrations exceeding Secondary Drinking Water Standards (SMCLs) in
groundwater samples collected from MW‐1R, MW‐3A, MW‐4 and MW‐5. The highest concentration of
Total Iron was reported at MW‐1R (82.5 mg/L). SMCLs are not health‐based standards but were
established to preserve the aesthetic qualities (i.e., odor and taste) of drinking water. In October 2013,
the MassDEP adopted an Office of Research and Standards Guideline (ORSG) for manganese based on a
modified version of the US EPA Health Advisory for this element. The OSRG considers lifetime exposure
(0.3 mg/L) and acute exposure (1.0 mg/L) for the general population, as well as a precautionary standard
for acute exposure for children <1 year old (0.3 mg/L). Total Manganese was reported at concentrations
exceeding the SMCL and OSRG in groundwater samples collected from all of the wells sampled, with the
exception of MW‐5B, where Manganese was reported below the OSRGs for chronic and acute
exposures. Iron and Manganese dissolve more readily in low oxygen environments and where the
4
groundwater is slightly acidic. This is consistent with the field parameters measured during the
November 2020 sampling event, wherein all wells exhibit Dissolved Oxygen concentrations below 1.0
mg/L, with the exception of MW‐3B and MW‐5B, where the lowest and third lowest concentrations of
Manganese were reported, respectively.
The tracking charts below show concentrations of Iron, Manganese and Arsenic over the past three
years. In general, Iron concentrations appear to be on an increasing trend over the past few years.
Manganese concentrations appear to be decreasing over time in MW‐5 and increasing slightly in the
other wells. Arsenic concentrations do not appear to show any clear trends, with higher concentrations
observed sporadically in MW‐1R in November 2019 and November 2020, and the higher concentration
most recently observed in MW‐3A.
0
10
20
30
40
50
60
70
80
90
100
mg/LSampling Date
Total Iron Concentrations in Selected Wells Over Time
MW ‐1R
MW ‐4A
MW ‐3A
MW ‐5
0
5
10
15
20
25
mg/LSampling Date
Total Manganese Concentrations in Selected Wells
Over Time
MW‐1R
MW‐4A
MW‐3A
MW‐5
5
3.2 Volatile Organic Compounds (VOCs)
Groundwater samples collected from monitoring wells MW‐1R, MW‐3A, MW‐4A, and MW‐5 were
analyzed for VOCs via EPA Method 8260. There were no VOCs reported in any of the wells tested above
the laboratory detection limits.
3.3 Poly‐nuclear Aromatic Hydrocarbons (PAHs)
Groundwater samples collected from monitoring wells MW‐1R, MW‐3A, MW‐4A, and MW‐5 were
analyzed for PAHs. There were no PAHs detected, in any of the wells sampled, at concentrations above
the laboratory reporting limits.
3.4 Aggregate Organic Constituents
Groundwater samples collected from monitoring wells MW‐1R, MW‐3A, MW‐4A, and MW‐5 were
analyzed for Tannin & Lignin, Chemical Oxygen Demand (COD) and Total Organic Carbon (TOC). Tannin &
Lignin was reported as Non‐Detect in monitoring well MW‐4A, with concentrations from the remaining
wells ranging from 1.5 to 2.8 mg/L. The highest concentration of Tannin & Lignin was reported in MW‐
3A at 2.8 mg/L. COD was also reported as Non‐Detect in MW‐4A. The highest concentration of COD
was reported in MW‐3A (100 mg/L) with lower concentrations reported in MW‐1R (68 mg/L) and MW‐5
(48 mg/L). Concentrations of TOC were reported in all wells, with the highest concentration reported in
MW‐3A (33 mg/L). Significant decreases in Tannin & Lignin, COD and TOC were observed in MW‐1R
from the previous sampling event, with slight increases of Tannin & Lignin, COD and TOC observed in
MW‐3A. Monitoring well MW‐1R is influenced by residual buried organics, where black sand was
observed above the groundwater interface during well installation. Additionally, monitoring well MW‐
3A, located directly downgradient of the working buried wood waste, has historically been most
impacted by organic influence as reflected in these parameters. There are no regulatory standards
established for these parameters. Historical data for these parameters are presented in Table 2.
0
0.01
0.02
0.03
0.04
0.05
0.06
0.07
mg/LSampling Date
Total Arsenic Concentrations in Seclected Wells Over
Time
MW‐1R
MW‐4A
MW‐3A
MW‐5
6
3.5 Formaldehyde
Groundwater samples collected from monitoring wells MW‐1R, MW‐3A, MW‐4A, and MW‐5 were
analyzed for formaldehyde. No concentrations of formaldehyde were detected in any monitoring wells
above the method detection limits.
3.6 General Chemistry
Groundwater samples collected from MW‐1R, MW‐3A, MW‐4A, and MW‐5 were analyzed for general
chemistry parameters including Alkalinity, Chloride, Total Cyanide, Sulfate, Sulfide and Total Dissolved
Solids (TDS). Historic data for the general chemistry parameters is presented in Table 2.
The highest alkalinity value of 230 mg/L was reported at MW‐1R. There are no regulatory
standards for alkalinity.
Chloride was detected in all wells at concentrations between 7.8 mg/L and 54 mg/L. All of the
wells reported Chloride below the SMCL of 250 mg/L. The highest chloride value was reported at
monitoring well MW‐1R (54 mg/L).
Total Cyanide was not detected in any well above the method detection limit of 0.005 mg/L.
Sulfide was also not detected in any of the wells sampled.
Sulfate was reported as Non‐Detect in monitoring well MW‐4A. Sulfate concentrations were
reported in the remaining wells below the Secondary Maximum Contaminant Levels and
consistent with historic data, as shown in Table 2.
TDS concentrations were reported below the SMCL of 500 mg/L in all wells. TDS concentrations
in monitoring wells MW‐1R and MW‐3A have moderated since the May 2020 sampling event,
where significant increases were observed based on historic data, as shown in Table 2. Based
on increased organic concentrations in MW‐3A with increased TOC, COD, and tannin/lignin,
future groundwater testing will include TDS in the further down gradient MW‐3B and MW‐5B
locations while TDS concentrations remains elevated at upgradient locations. Typically,
increased organic concentrations result in a reducing environment that would leach naturally
occurring metals and increase TDS.
Groundwater samples collected from MW‐1R, MW‐3A, MW‐4A, MW‐5 were analyzed for Total Kjeldahl
Nitrogen (TKN), Nitrate, Nitrite, Total Nitrogen and Total Phosphorus. Monitoring wells MW‐3B and
MW‐5B were analyzed for TKN, Nitrate, and Total Nitrogen only.
Nitrate was not reported in any well above the Drinking Water Standard of 10 mg/L. The
highest concentration of Nitrate (3.84 mg/L) was reported in MW‐4A. All other wells reported
concentrations of Nitrate below 1.0 mg/L.
Nitrite was reported as Non‐Detect in groundwater samples collected from all wells.
TKN was reported as Non‐Detect in monitoring wells MW‐4A and MW‐5B. All concentrations of
TKN were reported were below the Drinking Water Standard of 10 mg/L, with the highest
concentration detected in MW‐3A (7.67 mg/L).
7
Total Nitrogen was reported in all wells, with concentrations ranging from 0.6 mg/L in MW‐3B to
7.9 mg/L in MW‐3A. Both Total Nitrogen and Nitrate were noted to have decreased significantly
from the May 2020 sampling event.
Total Phosphorus was detected in each of the monitoring wells sampled, with concentrations
ranging from 0.034 mg/L to 0.694 mg/L. The highest concentration was detected in monitoring
well MW‐1R (0.694 mg/L). There is no state or federal groundwater standard for Phosphorus.
3.7 Field Parameters
Field parameters [temperature, pH, specific conductivity, dissolved oxygen (DO) and oxidation‐reduction
potential (ORP)] were recorded during the November 2020 groundwater sampling event. The historic
data for the field parameters are presented on Table 2.
Groundwater temperatures varied between wells ranging from 56.3 to 68.2 degrees Fahrenheit.
pH values observed in all monitoring wells were below the Secondary Drinking Water Standard
(<6.5 S.U.), with the exception of MW‐1R and MW‐3A (6.85 S.U., 6.84 S.U.). These values are
consistent with the slightly acidic groundwater conditions typical of Cape Cod and are consistent
with historic data.
Conductivity and DO concentrations varied from well to well with higher conductivity observed
in MW‐1R, MW‐3A, and MW‐5. Low DO was observed in all wells with the exception of MW‐5B.
4.0 CONCLUSIONS
The following is a summary of the key groundwater findings of the November 2020 groundwater
monitoring event:
Total Arsenic was reported in MW‐1R and MW‐3A at 0.0564 mg/L and 0.0166 mg/L,
respectively, both above the MA Drinking Water Standard (0.01 mg/L) and Method 1 GW‐1 Risk
Characterization Standard (0.01 mg/L). Although concentrations of Arsenic in MW‐1R and MW‐
3A exceed the Method 1 GW‐1 Risk Characterization Standards, the Site is considered
Adequately Regulated under the MCP and therefore, no Notification to the MA DEP is required.
Subsequent sampling at downgradient well MW‐3B reported arsenic concentrations as Non‐
Detect, indicating that arsenic concentrations are isolated to these wells. Concentrations of
arsenic reported in MW‐1R are associated with the leaching of metals from surrounding native
sands in a reducing environment. This is caused by organic leachate from previously buried
wood waste that has since been removed. Ongoing efforts to mitigate this issue include
consolidating all wood waste in the area of Site Assignment and maintaining a 10’ separation to
groundwater in areas where new wood waste is being deposited. Concentrations of Arsenic
reported in MW‐3A are most likely associated with active wood waste reclamation and
processing occurring directly upgradient of MW‐3A. Due to these concentrations reported at
the MW‐3A monitoring well, future sampling will include MW‐3B and MW‐5B for Arsenic
analysis.
Several groundwater parameters (pH, Total Iron and Total Manganese, TDS) were reported in
groundwater at concentrations exceeding the SMCLs/OSRG parameters. These findings are
PROJECT:SCALE:BY:CHECK:JOB NUMBER:P.O. BOX 1555 - BREWSTER, MA 02631PHONE: (508) 896-1706 FAX: (508) 896-51091573 MAIN STREET - BREWSTER, MA 02631A NATURAL SYSTEMS UTILITIES COMPANYwww.bennett-ea.comGEOLOGISTS, ENGINEERS BENNETT ENVIRONMENTAL ASSOCIATES, LLC.As NotedSRFJTWK10740AA.X.EV.910TITLE:DATE:BEACAPE SAND & RECYCLING, LLCGROUNDWATER MONITORING1515 FREEMAN'S WAY - BREWSTER, MA 02631c/o JAY MERCHANTLEGENDMONITORING WELL0200400SCALE 1"=200'600SKETCH PLANSMALL WOOD WASTE HANDLING FACILITYGROUNDWATER CONTOUR 11/17/20REFERENCE- PLAN TITLED "GROUNDWATER CONTOUR PLAN", PREPAREDBY SITEC ENVIRONMENTAL, DATED FEB 2015- MASSACHUSETTS GIS, 2019 PHOTOGRAPHYNOTE: THIS SITE PLAN WAS NOT PREPARED FROM ANYINSTRUMENT SURVEY AND UNDER NO CIRCUMSTANCESSHOULD THE DISTANCES, BEARING AND/OR OTHER FEATURESSHOWN BE USED TO ESTABLISH PROPERTY LINES. ALLLOCATIONS ARE APPROXIMATE.MW-1RMW-3BMW-1(DESTROYED)MW-3AMW-2AMW-5MW-5BMW-4AMW-6SITE ASSIGNED LIMITOF WOOD WASTERECLAMATION FACILITYAPPROXIMATE PROPERTYBOUNDARYABCPROCESSINGLEAFCOMPOSTINGWOOD WASTEDIVERSIONLICENSED SITE PROFESSIONALS, ENVIRONMENTAL SCIENTISTS, 12/2/2023.123.022.9
Job Name:Cape Sand & RecyclingDate(s): Time:AM/PMTide:NALocation:1515 Freemans Way, BrewsterJob Number:K10740ASampler:JTW, RPTMeasuring Point: Ground Surface or T.O.CTOCMW-1R 37.17 20.00 14.00 6.00 23.170.96 3.0+ NT 6.85 0.12 604 58.6MW-3A 66.43 49.00 43.69 5.31 22.740.85 3.0+ NT 6.64 0.11 680 68.2MW-4A 81.97 66.00 59.14 6.86 22.831.10 3.5+ NT 5.22 0.12 110.5 61.5MW-5 77.42 64.50 54.99 9.51 22.431.52 5.0+ NT 6.06 0.72 555 63.3MW-5B 68.99 56.00 46.28 9.72 22.711.56 5.0+ NT 5.26 5.98 77.3 57.2MW-3B 31.15 17.00 8.43 8.57 22.721.37 4.5+ NT 5.36 2.91 119.3 56.3NOTES:No odor, No sheenNo odor, No sheenNo odor, No sheen NA = Not Applicable; NE = Not Established; NT = Not TakenNo odor, No sheenNo odor, No sheenNo odor, No sheenAll wells sampled after parameter stabilization11/17/20BENNETT ENVIRONMENTAL ASSOCIATES, LLCA NATURAL SYSTEMS UTILITIES COMPANYLICENSED SITE PROFESSIONALS, ENVIRONMENTAL SCIENTISTS, GEOLOGISTS, ENGINEERSMONITORING WELL SAMPLING LOG1573Main StreetBrewster, MA 02631WellNumberElev. of referencepoint (feet)TotalDepthof Well(feet)Depth toWater(feet)StandingWaterHeight(feet)WaterTableElevation(feet)Static Volume(gallons)Volume Purged(gallons)HNUPI-101(ppm)pHDissolved Oxygen(mg/L)ConductivityTemperature(F)Comments:Phone: 508-896-1706Fax: 508-896-5109
Job Name:Merchant: Cape Sand & Recycling GW MonitoringDate(s): Time:1:00 PMTide:NALocation:1515 Freemans Way, BrewsterJob Number:K10740ASampler:RPTMeasuring Point: Ground Surface or T.O.CTOCMW-3B 31.15 17.00 8.49 8.51 22.66 1.36 4.1 NA NT NT NT NTNOTES:No odor, No sheen NA = Not Applicable; NE = Not Established; NT = Not TakenGroundwater samples collected from MW-3B to quantify precense of arsenic in MW-3B12/11/20BENNETT ENVIRONMENTAL ASSOCIATES, LLCA NATURAL SYSTEMS UTILITIES COMPANYLICENSED SITE PROFESSIONALS, ENVIRONMENTAL SCIENTISTS, GEOLOGISTS, ENGINEERSMONITORING WELL SAMPLING LOG1573Main StreetBrewster, MA 02631WellNumberElev. of referencepoint (feet)TotalDepthof Well(feet)Depth toWater(feet)StandingWaterHeight(feet)WaterTableElevation(feet)Static Volume(gallons)Volume Purged(gallons)HNUPI-101(ppm)pHDissolved Oxygen(mg/L)ConductivityTemperature(F)Comments:Phone: 508-896-1706Fax: 508-896-5109
0.01 0.01 0.9 0.0564 0.0166 <0.005 <0.005 NA NA
2 2 50 0.017 0.032 <0.01 0.048 NA NA
0.005 0.005 0.004 <0.004 <0.004 <0.004 <0.004 NA NA
0.100 0.100 0.300 <0.01 <0.01 <0.01 <0.01 NA NA
1.3 NS NS <0.01 <0.01 <0.01 <0.01 NA NA
0.3 S NS NS 82.5 23.6 0.084 31.6 NA NA
0.015 0.015 0.010 <0.01 0.01 <0.01 <0.01 NA NA
0.05 S, 0.3/1.0 G NS NS 5.96 4.44 1.33 12.2 1.52 0.127
0.002 0.002 0.020 <0.0002 <0.0002 <0.0002 <0.0002 NA NA
0.05 0.050 0.100 <0.01 <0.01 <0.01 <0.01 NA NA
0.1 S 0.100 0.007 <0.007 <0.007 <0.007 <0.007 NA NA
5 S 5 0.900 <0.05 <0.05 <0.05 <0.05 NA NA
I I I ND ND ND ND NA NA
NS 0.010 20 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.020 6 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.030 0.040 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.060 0.030 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.001 1 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
0.0002 0.0002 0.500 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.001 0.400 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.050 0.020 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.001 0.100 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.002 0.070 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.0005 0.040 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.090 0.200 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.030 0.040 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.0005 0.100 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.140 20 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.040 10 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS 0.080 0.020 <0.0001 <0.0001 <0.0001 <0.0001 NA NA
NS NS NS 1.5 2.8 <0.2 2.4 NA NA
NS NS NS 68 100 <20 48 NA NA
NS NS NS 20 33 0.87 15 NA NA
NS NS NS <0.075 <0.75 <0.75 <0.75 NA NA
NS NS NS 230 202 30.5 180 NA NA
250 S NS NS 54 48 7.8 44 NA NA
0.2 0.2 0.030 <0.005 <0.005 <0.005 <0.005 NA NA
10 NS NS 1.75 7.67 <0.300 3.84 0.304 <0.300
10 NS NS 0.1 0.19 3.84 0.247 0.304 0.88
1 NS NS <0.05 <0.05 <0.05 <0.05 NA NA
NS NS NS 2.1 7.9 3.8 4 0.6 0.88
NS NS NS 0.694 0.166 0.034 0.141 NA NA
250 S NS NS 33 100 <10 74 NA NA
NS NS NS <0.1 <0.1 <0.1 <0.1 NA NA
500 S NS NS 430 470 86 400 69 34
NS NS NS 58.6 68.2 61.5 63.3 56.3 57.2
6.5-8.5 S NS NS 6.85 6.64 5.22 6.06 5.36 5.26
NS NS NS 604 680 110.5 555 119.3 77.3
NS NS NS 0.12 0.11 0.12 0.72 2.91 5.98
NS NS NS -224 -145.9 142.1 -5.2 57.9 144.2
MDWS = Massachusetts Drinking Water Standard (MMCL)
GW-1 = Massachusetts MCP Method 1 GW-1 standard
GW-3 = Massachusetts MCP Method 1 GW-3 standard
G = Massachusetts Drinking Water Guideline (ORSG)
S = Secondary Maximum Contaminant Levels (SMCL)
NA = Not Analyzed for Indicated Compound
NS = No Standard
I = VOCs Standards Specific to Individual Compound
U↓ = All VOC Compounds Analyzed but not found, except Compound Specified Below
U = Analyzed but not found; detection limit listed
= Indicates an exceedance of MMCL, ORSG, or Method 1 Standard
= Indicates an exceedance of SMCL
= Analyzed but not found; detection limit above a Standard
RESULTS (mg/l)
TOTAL METALS
FIELD PARAMETERS
Sulfate
MW-5 MW-3B MW-5B
ALDEHYDES
GENERAL CHEMISTRY
Table 1: Results of Groundwater Analyses Compared to Various Standards
Brewster Sand and Recycling - Samples collected 11/17/2020
Manganese
Mercury
STANDARDS (mg/l)
MW-4A
Chemical Oxygen Demand (COD)
Naphthalene
Phenanthrene
Pyrene
Indeno(1,2,3-cd)Pyrene
Tannin & Lignin
Total Organic Carbon (TOC)
Specific Conductivity (uS/cm)
Alkalinity (as CaCO3)
Chloride
Cyanide, Total
Nitrate-N
Temperature (oF)
Fluoranthene
Fluorene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Selenium
Silver
Zinc
Dibenzo(a,h)anthracene
Benzo(ghi)perylene
Benzo(k)fluoranthene
Chrysene
Total VOCs
MW-3APARAMETERMDWS MW-1RGW-1 GW-3
AGGREGATE ORGANIC CONSTITUENTS
VOLATILE ORGANIC COMPOUNDS (VOCs)
POLY-NUCLEAR AROMATIC HYDROCARBONS (PAHs)
Lead
Arsenic
Barium
Cadmium
Chromium
Copper
Iron
Dissloved Oxygen
Oxidation Reduction Potential (mV)
Formaldehyde
Total K Nitrogen (TKN)
Nitrite-N
Nitrogen, Total
Total Phosphorus
Sulfide
Total Dissolved Solids
pH (pH units)
PARAMETERMay-18 Nov-18 May-19 Nov-19 May-20 Nov-20 May-18 Nov-18 May-19 Nov-19 May-20 Nov-20 May-18 Nov-18 May-19 Nov-19 May-20 Nov-20 May-18 Nov-18 May-19 Nov-19 May-20 Nov-20Arsenic 0.01 0.01 0.90.018 0.024 0.021 0.0580.0175 0.0564<0.001 0.0012 0.0020 0.006<0.0050.0166<0.001 <0.001 <0.001 <0.0010<0.005 <0.0050.0020 0.0019 0.002 0.002<0.005 <0.005Barium 2 2 50 <0.050 <0.050 <0.050 <0.0500.016 0.017<0.050 <0.050 <0.050 <0.050 0.059 0.032 <0.050 <0.050 <0.050 <0.050<0.01 <0.010.061 0.059 0.0602 0.066 0.066 0.048Cadmium 0.005 0.005 0.004 <0.001 <0.001 <0.001 <0.0010<0.004 <0.004<0.001 <0.001 <0.001 <0.0010<0.004 <0.004<0.001 <0.001 <0.001 <0.0010<0.004 <0.004<0.001 <0.001 <0.001 <0.0010<0.004 <0.004Chromium 0.100 0.100 0.300 <0.050 <0.050 <0.050 <0.050<0.01 <0.01<0.050 <0.050 <0.050 <0.050<0.01 <0.01<0.010 <0.050 <0.050 <0.050<0.01 <0.01<0.050 <0.050 <0.050 <0.050<0.01 <0.01Copper 1.3 NS NS <0.010 <0.010 <0.010 <0.010<0.01 <0.01<0.010 <0.010 <0.010 <0.0100.013 <0.01<0.010 <0.010 <0.010 <0.010<0.01 <0.01<0.010 <0.010 <0.010 <0.010<0.01 <0.01Iron0.3/1.0 GNS NS43.8 19.1 32.2 52.351.6 82.5<0.1001.14 2.21 9.610.23223.60.136 0.103 <0.100 <0.0500 <0.050.084 7.54 12.1 22.1 30.3 28.8 31.6Lead 0.015 0.015 0.010 <0.001 <0.001 0.002 <0.0010<0.01 <0.01<0.001 <0.001 <0.001 <0.0010<0.01 0.01<0.001 <0.001 <0.001 <0.0010<0.01 <0.01<0.001 <0.001 <0.001 0.0010<0.01 <0.01Manganese0.3 GNS NS1.99 0.734 1.450 2.892.56 5.96<0.0100.308 0.844 2.76 2.76 4.44 1.12 1.06 1.02 1.14 1.14 1.33 15.7 19 17.7 15.5 13.5 12.2Mercury 0.002 0.002 0.020 <0.0005 <0.0005 <0.0005 <0.0005<0.0002 <0.0002<0.0005 <0.0005 <0.0005 <0.0005<0.0002 <0.0002<0.0005 <0.0005 <0.0005 <0.0005<0.0002 <0.0002<0.0005 <0.0005 <0.0005 <0.0005<0.0002 <0.0002Selenium 0.05 0.050 0.100 0.004 <0.002 <0.002 <0.0020<0.01 <0.01<0.002 <0.002 <0.002 <0.0020<0.01 <0.01<0.002 <0.002 <0.002 <0.0020<0.01 <0.01<0.002 <0.002 <0.002 <0.0020<0.01 <0.01Silver0.1 S0.100 0.007 <0.001 <0.001 <0.001 <0.0010<0.007 <0.007<0.001 <0.001 <0.001 <0.0010<0.007 <0.007<0.001 <0.001 <0.001 <0.0010<0.007 <0.007<0.001 <0.001 <0.001 <0.0010<0.007 <0.007Zinc5 S5 0.900 <0.10 <0.10 <0.10 <0.10<0.05 <0.05<0.10 <0.10 <0.10 <0.10<0.05 <0.05<0.10 <0.10 <0.10 <0.10<0.05 <0.05<0.10 <0.10 <0.10 <0.10<0.05 <0.05Total VOCs I I I ND ND 0.017 ND 0.780 ND ND ND ND 0.0031 ND ND ND ND ND ND ND ND ND ND ND ND ND ND2-Butanone (MEK)4.0 G4 50 ND ND 0.005 ND 0.360 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NDAcetone6.3 G6.3 50 ND ND 0.012 ND 0.420 ND ND ND ND 0.0031 ND ND ND ND ND ND ND ND ND ND ND ND ND ND2-Methylnaphthalene NS 0.010 20 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Acenaphthene NS 0.020 6 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Acenaphthylene NS 0.030 0.040 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Anthracene NS 0.060 0.030 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001<0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Benzo(a)anthracene NS 0.001 1 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Benzo(a)pyrene 0.0002 0.0002 0.500 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Benzo(b)fluoranthene NS 0.001 0.400 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Benzo(ghi)perylene NS 0.050 0.020 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Benzo(k)fluoranthene NS 0.001 0.100 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Chrysene NS 0.002 0.070 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Dibenzo(a,h)anthracene NS 0.0005 0.040 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Fluoranthene NS 0.090 0.200 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Fluorene NS 0.030 0.040 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Indeno(1,2,3-cd)Pyrene NS 0.0005 0.100 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Naphthalene NS 0.140 20 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Phenanthrene NS 0.040 10 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Pyrene NS 0.080 0.020 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001Tannin & Lignin NS NS NS 1.5 1.9 5.3 <0.30 13 1.5 <0.12 0.45 0.44 1.7 1.3 2.8 <0.12 0.14 <0.12 <0.12 <0.2 <0.2 1.4 8.0 16 7.1 1.9 2.4Chemical Oxygen Demand (COD) NS NS NS 22 19 32 43 500 68 <10 <10 <10 26 86 100 <10 <10 <10 <10 <20 <20 34 35 38 44 73 48Total Organic Carbon (TOC) NS NS NS 7.3 8.5 12.0 15 170 20 3.4 7.5 5.7 11 28 33 1.4 1.6 0.9 0.79 0.79 0.87 13 16 15 17 15 15Formaldehyde NS NS NS <0.05 <0.1 <0.1 <0.1 <0.75 <0.75 <0.5 <0.1 <0.1 <0.1 <0.75 <0.75 <0.05 <0.1 <0.1 <0.1 <0.75 <0.75 <0.05 <0.1 <0.1 <0.1 <0.75 <0.75Alkalinity (as CaCO3) NS NS NS 150 120 220 220 287 230 26 77 62 130 137 202 43 41 40 39 32.6 30.5 180 220 200 190 183 180Chloride250 SNS NS 39 6.3 21 25 28 54 12 18 14 26 88 48 10.0 9.7 7.7 7.8 8.2 7.8 33 36 38 38 42 44Cyanide, Total 0.2 0.200 0.030 <0.01 <0.01 <0.01 <0.01 <0.005 <0.005 <0.01 <0.01 <0.01 <0.01 <0.005 <0.005 <0.01 <0.01 <0.01 <0.01 <0.005 <0.005 <0.01 <0.01 <0.01 <0.01 <0.005 <0.005Total K Nitrogen (TKN) 10 NS NS 0.56 <0.50 <0.50 3.3 2.08 1.75 0.88 0.65 1.2 2.70 3.92 7.67 <0.50 <0.50 <0.50 <0.50 <0.300 <0.300 4.8 5.1 5.5 4.8 3.9 3.84Nitrate-N 10 NS NS <0.25 <0.25 <0.25 <0.25 0.1 0.1 2.50 0.42 <0.25 <0.2515.70.19 0.9 0.8 0.75 0.52 1.58 3.84 0.32 <0.25 0.27 0.35 0.398 0.247Nitrite-N 1 NS NS <0.25 <0.25 <0.25 0.33 0.073 <0.05 <0.25 <0.25 <0.25 0.26 0.136 <0.05 <0.25 <0.25 <0.25 0.320 <0.05 <0.05 <0.25 <0.25 <0.25 0.38 0.066 <0.05Nitrogen, Total NS NS NS 0.56 <0.25 <0.25 3.63 2.253 2.1 3.38 1.07 1.2 2.9619.7567.9 0.9 0.8 0.75 0.84 1.58 3.8 5.12 5.10 5.77 5.53 4.364 4Total Phosphorus0.05 S, 0.3/1.0 GNS NS 0.12 0.16 0.32 0.62 0.694 0.694 0.05 0.06 0.12 0.16 0.138 0.166 0.08 0.08 0.07 0.05 0.073 0.034 0.14 0.15 0.13 0.16 0.174 0.141Sulfate250 SNS NS 23 10 10 6.6 <10 33 53 110 38 91 49 100 <5.0 <5.0 <5.0 <5.0 <10 <10 72 73 84 91 78 74Sulfide NS NS NS <0.20 <0.20 <0.20 <0.20 <0.1 <0.1 <0.20 <0.20 <0.20 <0.20 <0.1 <0.1 <0.20 <0.20 <0.20 <0.20 <0.1 <0.1 <0.20 <0.20 <0.20 <0.20 <0.1 <0.1Total Dissolved Solids500 SNS NS 310 120 260 230600430 190 240 150 300520470 98 56 94 76 75 86 380 310 370 380 380 400Temperature (o F)NS NS NS 48.29 60.98 60.3 60.6 46.3 58.6 64.0 63.7 63.14 63.9 65.6 68.2 62.29 62.87 63.32 62.7 62.4 61.5 63.7 58.46 64.04 63.6 63.8 63.3pH (pH units)6.5-8.5 SNS NS 7.08 7.156.176.8 6.97 6.856.35 6.46 5.86 6.29 6.216.645.49 5.64 5.19 5.22 5.10 5.22 6.07 5.42 5.62 6.08 6.00 6.06Specific Conductivity (uS/cm) NS NS NS 342.5 418.5 270.2 738 356 604 214.3 418.5 183 745 1215 680 106.6 106 80.4 158 160 110.5 489.5 71.3 440.8 928 925 555Dissolved Oxygen (mg/L) NS NS NS 0.29 0.25 0.67 0.05 0.84 0.12 1.92 0.3 0.28 0.06 0.15 0.11 -0.07 0.05 1.03 0.12 0.09 0.12 0.69 3.73 1.19 0.75 0.58 0.72MDWS = Massachusetts Drinking Water Standard (MMCL)GW-1 = Massachusetts MCP Method 1 GW-1 standardGW-3 = Massachusetts MCP Method 1 GW-3 standardNA = Not Analyzed for Indicated CompoundG = Massachusetts Drinking Water Guideline (ORSG)S = Secondary Maximum Contaminant Levels (SMCL)NA = Not Analyzed for Indicated CompoundNS = No StandardI = VOCs Standards Specific to Individual CompoundU↓ = All VOC Compounds Analyzed but not found, except Compound Specified BelowU = Analyzed but not found; detection limit listed = Indicates an exceedance of MMCL, ORSG, or Method 1 Standard = Indicates an exceedance of SMCL* DissolvedGENERAL CHEMISTRYMW-3AMW-1RBrewster, MassachusettsFIELD PARAMETERSPOLY-NUCLEAR AROMATIC HYDROCARBONS (PAHs)VOLATILE ORGANIC COMPOUNDS (VOCs)METALS AGGREGATE ORGANIC CONSTITUENTSALDEHYDESGW-3MW-4A1515 Freemans WayMDWSBrewster Sand and RecyclingTable 2: Temporal Groundwater Analysis Summary - May 2018 through November 2020STANDARDS (mg/l)GW-1MW-5
L2051285
Bennett Environmental Associates
K10740A
MERCHANT/BS&R
Client:
Project Name:
Project Number:
11/29/20
Eight Walkup Drive, Westborough, MA 01581-1019
Lab Number:
Report Date:
508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com
1573 Main Street
Brewster, MA 02631
John Tadema-WielandtATTN:
ANALYTICAL REPORT
Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148),
NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).
(508) 896-1706Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its
entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:11292019:05
Page 1 of 76
L2051285-01
L2051285-02
L2051285-03
L2051285-04
L2051285-05
L2051285-06
L2051285-07
L2051285-08
L2051285-09
L2051285-10
L2051285-11
Alpha
Sample ID
MW-1R
MW-1R (FILTERED)
MW-3A
MW-3A (FILTERED)
MW-4A
MW-4A (FILTERED)
MW-5
MW-5 (FILTERED)
MW-3B
MW-5B
TRIP BLANK
Client ID
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
1515 FREEMANS WAY, BREWSTER, MA
Sample
Location
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285
11/29/20
11/17/20 15:30
11/17/20 15:30
11/17/20 14:15
11/17/20 14:15
11/17/20 10:35
11/17/20 10:35
11/17/20 11:55
11/17/20 11:55
11/17/20 11:30
11/17/20 12:30
11/17/20 00:00
Collection
Date/TimeMatrix Receive Date
WATER
WATER
WATER
WATER
WATER
WATER
WATER
WATER
WATER
WATER
WATER
11/18/20
11/18/20
11/18/20
11/18/20
11/18/20
11/18/20
11/18/20
11/18/20
11/18/20
11/18/20
11/18/20
Serial_No:11292019:05
Page 2 of 76
Project Name:
Project Number:
Lab Number:
Report Date:
Were all samples received in a condition consistent with those described on the Chain-of-
Custody, properly preserved (including temperature) in the field or laboratory, and
prepared/analyzed within method holding times?
Were the analytical method(s) and all associated QC requirements specified in the selected
CAM protocol(s) followed?
Were all required corrective actions and analytical response actions specified in the selected
CAM protocol(s) implemented for all identified performance standard non-conformances?
Does the laboratory report comply with all the reporting requirements specified in CAM VII A,
"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical
Data?"
VPH, EPH, and APH Methods only: Was each method conducted without significant
modification(s)? (Refer to the individual method(s) for a list of significant modifications).
APH and TO-15 Methods only: Was the complete analyte list reported for each method?
Were all applicable CAM protocol QC and performance standard non-conformances identified
and evaluated in a laboratory narrative (including all "No" responses to Questions A through E)?
YES
YES
YES
YES
N/A
N/A
YES
A
B
C
D
E a.
E b.
F
MADEP MCP Response Action Analytical Report Certification
L2051285MERCHANT/BS&R
K10740A
Were the reporting limits at or below all CAM reporting limits specified in the selected CAM
protocol(s)?
Were all QC performance standards specified in the CAM protocol(s) achieved?
Were results reported for the complete analyte list specified in the selected CAM protocol(s)?
YES
NO
NO
G
H
I
A response to questions G, H and I is required for "Presumptive Certainty" status
This form provides certifications for all samples performed by MCP methods. Please refer to
the Sample Results and Container Information sections of this report for specification of
MCP methods used for each analysis. The following questions pertain only to MCP
Analytical Methods.
An affirmative response to questions A through F is required for "Presumptive Certainty" status
For any questions answered "No", please refer to the case narrative section on the following page(s).
11/29/20
Please note that sample matrix information is located in the Sample Results section of this report.
Serial_No:11292019:05
Page 3 of 76
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285
11/29/20
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter
(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list
for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified
Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target
Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality
control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"
or "RE", respectively.
When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in
the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed
Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria
for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the
specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC
information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in
conjunction with the sample result, associated regulatory criteria and any associated data usability implications.
Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms
used in this report are provided in the Glossary located at the back of the report.
HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21
calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put
on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air
canisters will be disposed after 3 business days from the date the project is completed.
Please contact Project Management at 800-624-9220 with any questions.
Serial_No:11292019:05
Page 4 of 76
Case Narrative (continued)
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285
11/29/20
MCP Related Narratives
Volatile Organics
In reference to question H:
The initial calibration, associated with L2051285-01, -03, -05, -07, and -11, did not meet the method required
minimum response factor on the lowest calibration standard for 1,4-dioxane (0.0021), as well as the average
response factor for acetone and 1,4-dioxane.
The continuing calibration standard, associated with L2051285-01, -03, -05, -07, and -11, is outside the
acceptance criteria for several compounds; however, it is within overall method allowances. A copy of the
continuing calibration standard is included as an addendum to this report.
PAHs by SIM
L2051285-03, -05, -07, WG1437172-1, and WG1437172-2/-3: The initial calibration utilized a quadratic fit for
nitrobenzene-d5.
In reference to question H:
L2051285-01: The surrogate recovery was outside the acceptance criteria for nitrobenzene-d5 (1%). Re-
extraction was performed; however, the results could not be reported due to laboratory error. Further re-
extraction could not be performed due to lack of additional sample. The results of the original analysis are
reported; however, all associated compounds are considered to have a potential bias.
In reference to question I:
All samples were analyzed for a subset of MCP analytes per client request.
Total Metals
In reference to question I:
All samples were analyzed for a subset of MCP analytes per client request.
Serial_No:11292019:05
Page 5 of 76
Case Narrative (continued)
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285
11/29/20
Non-MCP Related Narratives
Sample Receipt
L2051285-07: One of the sample containers was received below the appropriate pH for the Sulfide analysis.
The laboratory added additional NaOH to a pH >9.
Nitrogen, Total Kjeldahl
The WG1437883-4 MS recovery, performed on L2051285-10, is outside the acceptance criteria for nitrogen,
total kjeldahl (71%); however, the associated LCS recovery is within criteria. No further action was taken.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 11/29/20
Serial_No:11292019:05
Page 6 of 76
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
L2051285Lab Number:
Report Date:
QC OUTLIER SUMMARY REPORT
11/29/20
Method Client ID (Native ID)Lab ID Parameter QC Type
Recovery/RPD
(%)
QC Limits
(%)
Data Quality
Assessment
Associated
Samples
MCP Volatile Organics - Westborough Lab
MCP PAHs by SIM - Westborough Lab
General Chemistry - Westborough Lab
WG1438287-3
WG1438287-3
WG1438287-3
WG1438287-3
WG1438287-4
WG1438287-4
WG1438287-4
L2051285-01
WG1437883-4
Batch QC
Batch QC
Batch QC
Batch QC
Batch QC
Batch QC
Batch QC
MW-1R
Batch QC (L2051285-10)
8260C
8260C
8260C
8260C
8260C
8260C
8260C
8270D-SIM
4500NH3-H
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Tetrahydrofuran
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Nitrobenzene-d5
Nitrogen, Total Kjeldahl
LCS
LCS
LCS
LCS
LCSD
LCSD
LCSD
Surrogate
MS
65
64
53
69
68
68
59
1
71
70-130
70-130
70-130
70-130
70-130
70-130
70-130
30-130
77-111
01,03,05,07,
11
01,03,05,07,
11
01,03,05,07,
11
01,03,05,07,
11
01,03,05,07,
11
01,03,05,07,
11
01,03,05,07,
11
-
07,09-10
potential low bias
potential low bias
potential low bias
potential low bias
potential low bias
potential low bias
potential low bias
potential low bias
potential low bias
Serial_No:11292019:05
Page 7 of 76
ORGANICS
Serial_No:11292019:05
Page 8 of 76
VOLATILES
Serial_No:11292019:05
Page 9 of 76
FF
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,3-Dichloropropene, Total
1,1-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
0.40
0.40
0.40
2.0
2.0
1.0
0.50
1.0
1.0
2.0
2.0
1.0
2.0
1.0
1.0
11/29/20
MW-1RClient ID:
11/17/20 15:30Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-01Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
97,8260C
11/24/20 18:54
LAC
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 10 of 76
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
Xylenes, Total
cis-1,2-Dichloroethene
1,2-Dichloroethene, Total
Dibromomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Bromochloromethane
Tetrahydrofuran
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
1.0
1.0
1.0
1.0
2.0
2.0
1.0
1.0
1.0
1.0
2.0
2.0
1.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
1.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
0.60
2.0
2.0
2.0
2.0
11/29/20
MW-1RClient ID:
11/17/20 15:30Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-01Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 11 of 76
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Diethyl ether
Diisopropyl Ether
Ethyl-Tert-Butyl-Ether
Tertiary-Amyl Methyl Ether
1,4-Dioxane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
250
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
93
98
101
104
70-130
70-130
70-130
70-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
MW-1RClient ID:
11/17/20 15:30Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-01Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 12 of 76
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,3-Dichloropropene, Total
1,1-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
0.40
0.40
0.40
2.0
2.0
1.0
0.50
1.0
1.0
2.0
2.0
1.0
2.0
1.0
1.0
11/29/20
MW-3AClient ID:
11/17/20 14:15Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-03Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
97,8260C
11/24/20 19:25
LAC
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 13 of 76
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
Xylenes, Total
cis-1,2-Dichloroethene
1,2-Dichloroethene, Total
Dibromomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Bromochloromethane
Tetrahydrofuran
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
1.0
1.0
1.0
1.0
2.0
2.0
1.0
1.0
1.0
1.0
2.0
2.0
1.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
1.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
0.60
2.0
2.0
2.0
2.0
11/29/20
MW-3AClient ID:
11/17/20 14:15Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-03Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 14 of 76
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Diethyl ether
Diisopropyl Ether
Ethyl-Tert-Butyl-Ether
Tertiary-Amyl Methyl Ether
1,4-Dioxane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
250
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
93
96
97
103
70-130
70-130
70-130
70-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
MW-3AClient ID:
11/17/20 14:15Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-03Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 15 of 76
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,3-Dichloropropene, Total
1,1-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
0.40
0.40
0.40
2.0
2.0
1.0
0.50
1.0
1.0
2.0
2.0
1.0
2.0
1.0
1.0
11/29/20
MW-4AClient ID:
11/17/20 10:35Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-05Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
97,8260C
11/24/20 19:55
LAC
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 16 of 76
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
Xylenes, Total
cis-1,2-Dichloroethene
1,2-Dichloroethene, Total
Dibromomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Bromochloromethane
Tetrahydrofuran
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
1.0
1.0
1.0
1.0
2.0
2.0
1.0
1.0
1.0
1.0
2.0
2.0
1.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
1.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
0.60
2.0
2.0
2.0
2.0
11/29/20
MW-4AClient ID:
11/17/20 10:35Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-05Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 17 of 76
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Diethyl ether
Diisopropyl Ether
Ethyl-Tert-Butyl-Ether
Tertiary-Amyl Methyl Ether
1,4-Dioxane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
250
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
93
98
101
102
70-130
70-130
70-130
70-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
MW-4AClient ID:
11/17/20 10:35Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-05Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 18 of 76
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,3-Dichloropropene, Total
1,1-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
0.40
0.40
0.40
2.0
2.0
1.0
0.50
1.0
1.0
2.0
2.0
1.0
2.0
1.0
1.0
11/29/20
MW-5Client ID:
11/17/20 11:55Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-07Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
97,8260C
11/24/20 20:25
LAC
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 19 of 76
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
Xylenes, Total
cis-1,2-Dichloroethene
1,2-Dichloroethene, Total
Dibromomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Bromochloromethane
Tetrahydrofuran
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
1.0
1.0
1.0
1.0
2.0
2.0
1.0
1.0
1.0
1.0
2.0
2.0
1.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
1.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
0.60
2.0
2.0
2.0
2.0
11/29/20
MW-5Client ID:
11/17/20 11:55Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-07Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 20 of 76
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Diethyl ether
Diisopropyl Ether
Ethyl-Tert-Butyl-Ether
Tertiary-Amyl Methyl Ether
1,4-Dioxane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
250
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
94
96
102
103
70-130
70-130
70-130
70-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
MW-5Client ID:
11/17/20 11:55Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-07Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 21 of 76
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,3-Dichloropropene, Total
1,1-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
0.40
0.40
0.40
2.0
2.0
1.0
0.50
1.0
1.0
2.0
2.0
1.0
2.0
1.0
1.0
11/29/20
TRIP BLANKClient ID:
11/17/20 00:00Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-11Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
97,8260C
11/24/20 17:23
LAC
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 22 of 76
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
Xylenes, Total
cis-1,2-Dichloroethene
1,2-Dichloroethene, Total
Dibromomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Bromochloromethane
Tetrahydrofuran
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
1.0
1.0
1.0
1.0
2.0
2.0
1.0
1.0
1.0
1.0
2.0
2.0
1.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
1.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
0.60
2.0
2.0
2.0
2.0
11/29/20
TRIP BLANKClient ID:
11/17/20 00:00Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-11Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 23 of 76
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Diethyl ether
Diisopropyl Ether
Ethyl-Tert-Butyl-Ether
Tertiary-Amyl Methyl Ether
1,4-Dioxane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP Volatile Organics - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
250
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
89
99
102
100
70-130
70-130
70-130
70-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
TRIP BLANKClient ID:
11/17/20 00:00Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-11Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 24 of 76
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/24/20 16:23
97,8260CAnalytical Method:
Analytical Date:
11/29/20
Analyst:MKS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,3-Dichloropropene, Total
1,1-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
0.40
0.40
0.40
2.0
2.0
1.0
0.50
1.0
1.0
2.0
2.0
1.0
2.0
1.0
1.0
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
MCP Volatile Organics - Westborough Lab for sample(s): 01,03,05,07,11 Batch: WG1438287-5
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:11292019:05
Page 25 of 76
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/24/20 16:23
97,8260CAnalytical Method:
Analytical Date:
11/29/20
Analyst:MKS
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
Xylenes, Total
cis-1,2-Dichloroethene
1,2-Dichloroethene, Total
Dibromomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Bromochloromethane
Tetrahydrofuran
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.0
1.0
1.0
2.0
2.0
1.0
1.0
1.0
1.0
2.0
2.0
1.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
1.0
2.0
2.0
2.0
2.0
2.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
MCP Volatile Organics - Westborough Lab for sample(s): 01,03,05,07,11 Batch: WG1438287-5
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:11292019:05
Page 26 of 76
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/24/20 16:23
97,8260CAnalytical Method:
Analytical Date:
11/29/20
Analyst:MKS
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Diethyl ether
Diisopropyl Ether
Ethyl-Tert-Butyl-Ether
Tertiary-Amyl Methyl Ether
1,4-Dioxane
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
2.0
2.0
0.60
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
250
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
MCP Volatile Organics - Westborough Lab for sample(s): 01,03,05,07,11 Batch: WG1438287-5
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
91
96
102
100
70-130
70-130
70-130
70-130
Surrogate %Recovery Qualifier
Acceptance
Criteria
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:11292019:05
Page 27 of 76
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,1-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
100
91
96
96
85
97
90
110
110
100
88
95
92
87
90
93
100
92
97
100
98
77
72
100
94
98
98
86
100
94
120
110
110
88
97
92
90
92
96
110
97
100
100
100
81
87
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
0
3
2
2
1
3
4
9
0
10
0
2
0
3
2
3
10
5
3
0
2
5
19
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
MCP Volatile Organics - Westborough Lab Associated sample(s): 01,03,05,07,11 Batch: WG1438287-3 WG1438287-4
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Qual Qual Qual
Serial_No:11292019:05
Page 28 of 76
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Dibromomethane
1,2,3-Trichloropropane
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
Methyl ethyl ketone
Methyl isobutyl ketone
2-Hexanone
Bromochloromethane
Tetrahydrofuran
96
110
110
110
98
110
120
110
92
105
105
98
89
93
95
100
73
110
65
64
53
110
69
100
120
110
110
100
110
120
120
96
105
105
99
92
97
100
110
75
120
68
68
59
110
70
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
4
9
0
0
2
0
0
9
4
0
0
1
3
4
5
10
3
9
5
6
11
0
1
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
MCP Volatile Organics - Westborough Lab Associated sample(s): 01,03,05,07,11 Batch: WG1438287-3 WG1438287-4
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Qual Qual
Q
Q
Q
Q
Q
Q
Q
Qual
Serial_No:11292019:05
Page 29 of 76
2,2-Dichloropropane
1,2-Dibromoethane
1,3-Dichloropropane
1,1,1,2-Tetrachloroethane
Bromobenzene
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
o-Chlorotoluene
p-Chlorotoluene
1,2-Dibromo-3-chloropropane
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Naphthalene
n-Propylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Diethyl ether
Diisopropyl Ether
Ethyl-Tert-Butyl-Ether
97
91
88
100
110
98
97
100
100
96
94
120
100
100
95
96
120
110
100
99
100
72
77
100
96
92
100
120
100
100
110
100
100
99
130
100
110
100
100
120
120
100
100
110
74
79
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
3
5
4
0
9
2
3
10
0
4
5
8
0
10
5
4
0
9
0
1
10
3
3
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
MCP Volatile Organics - Westborough Lab Associated sample(s): 01,03,05,07,11 Batch: WG1438287-3 WG1438287-4
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Qual Qual Qual
Serial_No:11292019:05
Page 30 of 76
Tertiary-Amyl Methyl Ether
1,4-Dioxane
87
108
90
112
70-130
70-130
3
4
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
MCP Volatile Organics - Westborough Lab Associated sample(s): 01,03,05,07,11 Batch: WG1438287-3 WG1438287-4
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
91
96
87
99
70-130
70-130
70-130
70-130
88
97
87
100
Surrogate Qual%Recovery Qual%Recovery
LCS LCSD
11/29/20
Acceptance
Criteria
Qual Qual Qual
Serial_No:11292019:05
Page 31 of 76
SEMIVOLATILES
Serial_No:11292019:05
Page 32 of 76
FF
Acenaphthene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
2-Methylnaphthalene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP PAHs by SIM - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
1
68
64
30-130
30-130
30-130
Acceptance
Criteria
Q
Surrogate % Recovery Qualifier
11/29/20
MW-1RClient ID:
11/17/20 15:30Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-01Lab ID:
Field Prep:Not Specified
Matrix:Water Extraction Method:
Analytical Method:
Analytical Date:
Analyst:
97,8270D-SIM
11/22/20 20:00
ALS
EPA 3510C
Extraction Date:11/22/20 02:59
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 33 of 76
Acenaphthene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
2-Methylnaphthalene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP PAHs by SIM - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
81
67
56
30-130
30-130
30-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
MW-3AClient ID:
11/17/20 14:15Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-03Lab ID:
Field Prep:Not Specified
Matrix:Water Extraction Method:
Analytical Method:
Analytical Date:
Analyst:
97,8270D-SIM
11/22/20 20:17
ALS
EPA 3510C
Extraction Date:11/22/20 02:59
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 34 of 76
Acenaphthene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
2-Methylnaphthalene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP PAHs by SIM - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
84
69
64
30-130
30-130
30-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
MW-4AClient ID:
11/17/20 10:35Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-05Lab ID:
Field Prep:Not Specified
Matrix:Water Extraction Method:
Analytical Method:
Analytical Date:
Analyst:
97,8270D-SIM
11/22/20 20:33
ALS
EPA 3510C
Extraction Date:11/22/20 02:59
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 35 of 76
Acenaphthene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
2-Methylnaphthalene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
MCP PAHs by SIM - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
83
66
62
30-130
30-130
30-130
Acceptance
CriteriaSurrogate % Recovery Qualifier
11/29/20
MW-5Client ID:
11/17/20 11:55Date Collected:
11/18/20Date Received:
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-07Lab ID:
Field Prep:Not Specified
Matrix:Water Extraction Method:
Analytical Method:
Analytical Date:
Analyst:
97,8270D-SIM
11/22/20 20:49
ALS
EPA 3510C
Extraction Date:11/22/20 02:59
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 36 of 76
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/22/20 19:44
97,8270D-SIMAnalytical Method:
Analytical Date:
Extraction Method:EPA 3510C
Extraction Date:11/22/20 02:59
11/29/20
Analyst:ALS
Acenaphthene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
2-Methylnaphthalene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
MCP Semivolatile Organics by SIM - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1437172-1
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
88
69
78
30-130
30-130
30-130
Surrogate %Recovery Qualifier
Acceptance
Criteria
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:11292019:05
Page 37 of 76
Acenaphthene
Fluoranthene
Naphthalene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Acenaphthylene
Anthracene
Benzo(ghi)perylene
Fluorene
Phenanthrene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Pyrene
2-Methylnaphthalene
65
76
64
72
70
67
59
66
70
72
63
69
66
68
78
75
66
67
79
65
75
73
74
65
66
72
75
66
71
69
72
83
79
67
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
40-140
3
4
2
4
4
10
10
0
3
4
5
3
4
6
6
5
2
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
MCP Semivolatile Organics by SIM - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1437172-2 WG1437172-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Qual Qual Qual
Serial_No:11292019:05
Page 38 of 76
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
MCP Semivolatile Organics by SIM - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1437172-2 WG1437172-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Nitrobenzene-d5
2-Fluorobiphenyl
4-Terphenyl-d14
90
65
75
30-130
30-130
30-130
91
65
77
Surrogate Qual%Recovery Qual%Recovery
LCS LCSD
11/29/20
Acceptance
Criteria
Qual Qual Qual
Serial_No:11292019:05
Page 39 of 76
METALS
Serial_No:11292019:05
Page 40 of 76
FF
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
SAMPLE RESULTS
MW-1RClient ID:
11/17/20 15:30Date Collected:
11/18/20Date Received:
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-01Lab ID:
Field Prep:Not Specified
Parameter Result
Dilution
FactorQualifierUnitsRL
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
MCP Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Copper, Total
Iron, Total
Lead, Total
Manganese, Total
Mercury, Total
Selenium, Total
Silver, Total
Sodium, Total
Zinc, Total
0.0564
0.017
ND
49.4
ND
ND
82.5
ND
5.96
ND
ND
ND
39.2
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.0050
0.010
0.004
0.100
0.010
0.010
0.050
0.010
0.010
0.0002
0.010
0.007
2.00
0.050
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 09:57
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
11/25/20 17:53
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,7470A
97,6010D
97,6010D
97,6010D
97,6010D
BV
BV
BV
BV
BV
BV
BV
BV
BV
EW
BV
BV
BV
BV
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 07:03
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 7470A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
Prep
MethodMDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 41 of 76
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
SAMPLE RESULTS
MW-3AClient ID:
11/17/20 14:15Date Collected:
11/18/20Date Received:
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-03Lab ID:
Field Prep:Not Specified
Parameter Result
Dilution
FactorQualifierUnitsRL
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
MCP Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Copper, Total
Iron, Total
Lead, Total
Manganese, Total
Mercury, Total
Selenium, Total
Silver, Total
Sodium, Total
Zinc, Total
0.0166
0.032
ND
39.2
ND
ND
23.6
ND
4.44
ND
ND
ND
24.7
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.0050
0.010
0.004
0.100
0.010
0.010
0.050
0.010
0.010
0.0002
0.010
0.007
2.00
0.050
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 10:00
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
11/25/20 17:58
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,7470A
97,6010D
97,6010D
97,6010D
97,6010D
BV
BV
BV
BV
BV
BV
BV
BV
BV
EW
BV
BV
BV
BV
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 07:03
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 7470A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
Prep
MethodMDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 42 of 76
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
SAMPLE RESULTS
MW-4AClient ID:
11/17/20 10:35Date Collected:
11/18/20Date Received:
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-05Lab ID:
Field Prep:Not Specified
Parameter Result
Dilution
FactorQualifierUnitsRL
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
MCP Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Copper, Total
Iron, Total
Lead, Total
Manganese, Total
Mercury, Total
Selenium, Total
Silver, Total
Sodium, Total
Zinc, Total
ND
ND
ND
5.75
ND
ND
0.084
ND
1.33
ND
ND
ND
6.70
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.0050
0.010
0.004
0.100
0.010
0.010
0.050
0.010
0.010
0.0002
0.010
0.007
2.00
0.050
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 10:03
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
11/25/20 18:02
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,7470A
97,6010D
97,6010D
97,6010D
97,6010D
BV
BV
BV
BV
BV
BV
BV
BV
BV
EW
BV
BV
BV
BV
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 07:03
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 7470A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
Prep
MethodMDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 43 of 76
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
SAMPLE RESULTS
MW-5Client ID:
11/17/20 11:55Date Collected:
11/18/20Date Received:
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-07Lab ID:
Field Prep:Not Specified
Parameter Result
Dilution
FactorQualifierUnitsRL
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
MCP Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Copper, Total
Iron, Total
Lead, Total
Manganese, Total
Mercury, Total
Selenium, Total
Silver, Total
Sodium, Total
Zinc, Total
ND
0.048
ND
30.8
ND
ND
31.6
ND
12.2
ND
ND
ND
25.0
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.0050
0.010
0.004
0.100
0.010
0.010
0.050
0.010
0.010
0.0002
0.010
0.007
2.00
0.050
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 10:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
11/25/20 18:07
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,7470A
97,6010D
97,6010D
97,6010D
97,6010D
BV
BV
BV
BV
BV
BV
BV
BV
BV
EW
BV
BV
BV
BV
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 07:03
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 7470A
EPA 3005A
EPA 3005A
EPA 3005A
EPA 3005A
Prep
MethodMDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 44 of 76
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
SAMPLE RESULTS
MW-3BClient ID:
11/17/20 11:30Date Collected:
11/18/20Date Received:
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-09Lab ID:
Field Prep:None
Parameter Result
Dilution
FactorQualifierUnitsRL
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
MCP Total Metals - Mansfield Lab
Manganese, Total 1.52 mg/l 10.010 11/25/20 18:11 97,6010D BV11/25/20 05:55 EPA 3005A
Prep
MethodMDL
--
Sample Depth:
Serial_No:11292019:05
Page 45 of 76
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
SAMPLE RESULTS
MW-5BClient ID:
11/17/20 12:30Date Collected:
11/18/20Date Received:
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-10Lab ID:
Field Prep:None
Parameter Result
Dilution
FactorQualifierUnitsRL
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
MCP Total Metals - Mansfield Lab
Manganese, Total 0.127 mg/l 10.010 11/25/20 18:16 97,6010D BV11/25/20 05:55 EPA 3005A
Prep
MethodMDL
--
Sample Depth:
Serial_No:11292019:05
Page 46 of 76
FF
Parameter
Parameter
Result
Result
Dilution
Factor
Dilution
Factor
Qualifier
Qualifier
Units
Units
RL
RL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Date
Analyzed
Date
Analyzed
Analytical
Method
Analytical
Method
Analyst
Analyst
Date
Prepared
Date
Prepared
11/29/20
Arsenic, Total
Barium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Copper, Total
Iron, Total
Lead, Total
Manganese, Total
Selenium, Total
Silver, Total
Sodium, Total
Zinc, Total
Mercury, Total
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.0050
0.010
0.004
0.100
0.010
0.010
0.050
0.010
0.010
0.010
0.007
2.00
0.050
0.0002
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 17:49
11/25/20 09:40
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,6010D
97,7470A
BV
BV
BV
BV
BV
BV
BV
BV
BV
BV
BV
BV
BV
EW
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 05:55
11/25/20 07:03
MCP Total Metals - Mansfield Lab for sample(s): 01,03,05,07,09-10 Batch: WG1438132-1
MCP Total Metals - Mansfield Lab for sample(s): 01,03,05,07 Batch: WG1438133-1
EPA 3005A
EPA 7470A
Digestion Method:
Digestion Method:
Prep Information
Prep Information
MDL
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:11292019:05
Page 47 of 76
Arsenic, Total
Barium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Copper, Total
Iron, Total
Lead, Total
Manganese, Total
Selenium, Total
Silver, Total
Sodium, Total
Zinc, Total
Mercury, Total
108
104
118
101
106
114
104
105
105
101
112
104
112
100
110
106
117
101
108
117
104
106
105
99
117
105
113
100
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
2
2
1
0
2
3
0
1
0
2
4
1
1
0
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
MCP Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09-10 Batch: WG1438132-2 WG1438132-3
MCP Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07 Batch: WG1438133-2 WG1438133-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Qual Qual Qual
Serial_No:11292019:05
Page 48 of 76
INORGANICS
&
MISCELLANEOUS
Serial_No:11292019:05
Page 49 of 76
FF
MW-1RClient ID:
11/17/20 15:30Date Collected:
11/18/20Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
MCP General Chemistry - Westborough Lab
General Chemistry - Westborough Lab
Formaldehyde by EPA 8315A - Westborough Lab
Cyanide, Total
Color, Apparent
Alkalinity, Total
Solids, Total Dissolved
Chloride
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Nitrate/Nitrite
Total Nitrogen
Nitrogen, Total Kjeldahl
Phosphorus, Total
Sulfide
Sulfate
Chemical Oxygen Demand
Total Organic Carbon
Tannin & Lignin
Formaldehyde
ND
650
230.
430
54.
ND
ND
ND
1.8
1.75
0.567
ND
33.
68.
20
1.5
ND
mg/l
A.P.C.U.
mg CaCO3/L
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
50
1
1
1
1
1
1
1
1
1
1
2
1
10
1
1
0.005
250
2.00
10
1.0
0.050
0.100
0.10
0.30
0.300
0.010
0.10
20
20
5.0
0.20
0.075
11/23/20 13:48
11/19/20 04:45
11/23/20 15:48
11/21/20 06:05
11/22/20 08:15
11/19/20 03:48
11/19/20 03:48
11/19/20 03:48
11/29/20 12:05
11/28/20 09:55
11/19/20 14:01
11/20/20 21:18
11/24/20 16:31
11/20/20 20:07
11/19/20 10:23
11/24/20 12:58
11/20/20 13:50
97,9014
121,2120B
121,2320B
121,2540C
1,9251
121,4500NO3-F
121,4500NO3-F
121,4500NO3-F
107,-
121,4500NH3-H
121,4500P-E
1,9030B
1,9038
44,410.4
1,9060A
121,5550B
1,8315A
CR
AW
JB
DW
MR
MR
MR
MR
JO
MR
SD
EN
JB
TL
DW
SD
JT
Date
Prepared
11/23/20 10:00
-
-
-
-
-
-
-
-
11/23/20 15:00
11/19/20 09:00
11/20/20 16:20
11/24/20 16:31
11/20/20 17:00
-
-
11/19/20 07:49
11/29/20
MDL
--
--
NA
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 50 of 76
FF
MW-3AClient ID:
11/17/20 14:15Date Collected:
11/18/20Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
MCP General Chemistry - Westborough Lab
General Chemistry - Westborough Lab
Formaldehyde by EPA 8315A - Westborough Lab
Cyanide, Total
Color, Apparent
Alkalinity, Total
Solids, Total Dissolved
Chloride
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Nitrate/Nitrite
Total Nitrogen
Nitrogen, Total Kjeldahl
Phosphorus, Total
Sulfide
Sulfate
Chemical Oxygen Demand
Total Organic Carbon
Tannin & Lignin
Formaldehyde
ND
270
202.
470
48.
ND
0.190
0.19
7.9
7.67
0.166
ND
100
100
33
2.8
ND
mg/l
A.P.C.U.
mg CaCO3/L
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
10
1
1
1
1
1
1
1
1
1
1
5
1
10
2.5
1
0.005
50
2.00
10
1.0
0.050
0.100
0.10
0.30
0.300
0.010
0.10
50
20
5.0
0.50
0.075
11/23/20 13:49
11/19/20 04:45
11/23/20 15:48
11/21/20 06:05
11/22/20 08:16
11/19/20 03:49
11/19/20 03:49
11/19/20 03:49
11/29/20 12:05
11/28/20 09:59
11/19/20 14:02
11/20/20 21:18
11/24/20 16:31
11/20/20 20:07
11/19/20 10:48
11/24/20 13:00
11/20/20 14:10
97,9014
121,2120B
121,2320B
121,2540C
1,9251
121,4500NO3-F
121,4500NO3-F
121,4500NO3-F
107,-
121,4500NH3-H
121,4500P-E
1,9030B
1,9038
44,410.4
1,9060A
121,5550B
1,8315A
CR
AW
JB
DW
MR
MR
MR
MR
JO
MR
SD
EN
JB
TL
DW
SD
JT
Date
Prepared
11/23/20 10:00
-
-
-
-
-
-
-
-
11/23/20 15:00
11/19/20 09:00
11/20/20 16:20
11/24/20 16:31
11/20/20 17:00
-
-
11/19/20 07:49
11/29/20
MDL
--
--
NA
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 51 of 76
FF
MW-4AClient ID:
11/17/20 10:35Date Collected:
11/18/20Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-05Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
MCP General Chemistry - Westborough Lab
General Chemistry - Westborough Lab
Formaldehyde by EPA 8315A - Westborough Lab
Cyanide, Total
Color, Apparent
Alkalinity, Total
Solids, Total Dissolved
Chloride
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Nitrate/Nitrite
Total Nitrogen
Nitrogen, Total Kjeldahl
Phosphorus, Total
Sulfide
Sulfate
Chemical Oxygen Demand
Total Organic Carbon
Tannin & Lignin
Formaldehyde
ND
5.0
30.5
86.
7.8
ND
3.84
3.8
3.8
ND
0.034
ND
ND
ND
0.87
ND
ND
mg/l
A.P.C.U.
mg CaCO3/L
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.005
5.0
2.00
10
1.0
0.050
0.100
0.10
0.30
0.300
0.010
0.10
10
20
0.50
0.20
0.075
11/23/20 13:50
11/19/20 04:45
11/23/20 15:48
11/21/20 06:05
11/22/20 08:17
11/19/20 03:50
11/19/20 03:50
11/19/20 03:50
11/29/20 12:05
11/28/20 10:00
11/19/20 14:03
11/20/20 21:18
11/24/20 16:31
11/20/20 20:07
11/19/20 12:14
11/24/20 13:01
11/20/20 15:12
97,9014
121,2120B
121,2320B
121,2540C
1,9251
121,4500NO3-F
121,4500NO3-F
121,4500NO3-F
107,-
121,4500NH3-H
121,4500P-E
1,9030B
1,9038
44,410.4
1,9060A
121,5550B
1,8315A
CR
AW
JB
DW
MR
MR
MR
MR
JO
MR
SD
EN
JB
TL
DW
SD
JT
Date
Prepared
11/23/20 10:00
-
-
-
-
-
-
-
-
11/23/20 15:00
11/19/20 09:00
11/20/20 16:20
11/24/20 16:31
11/20/20 17:00
-
-
11/19/20 07:49
11/29/20
MDL
--
--
NA
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 52 of 76
FF
MW-5Client ID:
11/17/20 11:55Date Collected:
11/18/20Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-07Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
MCP General Chemistry - Westborough Lab
General Chemistry - Westborough Lab
Formaldehyde by EPA 8315A - Westborough Lab
Cyanide, Total
Color, Apparent
Alkalinity, Total
Solids, Total Dissolved
Chloride
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Nitrate/Nitrite
Total Nitrogen
Nitrogen, Total Kjeldahl
Phosphorus, Total
Sulfide
Sulfate
Chemical Oxygen Demand
Total Organic Carbon
Tannin & Lignin
Formaldehyde
ND
25
180.
400
44.
ND
0.247
0.25
4.0
3.84
0.141
ND
74.
48.
15
2.4
ND
mg/l
A.P.C.U.
mg CaCO3/L
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
2.5
1
10
1
1
0.005
5.0
2.00
10
1.0
0.050
0.100
0.10
0.30
0.300
0.010
0.10
25
20
5.0
0.20
0.075
11/23/20 13:51
11/19/20 04:45
11/23/20 15:48
11/21/20 06:05
11/22/20 08:19
11/19/20 03:52
11/19/20 03:52
11/19/20 03:52
11/29/20 12:05
11/28/20 09:00
11/19/20 14:06
11/20/20 21:19
11/24/20 16:31
11/20/20 20:07
11/19/20 12:38
11/24/20 13:01
11/20/20 15:32
97,9014
121,2120B
121,2320B
121,2540C
1,9251
121,4500NO3-F
121,4500NO3-F
121,4500NO3-F
107,-
121,4500NH3-H
121,4500P-E
1,9030B
1,9038
44,410.4
1,9060A
121,5550B
1,8315A
CR
AW
JB
DW
MR
MR
MR
MR
JO
MR
SD
EN
JB
TL
DW
SD
JT
Date
Prepared
11/23/20 10:00
-
-
-
-
-
-
-
-
11/24/20 10:00
11/19/20 09:00
11/20/20 16:20
11/24/20 16:31
11/20/20 17:00
-
-
11/19/20 07:49
11/29/20
MDL
--
--
NA
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 53 of 76
FF
MW-3BClient ID:
11/17/20 11:30Date Collected:
11/18/20Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-09Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Field Prep:
Date
Analyzed
Analytical
Method Analyst
None
General Chemistry - Westborough Lab
Solids, Total Dissolved
Nitrogen, Nitrate
Nitrogen, Nitrate/Nitrite
Total Nitrogen
Nitrogen, Total Kjeldahl
69.
0.304
0.30
0.60
0.304
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
10
0.100
0.10
0.30
0.300
11/21/20 06:05
11/19/20 03:53
11/19/20 03:53
11/29/20 12:05
11/28/20 08:52
121,2540C
121,4500NO3-F
121,4500NO3-F
107,-
121,4500NH3-H
DW
MR
MR
JO
MR
Date
Prepared
-
-
-
-
11/24/20 10:00
11/29/20
MDL
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 54 of 76
FF
MW-5BClient ID:
11/17/20 12:30Date Collected:
11/18/20Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2051285-10Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Field Prep:
Date
Analyzed
Analytical
Method Analyst
None
General Chemistry - Westborough Lab
Solids, Total Dissolved
Nitrogen, Nitrate
Nitrogen, Nitrate/Nitrite
Total Nitrogen
Nitrogen, Total Kjeldahl
34.
0.880
0.88
0.88
ND
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
10
0.100
0.10
0.30
0.300
11/21/20 06:05
11/19/20 03:58
11/19/20 03:58
11/29/20 12:05
11/28/20 08:53
121,2540C
121,4500NO3-F
121,4500NO3-F
107,-
121,4500NH3-H
DW
MR
MR
JO
MR
Date
Prepared
-
-
-
-
11/24/20 10:00
11/29/20
MDL
--
--
--
--
--
Sample Depth:
Serial_No:11292019:05
Page 55 of 76
FF
Parameter Result
Dilution
FactorQualifierUnitsRL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
11/29/20
Nitrogen, Nitrate
Nitrogen, Nitrite
Total Organic Carbon
Nitrogen, Nitrate/Nitrite
Formaldehyde
Phosphorus, Total
Sulfide
Chemical Oxygen Demand
Solids, Total Dissolved
Chloride
Cyanide, Total
Nitrogen, Total Kjeldahl
Alkalinity, Total
Tannin & Lignin
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg CaCO3/L
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.100
0.050
0.50
0.10
0.075
0.010
0.10
20
10
1.0
0.005
0.300
2.00
0.20
11/19/20 06:08
11/19/20 06:25
11/19/20 06:49
11/19/20 06:08
11/20/20 11:07
11/19/20 13:43
11/20/20 21:16
11/20/20 20:00
11/21/20 06:05
11/22/20 03:38
11/23/20 13:32
11/28/20 09:28
11/23/20 15:48
11/24/20 12:57
121,4500NO3-F
121,4500NO3-F
1,9060A
121,4500NO3-F
1,8315A
121,4500P-E
1,9030B
44,410.4
121,2540C
1,9251
97,9014
121,4500NH3-H
121,2320B
121,5550B
MR
MR
DW
MR
JT
SD
EN
TL
DW
MR
CR
MR
JB
SD
-
-
-
-
11/19/20 07:49
11/19/20 09:00
11/20/20 16:20
11/20/20 17:00
-
-
11/23/20 10:00
11/23/20 15:00
-
-
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09-10 Batch: WG1435968-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1435969-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1436007-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09-10 Batch: WG1436039-1
Formaldehyde by EPA 8315A - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1436071-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1436088-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1436768-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1436799-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09-10 Batch: WG1436959-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1437161-1
MCP General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1437447-1
General Chemistry - Westborough Lab for sample(s): 01,03,05 Batch: WG1437528-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1437545-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1437875-1
MDL
--
--
--
--
--
--
--
--
--
--
--
--
NA
--
Serial_No:11292019:05
Page 56 of 76
Parameter Result
Dilution
FactorQualifierUnitsRL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
11/29/20
Nitrogen, Total Kjeldahl
Sulfate
ND
ND
mg/l
mg/l
1
1
0.300
10
11/28/20 08:47
11/24/20 16:31
121,4500NH3-H
1,9038
MR
JB
11/24/20 10:00
11/24/20 16:31
General Chemistry - Westborough Lab for sample(s): 07,09-10 Batch: WG1437883-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07 Batch: WG1438102-1
MDL
--
--
Serial_No:11292019:05
Page 57 of 76
Nitrogen, Nitrate
Nitrogen, Nitrite
Total Organic Carbon
Nitrogen, Nitrate/Nitrite
Formaldehyde
Phosphorus, Total
Sulfide
93
99
100
92
74
104
104
-
-
-
-
-
-
-
90-110
90-110
90-110
90-110
39-153
80-120
75-125
-
-
-
-
-
-
-
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09-10 Batch: WG1435968-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1435969-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1436007-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09-10 Batch: WG1436039-2
Formaldehyde by EPA 8315A - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1436071-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1436088-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1436768-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Qual Qual Qual
Serial_No:11292019:05
Page 58 of 76
Chemical Oxygen Demand
Solids, Total Dissolved
Chloride
Cyanide, Total
Nitrogen, Total Kjeldahl
Alkalinity, Total
Tannin & Lignin
100
101
100
94
96
106
95
-
-
-
93
-
-
-
90-110
80-120
90-110
80-120
78-122
90-110
80-120
-
-
-
1
-
-
-
20
10
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1436799-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09-10 Batch: WG1436959-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1437161-2
MCP General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1437447-2 WG1437447-3
General Chemistry - Westborough Lab Associated sample(s): 01,03,05 Batch: WG1437528-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1437545-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1437875-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Serial_No:11292019:05
Page 59 of 76
Nitrogen, Total Kjeldahl
Sulfate
96
90
-
-
78-122
90-110
-
-
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 07,09-10 Batch: WG1437883-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 Batch: WG1438102-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Serial_No:11292019:05
Page 60 of 76
Total Organic Carbon
Chemical Oxygen Demand
Tannin & Lignin
Nitrogen, Total Kjeldahl
Sulfate
15
68
1.5
ND
33
53
320
2.8
5.71
87
96
105
80
71
108
-
-
-
-
-
-
-
-
-
-
80-120
90-110
75-125
77-111
55-147
-
-
-
-
-
20
20
20
24
14
Parameter
Native
Sample
MS
Found
MS
%Recovery
MSD
Found
MSD
%Recovery
Recovery
Limits RPD
RPD
Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1436007-4 QC Sample: L2051285-07 Client ID: MW-5
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1436799-3 QC Sample: L2051285-01 Client ID: MW-1R
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1437875-3 QC Sample: L2051285-01 Client ID: MW-1R
General Chemistry - Westborough Lab Associated sample(s): 07,09-10 QC Batch ID: WG1437883-4 QC Sample: L2051285-10 Client ID: MW-5B
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1438102-4 QC Sample: L2051285-01 Client ID: MW-1R
40
238
1.6
8
50
MS
Added
Matrix Spike Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2051285
11/29/20
Qual
Q
Qual Qual
Serial_No:11292019:05
Page 61 of 76
Total Organic Carbon
Chemical Oxygen Demand
Solids, Total Dissolved
Tannin & Lignin
Nitrogen, Total Kjeldahl
Sulfate
15
68
430
1.5
ND
33
15
73
410
1.4
ND
31
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
0
7
5
7
NC
6
20
20
10
20
24
14
Units RPDParameterNative Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1436007-3 QC Sample: L2051285-07 Client ID: MW-5
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1436799-4 QC Sample: L2051285-01 Client ID: MW-1R
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09-10 QC Batch ID: WG1436959-3 QC Sample: L2051285-01 Client ID: MW-
1R
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1437875-4 QC Sample: L2051285-01 Client ID: MW-1R
General Chemistry - Westborough Lab Associated sample(s): 07,09-10 QC Batch ID: WG1437883-3 QC Sample: L2051285-10 Client ID: MW-5B
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07 QC Batch ID: WG1438102-3 QC Sample: L2051285-01 Client ID: MW-1R
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
L2051285Lab Number:
Report Date:
Lab Duplicate Analysis
Batch Quality Control
11/29/20
Qual
Serial_No:11292019:05
Page 62 of 76
*Values in parentheses indicate holding time in days
L2051285-01A
L2051285-01B
L2051285-01C
L2051285-01D
L2051285-01E
L2051285-01F
L2051285-01G
L2051285-01H
L2051285-01I
L2051285-01J
L2051285-01K
L2051285-01L
L2051285-01M
L2051285-01N
L2051285-01O
L2051285-02A
L2051285-03A
L2051285-03B
Vial HCl preserved
Vial HCl preserved
Vial HCl preserved
Vial H2SO4 preserved
Vial H2SO4 preserved
Plastic 250ml unpreserved/No Headspace
Plastic 250ml HNO3 preserved
Plastic 250ml NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Plastic 250ml HNO3 preserved
Vial HCl preserved
Vial HCl preserved
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
B
B
NA
NA
NA
NA
NA
NA
<2
>12
>9
>9
<2
7
7
7
7
<2
NA
NA
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.2
2.2
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
A
B
Absent
Absent
Cooler Custody Seal
Cooler Information
MERCHANT/BS&R
K10740A
MCP-8260-10(14)
MCP-8260-10(14)
MCP-8260-10(14)
TOC-9060(28)
TOC-9060(28)
ALK-T-2320(14)
MCP-CR-6010T-10(180),MCP-FE-6010T-
10(180),MCP-MN-6010T-10(180),MCP-CA-
6010T-10(180),MCP-7470T-10(28),MCP-AS-
6010T-10(180),MCP-CD-6010T-10(180),MCP-
NA-6010T-10(180),MCP-CU-6010T-
10(180),MCP-AG-6010T-10(180),MCP-ZN-
6010T-10(180),MCP-SE-6010T-10(180),MCP-
BA-6010T-10(180),MCP-PB-6010T-10(180)
MCP-TCN9014-10(14)
SULFIDE-9030(7)
SULFIDE-9030(7)
TKN-4500(28),TPHOS-4500(28),COD-
410(28),NO3/NO2-4500(28),TNITROGEN(28)
CL-9251(28),SO4-9038(28),NO3-4500(2),NO2-
4500NO3(2),TDS-2540(7),T&L()
COLOR-A-2120(2),FORM-8315(3)
MCP-PAHSIM-10(7)
MCP-PAHSIM-10(7)
HOLD-METAL-DISSOLVED(180)
MCP-8260-10(14)
MCP-8260-10(14)
Project Name:
Project Number:
L2051285Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
11/29/20
Were project specific reporting limits specified?YES
<2
>12
>9
>9
<2
7
7
7
7
<2
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:11292019:05
Page 63 of 76
*Values in parentheses indicate holding time in days
L2051285-03C
L2051285-03D
L2051285-03E
L2051285-03F
L2051285-03G
L2051285-03H
L2051285-03I
L2051285-03J
L2051285-03K
L2051285-03L
L2051285-03M
L2051285-03N
L2051285-03O
L2051285-04A
L2051285-05A
L2051285-05B
L2051285-05C
L2051285-05D
L2051285-05E
L2051285-05F
L2051285-05G
Vial HCl preserved
Vial H2SO4 preserved
Vial H2SO4 preserved
Plastic 250ml unpreserved/No Headspace
Plastic 250ml HNO3 preserved
Plastic 250ml NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Plastic 250ml HNO3 preserved
Vial HCl preserved
Vial HCl preserved
Vial HCl preserved
Vial H2SO4 preserved
Vial H2SO4 preserved
Plastic 250ml unpreserved/No Headspace
Plastic 250ml HNO3 preserved
B
B
B
B
B
B
B
B
B
B
B
B
B
B
A
A
A
A
A
A
A
NA
NA
NA
NA
<2
>12
>9
>9
<2
7
7
7
7
<2
NA
NA
NA
NA
NA
NA
<2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.9
2.9
2.9
2.9
2.9
2.9
2.9
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
MERCHANT/BS&R
K10740A
MCP-8260-10(14)
TOC-9060(28)
TOC-9060(28)
ALK-T-2320(14)
MCP-CR-6010T-10(180),MCP-FE-6010T-
10(180),MCP-MN-6010T-10(180),MCP-AS-
6010T-10(180),MCP-CA-6010T-10(180),MCP-
7470T-10(28),MCP-CD-6010T-10(180),MCP-
NA-6010T-10(180),MCP-CU-6010T-
10(180),MCP-AG-6010T-10(180),MCP-ZN-
6010T-10(180),MCP-SE-6010T-10(180),MCP-
BA-6010T-10(180),MCP-PB-6010T-10(180)
MCP-TCN9014-10(14)
SULFIDE-9030(7)
SULFIDE-9030(7)
TKN-4500(28),COD-410(28),TPHOS-
4500(28),NO3/NO2-4500(28),TNITROGEN(28)
SO4-9038(28),CL-9251(28),NO3-4500(2),NO2-
4500NO3(2),TDS-2540(7),T&L()
COLOR-A-2120(2),FORM-8315(3)
MCP-PAHSIM-10(7)
MCP-PAHSIM-10(7)
HOLD-METAL-DISSOLVED(180)
MCP-8260-10(14)
MCP-8260-10(14)
MCP-8260-10(14)
TOC-9060(28)
TOC-9060(28)
ALK-T-2320(14)
MCP-CR-6010T-10(180),MCP-FE-6010T-
10(180),MCP-MN-6010T-10(180),MCP-7470T-
10(28),MCP-CA-6010T-10(180),MCP-AS-
6010T-10(180),MCP-CD-6010T-10(180),MCP-
NA-6010T-10(180),MCP-AG-6010T-
10(180),MCP-CU-6010T-10(180),MCP-ZN-
6010T-10(180),MCP-SE-6010T-10(180),MCP-
BA-6010T-10(180),MCP-PB-6010T-10(180)
Project Name:
Project Number:
L2051285Lab Number:
Report Date:
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
11/29/20
<2
>12
>9
>9
<2
7
7
7
7
<2
<2
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:11292019:05
Page 64 of 76
*Values in parentheses indicate holding time in days
L2051285-05H
L2051285-05I
L2051285-05J
L2051285-05K
L2051285-05L
L2051285-05M
L2051285-05N
L2051285-05O
L2051285-06A
L2051285-07A
L2051285-07B
L2051285-07C
L2051285-07D
L2051285-07E
L2051285-07F
L2051285-07G
L2051285-07H
L2051285-07I
L2051285-07J
L2051285-07K
L2051285-07L
L2051285-07M
L2051285-07N
Plastic 250ml NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Plastic 250ml HNO3 preserved
Vial HCl preserved
Vial HCl preserved
Vial HCl preserved
Vial H2SO4 preserved
Vial H2SO4 preserved
Plastic 250ml unpreserved/No Headspace
Plastic 250ml HNO3 preserved
Plastic 250ml NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 250ml Zn Acetate/NaOH preserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
A
A
A
A
A
A
A
A
A
B
B
B
B
B
B
B
B
B
B
B
B
B
B
>12
>9
>9
<2
7
7
7
7
<2
NA
NA
NA
NA
NA
NA
<2
>12
>9
8
<2
7
7
7
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.9
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
N
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
MERCHANT/BS&R
K10740A
MCP-TCN9014-10(14)
SULFIDE-9030(7)
SULFIDE-9030(7)
TKN-4500(28),TPHOS-4500(28),COD-
410(28),NO3/NO2-4500(28),TNITROGEN(28)
SO4-9038(28),CL-9251(28),NO3-4500(2),NO2-
4500NO3(2),T&L(),TDS-2540(7)
COLOR-A-2120(2),FORM-8315(3)
MCP-PAHSIM-10(7)
MCP-PAHSIM-10(7)
HOLD-METAL-DISSOLVED(180)
MCP-8260-10(14)
MCP-8260-10(14)
MCP-8260-10(14)
TOC-9060(28)
TOC-9060(28)
ALK-T-2320(14)
MCP-FE-6010T-10(180),MCP-CR-6010T-
10(180),MCP-MN-6010T-10(180),MCP-CA-
6010T-10(180),MCP-AS-6010T-10(180),MCP-
7470T-10(28),MCP-CD-6010T-10(180),MCP-
NA-6010T-10(180),MCP-ZN-6010T-
10(180),MCP-AG-6010T-10(180),MCP-CU-
6010T-10(180),MCP-SE-6010T-10(180),MCP-
BA-6010T-10(180),MCP-PB-6010T-10(180)
MCP-TCN9014-10(14)
SULFIDE-9030(7)
SULFIDE-9030(7)
TKN-4500(28),COD-410(28),TPHOS-
4500(28),NO3/NO2-4500(28),TNITROGEN(28)
CL-9251(28),SO4-9038(28),NO3-4500(2),NO2-
4500NO3(2),TDS-2540(7),T&L()
COLOR-A-2120(2),FORM-8315(3)
MCP-PAHSIM-10(7)
Project Name:
Project Number:
L2051285Lab Number:
Report Date:
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
11/29/20
>12
>9
>9
<2
7
7
7
7
<2
<2
>12
>9
>9
<2
7
7
7
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:11292019:05
Page 65 of 76
*Values in parentheses indicate holding time in days
L2051285-07O
L2051285-08A
L2051285-09A
L2051285-09B
L2051285-09C
L2051285-10A
L2051285-10B
L2051285-10C
L2051285-11A
L2051285-11B
Amber 1000ml unpreserved
Plastic 250ml HNO3 preserved
Plastic 250ml HNO3 preserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Plastic 250ml HNO3 preserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Vial HCl preserved
Vial HCl preserved
B
B
B
B
B
B
B
B
B
B
7
<2
<2
<2
7
<2
<2
7
NA
NA
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
MERCHANT/BS&R
K10740A
MCP-PAHSIM-10(7)
HOLD-METAL-DISSOLVED(180)
MCP-MN-6010T-10(180)
TKN-4500(28),NO3/NO2-
4500(28),TNITROGEN(28)
NO3-4500(2),TDS-2540(7)
MCP-MN-6010T-10(180)
TKN-4500(28),NO3/NO2-
4500(28),TNITROGEN(28)
NO3-4500(2),TDS-2540(7)
MCP-8260-10(14)
MCP-8260-10(14)
Project Name:
Project Number:
L2051285Lab Number:
Report Date:
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
11/29/20
7
<2
<2
<2
7
<2
<2
7
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:11292019:05
Page 66 of 76
Report Format:Data Usability Report
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285MERCHANT/BS&R
K10740A 11/29/20
Acronyms
DL
EDL
EMPC
EPA
LCS
LCSD
LFB
LOD
LOQ
MDL
MS
MSD
NA
NC
NDPA/DPA
NI
NP
NR
RL
RPD
SRM
STLP
TEF
TEQ
TIC
Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when
those target analyte concentrations are quantified below the limit of quantitation (LOQ). The DL includes any adjustments
from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)
Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction (SPME).
Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an
analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case
estimate of the concentration.
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Limit of Detection: This value represents the level to which a target analyte can reliably be detected for a specific analyte in a
specific matrix by a specific method. The LOD includes any adjustments from dilutions, concentrations or moisture content,
where applicable. (DoD report formats only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable.
Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available. For Method 332.0, the spike recovery is calculated
using the native concentration, including estimated values.
Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit.
N-Nitrosodiphenylamine/Diphenylamine.
Not Ignitable.
Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.
No Results: Term is utilized when 'No Target Compounds Requested' is reported for the analysis of Volatile or Semivolatile
Organic TIC only requests.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL
includes any adjustments from dilutions, concentrations or moisture content, where applicable.
Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less
than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values; although the RPD value will be provided in the report.
Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the
associated field samples.
Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.
Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF
and then summing the resulting values.
Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound
list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Serial_No:11292019:05
Page 67 of 76
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285MERCHANT/BS&R
K10740A 11/29/20
Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is
shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Difference: With respect to Total Oxidizable Precursor (TOP) Assay analysis, the difference is defined as the Post-Treatment value minus the
Pre-Treatment value.
Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after
adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.
Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-
preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.
Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined upon
receipt, if applicable.
PAH Total: With respect to Alkylated PAH analyses, the 'PAHs, Total' result is defined as the summation of results for all or a subset of the
following compounds: Naphthalene, C1-C4 Naphthalenes, 2-Methylnaphthalene, 1-Methylnaphthalene, Biphenyl, Acenaphthylene,
Acenaphthene, Fluorene, C1-C3 Fluorenes, Phenanthrene, C1-C4 Phenanthrenes/Anthracenes, Anthracene, Fluoranthene, Pyrene, C1-C4
Fluoranthenes/Pyrenes, Benz(a)anthracene, Chrysene, C1-C4 Chrysenes, Benzo(b)fluoranthene, Benzo(j)+(k)fluoranthene, Benzo(e)pyrene,
Benzo(a)pyrene, Perylene, Indeno(1,2,3-cd)pyrene, Dibenz(ah)+(ac)anthracene, Benzo(g,h,i)perylene. If a 'Total' result is requested, the
results of its individual components will also be reported.
PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA,
PFNA and PFOS. If a 'Total' result is requested, the results of its individual components will also be reported.
The target compound Chlordane (CAS No. 57-74-9) is reported for GC ECD analyses. Per EPA,this compound "refers to a mixture of
chlordane isomers, other chlorinated hydrocarbons and numerous other components." (Reference: USEPA Toxicological Review of
Chlordane, In Support of Summary Information on the Integrated Risk Information System (IRIS), December 1997.)
Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total'
result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081
and 8082.
Data Qualifiers
A
B
C
D
E
F
G
H
I
J
M
ND
NJ
P
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensates" are byproducts of the extraction/concentration procedures when acetone is introduced in
the process.
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related
projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x)
the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above
one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-
Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable
concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone).
Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted
analyses.
Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations
of the analyte.
Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The ratio of quantifier ion response to qualifier ion response falls outside of the laboratory criteria. Results are considered to be an
estimated maximum concentration.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should
be considered estimated.
The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The lower value for the two columns has been reported due to obvious interference.
Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).
Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Not detected at the reporting limit (RL) for the sample.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where
the identification is based on a mass spectral library search.
The RPD between the results for the two columns exceeds the method-specified criteria.
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
-
Footnotes
Serial_No:11292019:05
Page 68 of 76
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285MERCHANT/BS&R
K10740A 11/29/20
Data Qualifiers
Q
R
RE
S
-
-
-
-
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than 5x the RL. (Metals only.)
Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
Analytical results are from modified screening analysis.
Serial_No:11292019:05
Page 69 of 76
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
1
44
97
107
121
Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846.
Third Edition. Updates I - VI, 2018.
Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
EPA Test Methods (SW-846) with QC Requirements & Performance Standards for the
Analysis of EPA SW-846 Methods under the Massachusetts Contingency Plan, WSC-
CAM-IIA, IIB, IIIA, IIIB, IIIC, IIID, VA, VB, VC, VIA, VIB, VIIIA and VIIIB, July 2010.
Alpha Analytical - In-house calculation method.
Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
Project Name:
Project Number:
Lab Number:
Report Date:
L2051285MERCHANT/BS&R
K10740A
REFERENCES
11/29/20
Serial_No:11292019:05
Page 70 of 76
Alpha Analytical, Inc.ID No.:17873
Facility: Company-wide Revision 17
Department: Quality Assurance Published Date: 4/28/2020 9:42:21 AM
Title: Certificate/Approval Program Summary Page 1 of 1
Document Type: Form Pre-Qualtrax Document ID: 08-113
Certification Information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA 624/624.1: m/p-xylene, o-xylene, Naphthalene
EPA 8260C: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), 1,2,4,5-Tetramethylbenzene; 4-
Ethyltoluene.
EPA 8270D: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.
SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.
Mansfield Facility
SM 2540D: TSS
EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.
EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene,
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene.
EPA TO-12 Non-methane organics
EPA 3C Fixed gases
Biological Tissue Matrix: EPA 3050B
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE,
EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B, SM4500NO2-B
EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.
Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1:
Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E,
SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate.
EPA 624.1: Volatile Halocarbons & Aromatics,
EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II,
Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603.
Mansfield Facility:
Drinking Water
EPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.
EPA 522.
Non-Potable Water
EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn.
EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Serial_No:11292019:05
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Serial_No:11292019:05
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Serial_No:11292019:05
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Method Blank SummaryMethod Blank Summary Form 4Form 4 VolatilesVolatiles
Client : Bennett Environmental Associates Lab Number : L2051285
Project Name : MERCHANT/BS&R Project Number : K10740A
Lab Sample ID : WG1438287-5 Lab File ID :VQ201124N04
Instrument ID : QUIMBY
Matrix : WATER Analysis Date : 11/24/20 16:23
Client Sample No. Lab Sample ID Analysis Date
WG1438287-3LCS WG1438287-3 11/24/20 14:52
WG1438287-4LCSD WG1438287-4 11/24/20 15:22
TRIP BLANK L2051285-11 11/24/20 17:23
MW-1R L2051285-01 11/24/20 18:54
MW-3A L2051285-03 11/24/20 19:25
MW-4A L2051285-05 11/24/20 19:55
MW-5 L2051285-07 11/24/20 20:25
Serial_No:11292019:05
Page 74 of 76
Calibration Verification SummaryCalibration Verification Summary Form 7Form 7 VolatilesVolatiles
Client : Bennett Environmental Associates Lab Numbe r : L2051285
Project Name : MERCHANT/BS&R Project Number : K10740A
Instrument ID : QUIMBY Calibration Date : 11/24/20 14:52
Lab File ID : VQ201124N01 Init. Calib. Date(s) : 08/19/20 08/19/20
Sample No : WG1438287-2 Init. Calib. Times : 07:07 11:41
Channel :
Compound Ave. RRF RRF Min RRF %D Max %D Area% Dev(min)
Fluorobenzene 1 1 - 0 20 96 -.02
Dichlorodifluoromethane 0.437 0.454 - -3.9 20 107 0
Chloromethane 0.6 0.463 - 22.8* 20 80 0
Vinyl chloride 0.546 0.522 - 4.4 20 99 0
Bromomethane 0.273 0.197 - 27.8* 20 73 0
Chloroethane 0.31 0.352 - -13.5 20 109 0
Trichlorofluoromethane 0.66 0.698 - -5.8 20 108 0
Ethyl ether 0.188 0.192 - -2.1 20 101 0
1,1-Dichloroethene 0.397 0.424 - -6.8 20 110 0
Carbon disulfide 0.945 1.045 - -10.6 20 113 0
Methylene chloride 0.422 0.44 - -4.3 20 104 0
Acetone 10 7.266 - 27.3* 20 68 0
trans-1,2-Dichloroethene 0.438 0.48 - -9.6 20 111 0
Methyl tert-butyl ether 0.937 0.867 - 7.5 20 90 -.01
Diisopropyl ether 1.579 1.137 - 28* 20 73 -.01
1,1-Dichloroethane 0.907 0.824 - 9.2 20 92 0
Ethyl tert-butyl ether 1.364 1.054 - 22.7* 20 77 -.01
cis-1,2-Dichloroethene 0.516 0.505 - 2.1 20 97 -.01
2,2-Dichloropropane 0.793 0.77 - 2.9 20 102 -.01
Bromochloromethane 0.197 0.221 - -12.2 20 106 -.01
Chloroform 0.812 0.779 - 4.1 20 95 0
Carbon tetrachloride 0.689 0.66 - 4.2 20 99 -.01
Tetrahydrofuran 0.098 0.068 - 30.6* 20 70 -.02
Dibromofluoromethane 0.236 0.234 - 0.8 20 95 -.01
1,1,1-Trichloroethane 0.784 0.746 - 4.8 20 97 -.01
2-Butanone 0.122 0.08* - 34.4* 20 70 -.02
1,1-Dichloropropene 0.691 0.641 - 7.2 20 97 -.01
Benzene 1.886 1.831 - 2.9 20 97 -.02
tert-Amyl methyl ether 1.057 0.92 - 13 20 86 0
1,2-Dichloroethane-d4 0.271 0.247 - 8.9 20 90 -.01
1,2-Dichloroethane 0.569 0.498 - 12.5 20 86 -.01
Trichloroethene 0.505 0.494 - 2.2 20 100 -.01
Dibromomethane 0.221 0.197 - 10.9 20 86 -.01
1,2-Dichloropropane 0.47 0.399 - 15.1 20 84 -.01
Bromodichloromethane 0.596 0.548 - 8.1 20 91 -.02
1,4-Dioxane 0.00209 0.00226* - -8.1 20 106 -.02
cis-1,3-Dichloropropene 0.743 0.671 - 9.7 20 89 -.02
Chlorobenzene-d5 1 1 - 0 20 98 -.02
Toluene-d8 1.31 1.262 - 3.7 20 96 -.02
Toluene 1.574 1.589 - -1 20 105 -.01
4-Methyl-2-pentanone 0.126 0.081* - 35.7* 20 64 -.02
Tetrachloroethene 0.641 0.733 - -14.4 20 123 -.01
trans-1,3-Dichloropropene 0.811 0.709 - 12.6 20 89 -.02
* Value outside of QC limits.
Serial_No:11292019:05
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Calibration Verification SummaryCalibration Verification Summary Form 7Form 7 VolatilesVolatiles
Client : Bennett Environmental Associates Lab Numbe r : L2051285
Project Name : MERCHANT/BS&R Project Number : K10740A
Instrument ID : QUIMBY Calibration Date : 11/24/20 14:52
Lab File ID : VQ201124N01 Init. Calib. Date(s) : 08/19/20 08/19/20
Sample No : WG1438287-2 Init. Calib. Times : 07:07 11:41
Channel :
Compound Ave. RRF RRF Min RRF %D Max %D Area% Dev(min)
1,1,2-Trichloroethane 0.327 0.293 - 10.4 20 90 -.01
Chlorodibromomethane 0.48 0.464 - 3.3 20 95 -.02
1,3-Dichloropropane 0.719 0.63 - 12.4 20 88 -.02
1,2-Dibromoethane 0.379 0.345 - 9 20 91 -.02
2-Hexanone 0.234 0.125 - 46.6* 20 56 -.02
Chlorobenzene 1.637 1.769 - -8.1 20 109 -.02
Ethylbenzene 3.069 2.992 - 2.5 20 104 -.02
1,1,1,2-Tetrachloroethane 0.561 0.569 - -1.4 20 102 -.02
p/m Xylene 1.112 1.155 - -3.9 20 112 -.01
o Xylene 0.991 1.024 - -3.3 20 110 -.01
Styrene 1.649 1.597 - 3.2 20 100 -.01
1,4-Dichlorobenzene-d4 1 1 - 0 20 99 -.01
Bromoform 0.594 0.62 - -4.4 20 100 -.01
Isopropylbenzene 6.581 6.674 - -1.4 20 107 -.01
4-Bromofluorobenzene 1.146 0.995 - 13.2 20 83 -.01
Bromobenzene 1.387 1.573 - -13.4 20 112 0
n-Propylbenzene 6.985 6.727 - 3.7 20 105 0
1,1,2,2-Tetrachloroethane 0.902 0.834 - 7.5 20 90 -.02
2-Chlorotoluene 4.474 4.486 - -0.3 20 107 -.01
1,3,5-Trimethylbenzene 3.767 3.782 - -0.4 20 109 -.01
1,2,3-Trichloropropane 0.797 0.744 - 6.6 20 91 -.02
4-Chlorotoluene 4.117 3.955 - 3.9 20 101 -.01
tert-Butylbenzene 4.15 4.278 - -3.1 20 113 0
1,2,4-Trimethylbenzene 3.497 3.472 - 0.7 20 105 -.01
sec-Butylbenzene 5.586 5.431 - 2.8 20 108 -.01
p-Isopropyltoluene 4.358 4.488 - -3 20 114 -.01
1,3-Dichlorobenzene 2.419 2.786 - -15.2 20 118 -.01
1,4-Dichlorobenzene 2.339 2.586 - -10.6 20 114 -.01
n-Butylbenzene 3.373 3.319 - 1.6 20 111 -.01
1,2-Dichlorobenzene 2.13 2.39 - -12.2 20 114 -.01
1,2-Dibromo-3-chloropropan 0.136 0.128 - 5.9 20 91 -.02
Hexachlorobutadiene 0.624 0.76 - -21.8* 20 142 -.01
1,2,4-Trichlorobenzene 0.881 1.009 - -14.5 20 112 -.01
Naphthalene 1.496 1.428 - 4.5 20 86 -.01
1,2,3-Trichlorobenzene 0.748 0.863 - -15.4 20 111 -.01
* Value outside of QC limits.
Serial_No:11292019:05
Page 76 of 76
L2055630
Bennett Environmental Associates
K10740A
MERCHANT/BS&R
Client:
Project Name:
Project Number:
12/16/20
Eight Walkup Drive, Westborough, MA 01581-1019
Lab Number:
Report Date:
508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com
1573 Main Street
Brewster, MA 02631
John Tadema-WielandtATTN:
ANALYTICAL REPORT
Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148),
NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).
(508) 896-1706Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its
entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:12162012:55
Page 1 of 17
L2055630-01
Alpha
Sample ID
MW-3B
Client ID
1515 FREEMANS WAY, BREWSTER, MA
Sample
Location
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
Lab Number:
Report Date:
L2055630
12/16/20
12/11/20 14:00
Collection
Date/TimeMatrix Receive Date
WATER 12/11/20
Serial_No:12162012:55
Page 2 of 17
Project Name:
Project Number:
Lab Number:
Report Date:
Were all samples received in a condition consistent with those described on the Chain-of-
Custody, properly preserved (including temperature) in the field or laboratory, and
prepared/analyzed within method holding times?
Were the analytical method(s) and all associated QC requirements specified in the selected
CAM protocol(s) followed?
Were all required corrective actions and analytical response actions specified in the selected
CAM protocol(s) implemented for all identified performance standard non-conformances?
Does the laboratory report comply with all the reporting requirements specified in CAM VII A,
"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical
Data?"
VPH, EPH, and APH Methods only: Was each method conducted without significant
modification(s)? (Refer to the individual method(s) for a list of significant modifications).
APH and TO-15 Methods only: Was the complete analyte list reported for each method?
Were all applicable CAM protocol QC and performance standard non-conformances identified
and evaluated in a laboratory narrative (including all "No" responses to Questions A through E)?
YES
YES
YES
YES
N/A
N/A
YES
A
B
C
D
E a.
E b.
F
MADEP MCP Response Action Analytical Report Certification
L2055630MERCHANT/BS&R
K10740A
Were the reporting limits at or below all CAM reporting limits specified in the selected CAM
protocol(s)?
Were all QC performance standards specified in the CAM protocol(s) achieved?
Were results reported for the complete analyte list specified in the selected CAM protocol(s)?
YES
YES
NO
G
H
I
A response to questions G, H and I is required for "Presumptive Certainty" status
This form provides certifications for all samples performed by MCP methods. Please refer to
the Sample Results and Container Information sections of this report for specification of
MCP methods used for each analysis. The following questions pertain only to MCP
Analytical Methods.
An affirmative response to questions A through F is required for "Presumptive Certainty" status
For any questions answered "No", please refer to the case narrative section on the following page(s).
12/16/20
Please note that sample matrix information is located in the Sample Results section of this report.
Serial_No:12162012:55
Page 3 of 17
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
Lab Number:
Report Date:
L2055630
12/16/20
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter
(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list
for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified
Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target
Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality
control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"
or "RE", respectively.
When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in
the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed
Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria
for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the
specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC
information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in
conjunction with the sample result, associated regulatory criteria and any associated data usability implications.
Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms
used in this report are provided in the Glossary located at the back of the report.
HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21
calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put
on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air
canisters will be disposed after 3 business days from the date the project is completed.
Please contact Project Management at 800-624-9220 with any questions.
Serial_No:12162012:55
Page 4 of 17
Case Narrative (continued)
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
Lab Number:
Report Date:
L2055630
12/16/20
MCP Related Narratives
Total Metals
In reference to question I:
All samples were analyzed for a subset of MCP analytes per client request.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 12/16/20
Serial_No:12162012:55
Page 5 of 17
MERCHANT/BS&R
K10740A
Project Name:
Project Number:
L2055630Lab Number:
Report Date:
QC OUTLIER SUMMARY REPORT
12/16/20
Method Client ID (Native ID)Lab ID Parameter QC Type
Recovery/RPD
(%)
QC Limits
(%)
Data Quality
Assessment
Associated
Samples
There are no QC Outliers associated with this report.
Serial_No:12162012:55
Page 6 of 17
METALS
Serial_No:12162012:55
Page 7 of 17
FF
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2055630
12/16/20
SAMPLE RESULTS
MW-3BClient ID:
12/11/20 14:00Date Collected:
12/11/20Date Received:
Matrix:Water
1515 FREEMANS WAY, BREWSTER, MASample Location:
L2055630-01Lab ID:
Field Prep:Refer to COC
Parameter Result
Dilution
FactorQualifierUnitsRL
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
MCP Total Metals - Mansfield Lab
Arsenic, Total ND mg/l 10.0050 12/16/20 11:36 97,6010D GD12/15/20 20:17 EPA 3005A
Prep
MethodMDL
--
Sample Depth:
Serial_No:12162012:55
Page 8 of 17
FF
Parameter Result
Dilution
FactorQualifierUnitsRL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2055630
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
12/16/20
Arsenic, Total ND mg/l 10.0050 12/16/20 10:23 97,6010D GD12/15/20 20:17
MCP Total Metals - Mansfield Lab for sample(s): 01 Batch: WG1445437-1
EPA 3005ADigestion Method:
Prep Information
MDL
--
Serial_No:12162012:55
Page 9 of 17
Arsenic, Total 110 110 80-120 0 20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
MCP Total Metals - Mansfield Lab Associated sample(s): 01 Batch: WG1445437-2 WG1445437-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MERCHANT/BS&R
K10740A
L2055630
12/16/20
Qual Qual Qual
Serial_No:12162012:55
Page 10 of 17
*Values in parentheses indicate holding time in days
L2055630-01A
L2055630-01B
Plastic 120ml HNO3 preserved
Plastic 120ml HNO3 preserved
A
A
<2
<2
4.6
4.6
Y
Y
Absent
Absent
A Absent
Cooler Custody Seal
Cooler Information
MERCHANT/BS&R
K10740A
HOLD-METAL-DISSOLVED(180)
MCP-AS-6010T-10(180)
Project Name:
Project Number:
L2055630Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
12/16/20
Were project specific reporting limits specified?YES
<2
<2
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:12162012:55
Page 11 of 17
Report Format:Data Usability Report
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L2055630MERCHANT/BS&R
K10740A 12/16/20
Acronyms
DL
EDL
EMPC
EPA
LCS
LCSD
LFB
LOD
LOQ
MDL
MS
MSD
NA
NC
NDPA/DPA
NI
NP
NR
RL
RPD
SRM
STLP
TEF
TEQ
TIC
Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when
those target analyte concentrations are quantified below the limit of quantitation (LOQ). The DL includes any adjustments
from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)
Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction (SPME).
Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an
analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case
estimate of the concentration.
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Limit of Detection: This value represents the level to which a target analyte can reliably be detected for a specific analyte in a
specific matrix by a specific method. The LOD includes any adjustments from dilutions, concentrations or moisture content,
where applicable. (DoD report formats only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable.
Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available. For Method 332.0, the spike recovery is calculated
using the native concentration, including estimated values.
Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit.
N-Nitrosodiphenylamine/Diphenylamine.
Not Ignitable.
Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.
No Results: Term is utilized when 'No Target Compounds Requested' is reported for the analysis of Volatile or Semivolatile
Organic TIC only requests.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL
includes any adjustments from dilutions, concentrations or moisture content, where applicable.
Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less
than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values; although the RPD value will be provided in the report.
Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the
associated field samples.
Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.
Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF
and then summing the resulting values.
Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound
list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Serial_No:12162012:55
Page 12 of 17
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2055630MERCHANT/BS&R
K10740A 12/16/20
Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is
shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Difference: With respect to Total Oxidizable Precursor (TOP) Assay analysis, the difference is defined as the Post-Treatment value minus the
Pre-Treatment value.
Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after
adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.
Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-
preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.
Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined upon
receipt, if applicable.
PAH Total: With respect to Alkylated PAH analyses, the 'PAHs, Total' result is defined as the summation of results for all or a subset of the
following compounds: Naphthalene, C1-C4 Naphthalenes, 2-Methylnaphthalene, 1-Methylnaphthalene, Biphenyl, Acenaphthylene,
Acenaphthene, Fluorene, C1-C3 Fluorenes, Phenanthrene, C1-C4 Phenanthrenes/Anthracenes, Anthracene, Fluoranthene, Pyrene, C1-C4
Fluoranthenes/Pyrenes, Benz(a)anthracene, Chrysene, C1-C4 Chrysenes, Benzo(b)fluoranthene, Benzo(j)+(k)fluoranthene, Benzo(e)pyrene,
Benzo(a)pyrene, Perylene, Indeno(1,2,3-cd)pyrene, Dibenz(ah)+(ac)anthracene, Benzo(g,h,i)perylene. If a 'Total' result is requested, the
results of its individual components will also be reported.
PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA,
PFNA and PFOS. In addition, the 'PFAS, Total (6)' result is defined as the summation of results at or above the RL for: PFHpA, PFHxS,
PFOA, PFNA, PFDA and PFOS. (Note: 'PFAS, Total (6)' is applicable to MassDEP DW compliance analysis only.). If a 'Total' result is
requested, the results of its individual components will also be reported.
The target compound Chlordane (CAS No. 57-74-9) is reported for GC ECD analyses. Per EPA,this compound "refers to a mixture of
chlordane isomers, other chlorinated hydrocarbons and numerous other components." (Reference: USEPA Toxicological Review of
Chlordane, In Support of Summary Information on the Integrated Risk Information System (IRIS), December 1997.)
Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total'
result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081
and 8082.
Data Qualifiers
A
B
C
D
E
F
G
H
I
J
M
ND
NJ
-
-
-
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensates" are byproducts of the extraction/concentration procedures when acetone is introduced in
the process.
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related
projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x)
the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above
one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-
Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable
concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone).
Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted
analyses.
Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations
of the analyte.
Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The ratio of quantifier ion response to qualifier ion response falls outside of the laboratory criteria. Results are considered to be an
estimated maximum concentration.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should
be considered estimated.
The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The lower value for the two columns has been reported due to obvious interference.
Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).
Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Not detected at the reporting limit (RL) for the sample.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
-
Footnotes
Serial_No:12162012:55
Page 13 of 17
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2055630MERCHANT/BS&R
K10740A 12/16/20
Data Qualifiers
P
Q
R
RE
S
-
-
-
-
-
the identification is based on a mass spectral library search.
The RPD between the results for the two columns exceeds the method-specified criteria.
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than 5x the RL. (Metals only.)
Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
Analytical results are from modified screening analysis.
Serial_No:12162012:55
Page 14 of 17
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
97 EPA Test Methods (SW-846) with QC Requirements & Performance Standards for the
Analysis of EPA SW-846 Methods under the Massachusetts Contingency Plan, WSC-
CAM-IIA, IIB, IIIA, IIIB, IIIC, IIID, VA, VB, VC, VIA, VIB, VIIIA and VIIIB, July 2010.
Project Name:
Project Number:
Lab Number:
Report Date:
L2055630MERCHANT/BS&R
K10740A
REFERENCES
12/16/20
Serial_No:12162012:55
Page 15 of 17
Alpha Analytical, Inc.ID No.:17873
Facility: Company-wide Revision 17
Department: Quality Assurance Published Date: 4/28/2020 9:42:21 AM
Title: Certificate/Approval Program Summary Page 1 of 1
Document Type: Form Pre-Qualtrax Document ID: 08-113
Certification Information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA 624/624.1: m/p-xylene, o-xylene, Naphthalene
EPA 8260C: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), 1,2,4,5-Tetramethylbenzene; 4-
Ethyltoluene.
EPA 8270D: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.
SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.
Mansfield Facility
SM 2540D: TSS
EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.
EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene,
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene.
EPA TO-12 Non-methane organics
EPA 3C Fixed gases
Biological Tissue Matrix: EPA 3050B
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE,
EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B, SM4500NO2-B
EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.
Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1:
Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E,
SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate.
EPA 624.1: Volatile Halocarbons & Aromatics,
EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II,
Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603.
Mansfield Facility:
Drinking Water
EPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.
EPA 522.
Non-Potable Water
EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn.
EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Serial_No:12162012:55
Page 16 of 17
Serial_No:12162012:55
Page 17 of 17
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Important: When completing
this form on a computer, use
only the Tab key to move your
cursor – not the Return key.
Third-Party Inspection Report (O&M) – Rev. 12/4/14 Page 1 of 20
Instructions
Use this form to record and report the results of a Third-Party Operation and Maintenance
Inspection conducted pursuant to 310 CMR 19.018. Be sure to obtain the most recent version
of this form. All applicable sections of the submitted form must be completed to be accepted by
MassDEP.
Pursuant to 310 CMR 19.018(8)(a), the third-party inspector and facility owner/operator must sign
this Third-Party Inspection Report form and submit the completed report to the appropriate
MassDEP regional office and one copy of each completed report to the board of health of the
municipality in which the facility is located.
In the event that this inspection report contains a recommendation for corrective action(s), the
owner/operator shall also submit the information required by 310 CMR 19.018(8)(c)2.
Forms and instructions are available online:
http://www.mass.gov/eea/agencies/massdep/recycle/approvals/solid-waste-applications-and-forms.html#8
Note: This form does not identify all of the requirements applicable to each solid waste
management facility; other requirements and/or policies may apply to the operation, maintenance
and monitoring for each facility.
MassDEP Use Only
Rec’d Date:
FMF #:
RO #:
Reviewer:
Comments:
I. Facility Information
Facility Type (check one):
Transfer Station/Handling Facility C&D Waste Processor or C&D Waste Transfer Station Municipal Waste Combustor
Active Landfill Closed Landfill Other: Wood Waste Reclamation Facility
Specify
Facility:
Cape Sand and Recycling WWRF
Facility Name
Brewster
City/Town
MA
State
02631
ZIP Code
508-255-1550
Telephone Number
298388
Regulated Object Account Number
FMF Number
Operator:
Cape Sand and Recycling, LLC
Operator Name (Doing Business As/Company Name)
508-294-1010
Telephone Number
info@capesandandrecycling.com
Email Address
PO Box 1555
Mailing Address
Brewster
City/T Cape Sand and Recycling, LLC own
MA
State
02631
ZIP Code
Permittee:
Cape Sand and Recycling, LLC
Permittee Name (Entity Identified on Facility Permit)
PO Box 1555
Mailing Address
Brewster
City/Town
MA
State
02631
ZIP Code
Responsible Official for the Facility:
Jay Merchant
Responsible Official Name (Individual)
theo@capesandandrecycling.com
Responsible Official Email Address
Cape Sand and Recycling, LLC
Responsible Official Company Name
508-294-1010
Responsible Official Telephone Number
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 2 of 20
II. Third-Party Inspector
Peter Flood
Third-Party Inspector Name
Green Seal Environmental, Inc.
Company Name
SW48-0000045
MassDEP Third-Party Inspector Identification Number
06/01/2021
MassDEP Third-Party Inspector Expiration Date (MM/DD/YYYY)
508-888-6034
Telephone Number
peter@gseenv.com
Email Address
114 State Road Building B
Mailing Address
Sagamore Beach
City/Town
MA
State
02562
ZIP Code
Construction and Demolition Waste (C&D Waste) Processing Facility or C&D Waste Transfer Station Only:
Identify the qualified individual that conducted the observation of incoming waste loads and collection of samples of suspect asbestos-
containing materials during the inspection [pursuant to 310 CMR 19.018(6)(f)]. If the entire inspection was conducted by the third-party
inspector listed above, then check the box and enter only the Asbestos Inspector Certification Number.
III. Inspection Details
A. FREQUENCY
Indicate the scheduled inspection frequency for this facility as required by 310 CMR 19.018(6)(b), or a more frequent schedule set forth
in the Facility Permit/Other Approval:
Bi-Monthly Quarterly Semi-Annual Annual Biennial
Other (include permit/approval type and date of issuance):
B. DATE, TIME & PERSONNEL
Inspection Date (MM/DD/YYYY): 11/17/2020
Inspection Start Time: 12:20 AM PM
Facility Representatives in Attendance During Inspection: Several CSR employees
C. CONDITIONS
Air Temperature: Approximately 48 degrees F. Wind Direction (direction from which the wind is blowing):
Weather: Clear Partly Cloudy Cloudy NW N NE
Dry Rain Snow W Wind E
Wind Speed: Calm Breeze Moderate Strong SW S SE
Same as above. Provide Asbestos Certification Number ► AI-014709
MA Dept. of Labor Standards Asbestos Inspector Certification Number
Asbestos Inspector Name
Company Name
Telephone Number
Email Address
Mailing Address
City/Town
State
ZIP Code
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 3 of 20
IV. Pre-Inspection Preparation
A. FACILITY-SPECIFIC O&M REQUIREMENTS
During each third-party inspection, the third-party inspector shall examine and evaluate the facility’s solid waste activities, equipment,
operations, practices, procedures, and records relevant to the type of third-party inspection being conducted in order to determine the
facility’s compliance with all applicable requirements as set forth in 310 CMR 19.018(6)(a)1.
Therefore, pursuant to 310 CMR 19.018(6)(a)1, prior to conducting a third-party facility operation and maintenance
inspection, the third-party inspector shall, without limitation, complete all of the following:
Review and become familiar with the regulations set forth at 310 CMR 19.000 – Massachusetts Solid Waste Regulations.
Identify, review and become familiar with all solid waste permits, plans, approvals, and orders (or other enforcement documents
issued to the facility by the Department), and the solid waste requirements applicable to the operation and maintenance of the
facility.
Relevant requirements may include, without limitation, specific practices and procedures for the operation, maintenance and
monitoring of the facility, waste acceptance/storage limits, and other requirements related to the facility’s solid waste activities.
Without limitation, these facility-specific requirements may be contained in the Facility Permit, Authorization to Construct,
Authorization to Operate, Operation and Maintenance Plan, Closure/Post-Closure Plans and Approvals, Facility Modification
Approvals, Beneficial Use Determinations, Administrative Consent Orders, and other determinations, authorizations or
enforcement actions issued by the Department.
I, Peter Flood, have identified, reviewed and understand all of the aforementioned requirements that are
applicable to this facility and the following are my observations and recommendations related to the
facility-specific requirements.
► PF
Inspector Initials
B. SOLID WASTE PERMITS, PLANS, APPROVALS & ORDERS
List all relevant solid waste permits, plans, approvals, orders or other enforcement actions issued to the facility by the Department that
contain specific practices, procedures and other requirements still in effect for the operation, maintenance and monitoring or
closure/post-closure of the facility. Where applicable, provide the plan or issue date for each item. For enforcement actions, include
the document number, effective date, and status of implementation by the facility.
Discussion: MassDEP (#234209) Sequence Change GW Monitoring (#X234209) – October 19, 2010; MassDEP ATO (#W229293) -
December 29, 2009; MassDEP ATC (#W227916), February 10, 2009.
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 4 of 20
V. Performance Standards
Examine and evaluate the facility’s solid waste activities, equipment, operations, practices, procedures and records relevant to the type
of solid waste facility.
Using the tables below, identify all areas evaluated by the inspector during the inspection by checking the box in the first column.
Describe all deviations noted during the inspection in the third column. Provide recommendations for corrective action to return to
compliance with the applicable performance standard in the fourth column.
Facility Type Performance Standards
Transfer Station/Handling Facility
(Including C&D Facility)
Complete Section A.
If C&D Handling/ Processing Facility, then also complete Section B.
Municipal Waste Combustor Complete Section A.
Active Landfill Complete Sections C. and F.
If active ash landfill, then also complete Section D.
Closed Landfill Complete Sections E. and F.
A. TRANSFER STATION, HANDLING FACILITY, OR MUNICIPAL WASTE COMBUSTOR (INCLUDING C&D FACILITY)
Evaluated Performance Standard Deviation(s)
Comments/Observations and
Recommended Corrective
Action(s)
19.205(1)
Storm Water Controls.
19.205(2)
Equipment.
19.205(3)
Weighing Facilities.
19.207(1)
General. Discuss in Section VI. Discuss in Section VI.
19.207(2)
Supervision of Operation.
19.207(3)
Access to Facilities.
19.207(4)
Security.
19.207(5)
Posting of Handling Facility.
19.207(6)
Unloading of Refuse.
19.207(7)
Special Wastes.
19.207(8)
Banned/Restricted Wastes.
19.207(9)
Hazardous Waste.
19.207(10)
Household Hazardous Waste
and Waste Oil Collections.
19.207(11)
Bulky Waste.
19.207(12)
Liquid Wastes.
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 5 of 20
Evaluated Performance Standard Deviation(s)
Comments/Observations and
Recommended Corrective
Action(s)
19.207(13)
Bird Hazards.
19.207(14)
Dust Control.
19.207(15)
Vector Control.
19.207(16)
Control of Wind-blown Litter.
19.207(17)
Staffing.
19.207(18)
Employee Facilities.
19.207(19)
Accident Prevention/Safety.
19.207(20)
Fire Protection.
19.207(21)
Recycling Operations.
19.207(22)
Records for Operational and
Plan Execution.
19.207(23)
Screening and/or Fencing.
19.207(24)
Open Burning.
19.207(25)
Inspections.
19.207(26)
End-of-Life Mercury-added
Products.
B. CONSTRUCTION AND DEMOLITION (C&D) WASTE PROCESSING FACILITY OR C&D WASTE TRANSFER STATION
Evaluated Performance Standard Deviation(s)
Comments/Observations and
Recommended Corrective
Action(s)
19.206(1)
Enclosed Operations.
19.206(2)
Storage.
19.206(3)
Contact Water.
Suspect Asbestos-Containing
Material (ACM) Inspection and
Management Protocol.
Sample collection of suspect
ACM from incoming loads. Discuss sample results:
► Attach analytical reports.
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 6 of 20
C. ACTIVE LANDFILL
Evaluated Performance Standard Deviation(s) Comments/Observations and
Recommended Corrective Action(s)
19.130(1)
General. Discuss in Section VI. Discuss in Section VI.
19.130(2)
Operator Supervision. None observed Facility care and maintenance under the
supervision of a qualified operator.
19.130(3)
Special Wastes. Not applicable Facility does not accept or manage
Special Wastes
19.130(4)
Banned/Restricted Wastes. None observed Facility accepts stumps and brush for
recycling.
19.130(5)
Hazardous Waste.
Not applicable Facility does not accept Hazardous
Waste
19.130(6)
Bulky Wastes.
Not applicable Facility does not accept Bulky Wastes
19.130(7)
Liquid Wastes.
Not applicable Facility does not accept Liquid
Wastes
19.130(8)
Solid Waste Handling. None observed Yard manager/load inspector directly
supervising waste handling
19.130(9)
Bird Hazards. None observed There was no indication of bird
hazards and/or bird congregation at
the time of the inspection
19.130(10)
Equipment and Shelter. None observed Facility has enough on-site mobile
equipment to properly run the
WWRF. Significant quantities of spare
equipment exist on-site as part of the
construction entity of the facility
19.130(11)
Staffing.
None observed Adequate staff on site to properly run
the facility
19.130(12)
Employee Facilities.
None observed Full facilities are provided to staff in
the office building, scale house and
maintenance building
19.130(13)
Accident Prevention/Safety.
None observed Employees reportedly participate in
regular safety training
19.130(14)
Spreading and Compacting of
Solid Waste.
Not applicable Although permitted to do so, the
facility is not currently landfilling
materials. Stumps and brush are
stockpiled and chipped on the surface
19.130(15)
Cover Material.
None observed Sufficient quantities of cover material
are available on site if needed
19.130(16)
Vector, Dust and Odor Control.
None observed No vector, dust or odor issues noted on
the day of inspection. Dust is controlled
by reducing vehicle speeds through the
WWRF and wetting of access roads.
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 7 of 20
Evaluated Performance Standard Deviation(s) Comments/Observations and
Recommended Corrective Action(s)
19.130(17)
Litter Control.
None observed NO windblown materials were
observed on and/or off-site from the
WWRF operations during inspection.
Facility in excellent condition
19.130(18)
Top Slope and Side Slopes.
None observed Facility not currently landfilling stumps
and brush. Stockpiles of stumps,
brush and tailings noted were neat
and orderly
19.130(19)
Storm Water Drainage.
None observed Controls consist of loose permeable
sands, and directing stormwater to
lower portions of the WWRF
19.130(20)
Erosion Control.
None observed Controls consist of grading to lower
portions of the site.
19.130(21)
Boundary/Elevation Markers.
None observed No landfilling/sloping taking place,
only temporarily stockpiling of
materials
19.130(22)
Access Roads.
None observed Paved surfaces appeared to be in
excellent condition on the day of
inspection. Dirt roads within the
WWRF area were properly graded to
promote safe and easy access
19.130(23)
Security.
None observed Gates, berms and fencing were in
good condition and observed to be
functioning properly to limit
unauthorized access to the facility
19.130(24)
Posting of the Landfill.
None observed Appropriate signage posted at
entrance to WWRF. Signs direct
users to tipping area.
19.130(25)
Open Burning. Not applicable No open burning exists on-site
19.130(26)
Fire Protection and Control. None observed Facility in compliance with
requirements. Extinguishers
mounted strategically around the
facility as well as in mobile
equipment as needed.
19.130(27)
Convenience and Recycling
Drop-off Areas at Landfills.
Not applicable
19.130(28)
Waste Oil Collections at
Landfills.
Not applicable Waste oil is not accepted at this
facility
19.130(29)
Household Hazardous Waste
Collections at Landfills.
Not applicable Household hazardous waste
collection does not occur at this
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 8 of 20
Evaluated Performance Standard Deviation(s) Comments/Observations and
Recommended Corrective Action(s)
facility
19.130(30)
Leachate Collection,
Treatment and Disposal.
Not applicable
19.130(31)
Phase Completion of the
Landfill.
Not applicable
19.130(32)
Disruption of Landfilled Areas. None observed Facility is permitted for active stump
recovery and recycling
19.130(33)
Construction of Buildings. Not applicable
19.130(34)
Records for Operational and
Plan Execution.
None observed Maintained and accessible in the
scalehouse.
19.130(35)
Inspections. None observed Inspections performed by a MassDEP
approved 3rd party inspector per 310
CMR 19.018
19.130(36)
Re-circulation of Leachate. Not applicable
19.130(37) End-of-Life
Mercury-added Products. None observed Facility only accepts stumps and brush
D. ASH LANDFILL
Evaluated Performance Standard Deviation(s) Comments/Observations and
Recommended Corrective Action(s)
19.131(1)
General. Discuss in Section VI. Discuss in Section VI.
19.131(2)
Fugitive Emissions.
19.131(3)
Ash Moisture Content.
19.131(4)
Spreading/Compacting of Ash.
19.131(5)
Vehicle Washdown /
Wheelwash / Other Measures.
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 9 of 20
E. CLOSED LANDFILL
Evaluated Performance Standard Deviation(s) Comments/Observations and
Recommended Corrective Action(s)
19.016
Post-closure Use.
19.142(1)
General. Discuss in Section VI. Discuss in Section VI.
19.142(2)
Post-closure Period.
19.142(3)
Post-closure Period Waiver.
19.142(4)
Post-closure Period Extension.
19.142(5)
Post-closure Requirements.
19.142(6)
Inspection Requirements.
19.142(7)
Additional Measures.
19.142(8)
Termination of the Post-
Closure Period.
19.143(1)
Applicability.
19.143(2)
Submission of Post-closure
Use Plans.
19.143(3)
Criteria for Approval of Post-
closure Use.
19.143(4)
Post-closure Construction.
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 10 of 20
F. ADDITIONAL LANDFILL REQUIREMENTS
Evaluated Performance Standard Comments/Observations and
Recommended Corrective Action(s)
19.132
Environmental Monitoring Requirements.
Is the monitoring of surface water, ground water, landfill
gas and any other media as determined by the
Department, including without limitation, soil and
sediment, being conducted on the schedule established in
the permit or as otherwise required by the Department?
YES NO
Are the analytical results of the environmental monitoring
submitted to the Department within 60 days after the date
of sample collection or as otherwise specified by the
Department?
YES NO
19.133
Maintenance of Environmental Control and Monitoring
Systems.
Are the facility operations conducted in a manner which
protects all environmental control systems as approved in
the Operation and Maintenance plan and monitoring
systems as approved in the Operation and Maintenance
plan or permit?
YES NO
Is regular maintenance of all landfill environmental control
systems performed as approved in the Operation and
Maintenance plan or permit?
YES NO
Has the Department been notified of the existence and
extent of damaged or destroyed environmental control
systems, monitoring devices, or surface water sampling
location markers in accordance with 310 CMR
19.133(1)(c) and/or 19.133(1)(e)?
N/A (if no damage to report) YES NO
Continue to Next Page ►
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 11 of 20
F. ADDITIONAL LANDFILL REQUIREMENTS – Continued
Evaluated Performance Standard Comments/Observations and
Recommended Corrective Action(s)
19.121(4)
Landfill Gas Recovery Operation and Maintenance
Requirements.
N/A
Is condensate generation kept to a minimum and
condensate recirculation, if proposed, performed in
accordance with the permit?
YES NO
Are the sampling and analysis of condensate conducted
on the schedule established in the permit or as otherwise
required by the Department?
YES NO
Are the analytical results of condensate monitoring
reported to the Department as established in the permit or
as otherwise required by the Department?
YES NO
Is an annual report on the operation of the landfill gas
recovery facility submitted to the Department as specified
in the permit?
YES NO
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 12 of 20
VI. Inspection Observations
A. FACILITY CONDITION AND OPERATIONS
Examine and evaluate the facility condition and operations as observed during the inspection, including the following:
Describe any evidence of the following conditions observed at the time of the inspection:
• Unpermitted discharges to air, water, land or other natural resources of the Commonwealth; and
• Dust, odors, litter, and/or other nuisance conditions.
Document and discuss all deviations from any specific requirements for the facility that are not addressed in the previous section
(Section V. – Performance Standards), including without limitation, the requirements set forth in the facility’s operation and
maintenance plan, orders or other enforcement documents, and other solid waste permits, approvals, and authorizations issued to
the facility by MassDEP.
List the types and estimated quantities of all waste and materials stored at the facility at the time of the inspection.
Provide a narrative that describes the overall status of the general condition, operation and performance of the facility as
observed at the time of the inspection.
Attach photographs taken during the inspection that depict the general condition and operation of the facility. At a minimum, include
photographs, as applicable, of the waste unloading (tipping) area, waste storage areas, recyclable material storage and, for transfer
stations, the waste reloading activity.
Discussion: No unpermitted discharges to air, water or land were noted on site on the day of inspection. No deviations were noted
from the facility operation and maintenance plan. The facility appeared to be in good condition on the day of inspection. Stockpiles
of loam, mulch, wood chips, stumps brush and tailings were noted neat and orderly on the day of inspection.
Screening of loam materials and reclamation activities was noted on the day of inspection. Conditionally exempt ABC stockpile
was well below the permitted volume of 3,000 cubic yards.
B. RECORD REVIEW
Examine and evaluate the facility’s record-keeping. Without limitation, document the status of the facility’s compliance with, and any
deviations from, the record-keeping required by 310 MCR 19.000; the facility’s operation and maintenance plan; orders or other
enforcement documents issued to the facility; and other solid waste permits, approvals, determinations and authorizations issued to the
facility by the Department, including the following:
Discuss the evaluation of the Facility’s “daily log” such as, daily tonnage records.
List and discuss any special incidents that have occurred since the previous inspection such as exceedances of the facility’s
permitted waste acceptance limits, nature and outcome of complaints reported to the facility operator (including the identity of the
complainant, if known), fires, emergencies, or other disruptions to the routine operation of the facility.
Discussion: Inbound and outbound tonnage and volumes are maintained in the scalehouse. The daily log is orderly and up to date.
No special incidents were reported to GSE since the previous inspection of the facility.
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 13 of 20
VII. Summary and Recommendations
Pursuant to 310 CMR 19.018(6)(a)4., where a third-party inspector observes that the operation or maintenance of the facility deviates
from the aforementioned applicable requirements, he or she shall document all such deviations and recommend corrective actions for
the facility to take to return to compliance.
A. INSPECTION RESULTS
Based on the examinations and evaluations conducted in Sections V. and VI., please summarize the inspection results by checking one
of the following determinations:
No deviations from the applicable performance standards or additional requirements listed at 310 CMR 19.018(6)
were identified during this inspection.
If no deviations were identified during the inspection, check this box and proceed to Section VII.B.
Deviations from the applicable performance standards or additional requirements listed at 310 CMR 19.018(6) were
identified during this inspection and are discussed further in this report.
If deviations were identified during the inspection, check this box and ensure that each deviation and the recommended
corrective actions are discussed in the applicable section(s) below.
B. STATUS OF PREVIOUS RECOMMENDATIONS FOR CORRECTIVE ACTION
If a previous inspection report identified deviations with recommendations for corrective action, please describe the action(s) taken
since the last inspection to return the facility to compliance with the applicable requirements.
Discussion: N/A
C. RECOMMENDATIONS FOR CORRECTIVE ACTION
Based on the results of this inspection, please list all deviations noted during the inspection and provide recommendations for corrective
action to return to compliance with the applicable requirement.
Recommendations: None at this time
D. ADDITIONAL COMMENTS
Comments: None at this time.
VIII. Additional Information Checklist
Attach the following additional information, as applicable, to complete the inspection report.*
Attach photographs taken during the inspection that depict the general condition and operation of the facility, as required in
Section VI.A.
For C&D Waste facilities only, attach the analytical results, as required in Section V.B.
*Note: Pursuant to 310 CMR 19.018(8), MassDEP may request additional information.
Continue to Certification Statement on Next Page ►
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 15 of 20
General area and access roads
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 16 of 20
Stumps to be processed
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 17 of 20
WWRF material mining
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 18 of 20
Wood chips
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 19 of 20
Material stockpiles and access roads
Massachusetts Department of Environmental Protection
Bureau of Waste Prevention / Solid Waste Management
Third-Party Inspection Report – 310 CMR 19.018(8)
Operation & Maintenance
Third-Party Inspection Report (O&M) Page 20 of 20
Clean ABC stockpiles
WQRC Meeting Minutes
12-18-2020 1
Date Approved:
Vote:
TOWN OF BREWSTER
MINUTES of WATER QUALITY REVIEW COMMITTEE
Friday, December 18, 2020 at 9:00 AM
VIRTUAL MEETING
Attending Committee Members:
Vice Chair Amy von Hone convened the Water Quality Review Committee meeting at 9:00 AM with
members Victor Staley, Chris Miller, Ned Chatelain, Penny Holeman (9:20), and Roberta Barrett
Members Absent: Chair Cyndi Baron
Guests: Steve Colarusso, Pleasant Bay Health; John Williams, Pleasant Bay Health; Mike
Gradone, Brewster Recreation
Item 1: Pleasant Bay Health
John Williams, Director of Plant Operations, said that in the last three years there have been no
changes to the waste water treatment plant or water system for the building. Steve Colarusso,
Administrator, said the only change was the change in ownership in September of 2019 – Avinnia
Point Group Care out of Norwood, MA.
Roberta noticed there was a building permit application in July and wondered if there was anything
that we needed to look at. John Williams replied that the permit was to build a PPE cage to keep our
Personal Protective Equipment under lock and key.
Victor said there was another building permit in 2018 for storage in the basement, no increase on
occupancy or septic. He went on to say the Building Department is there on an annual basis for
inspections, and they are current with their Certificate of Inspection.
Amy questioned if occupancy has been pretty consistent? Steve Colarusso said they have 100
residents now and a full house would be 135. They are slightly down from where they were before
the pandemic where they were running in the 115-120 census. Amy followed up asking with the
pandemic if there were any additional water usage or cleaners going into the system. John Williams
answered that the treatment facility was only used for cleaner disposal, and if they were up in water
usage, it would be from more hand washing in the building.
MOTION to approve the renewal application for Pleasant Bay Health.
MOVED by Victor Staley. Seconded by Roberta Barrett.
TOWN OF BREWSTER
Water Quality Review Committee
2198 Main Street
Brewster, Massachusetts 02631-1898
(508) 896-3701 x1121
FAX (508) 896-8089
WQRC Meeting Minutes
12-18-2020 2
Roll Call Vote: Ned Chatelain – yes, Roberta Barrett – yes, Victor Staley – yes, Chris Miller –
yes, Vice Chair Amy von Hone - yes
VOTE: 5-yes 0-no
Item 2: Camp Mitton/Crossroads for Kids
Amy said this is a straight renewal and unfortunately, this past summer the camp was unable to
open during the pandemic. There were no changes from their prior certificate.
Victor said this is also a site that the Building Department visits every year and hasn’t observed any
changes.
Amy said they did not take their annual well water sample as required due to the pandemic, but that
is part of the separate licensing for Camp renewal. Otherwise, she has no issues or questions. The
Health Department licenses them on an annual basis.We will look for a Water Quality Analysis for
next year if they are open.
MOTION to approve the renewal application for Camp Mitton.
MOVED by Victor Staley. Seconded by Ned Chatelain.
Roll Call Vote: Ned Chatelain – yes, Roberta Barrett – yes, Victor Staley – yes, Chris Miller –
yes, Vice Chair Amy von Hone - yes
VOTE: 5-yes 0-no
Chris Miller said we don’t require water quality testing as part of the WQRC for drinking
water. We strictly look at if we have reason to monitor for Nitrogen and things like that, but
we don’t address drinking water quality, unless the Board of Health had septic issues.
Item 3: Eldredge Farm
Amy said there were no changes and no septic system servicing this area of the property, and they
did include a well report that services that area.
MOTION to renew the certificate for Eldredge Farm.
MOVED by Victor Staley. Seconded by Ned Chatelain.
Roll Call Vote: Ned Chatelain – yes, Roberta Barrett – yes, Victor Staley – yes, Chris Miller –
yes, Vice Chair Amy von Hone - yes
VOTE: 5-yes 0-no
Item 4: Brewster Recreation
Amy said this renewal is for the fields off of Freeman’s Way. Recreation Director, Mike Gradone is
here. Please introduce yourself and give us a brief history on what the fields are used for at this time.
Mike Gradone addressed the Committee saying that the fields are at Freeman’s Way – one
soccer/lacrosse field in the back, Babe Ruth Field and 2 little league fields – all used for baseball.
We used to have a snack shack, but it is not being used as a snack shack now, but only as storage.
The last inspection was done in 2011, repair work in 2012, but again, it hasn’t been used in at least 6
years.
WQRC Meeting Minutes
12-18-2020 3
Amy asked who maintains the field and what that involves re: fertilizer and the like. Mike Gradone
answered that Public Works maintains the field, there is irrigation with town water. As far as
fertilizers, he is not 100% sure, but would say they follow Town procedures. He could find out if
necessary.
Chris asked if one of those fields had been redone recently. There has been some irrigation issues.
Mike Gradone said it is in his Capital Plan for next year to replace just the Babe Ruth field to replace
some of the parts of the irrigation system. Chris asked about a proposal to make the field more
accessible? Mike Gradone replied that they do have plans to make all the fields ADA accessible. We
are waiting on the State for funding to fully implement. Chris said we may need to review the plans
once things are finalized. Mike Gradone said once we get a final plan, we will make sure you get the
information for review.
Ned wondered about the long term plan for what’s there now. Mike Gradone said the plan would be
to get rid of the snack shack entirely and put in an all-inclusive playground in that area. Ned asked if
they would anticipate having a bathhouse there as well. Mike Gradone replied yes, they would.
Amy wanted to make note that anything added, including bath houses or food service facilities would
have to be vetted through the health department as an additional oversight.
Chris wanted to know if this location would have a water filling station there. Mike Gradone said yes,
there was interest to put some there.
MOTION to approve the renewal application for Brewster Recreation.
MOVED by Victor Staley. Seconded by Ned Chatelain.
Roll Call Vote: Ned Chatelain – yes, Roberta Barrett – yes, Penny Holeman – yes, Victor
Staley – yes, Chris Miller – yes, Vice Chair Amy von Hone - yes
VOTE: 6-yes 0-no
Item 4: Minutes from September 18, 2020
MOTION to approve the September 18, 2020 meeting Minutes.
MOVED by Roberta Barrett. Seconded by Penny Holeman.
Roll Call Vote: Roberta Barrett – yes, Ned Chatelain – yes, Penny Holeman – yes, Victor
Staley – yes, Chris Miller – yes, Vice Chair Amy von Hone - yes
VOTE: 6-yes 0-no
Item 5: Informational Items
Amy mentioned that Cyndi was not able to attend this meeting and hopes to be at the next
meeting.
Item 6: Topics the Chair did not Reasonably Anticipate – none
Next Meeting: TBD – right now, it is on the schedule for Friday, January 29th at 9AM.
MOTION to adjourn the meeting at 9:35 A.M.
MOVED by Ned Chatelain. Seconded by Victor Staley
WQRC Meeting Minutes
12-18-2020 4
Roll Call Vote: Roberta Barrett – yes, Ned Chatelain – yes, Penny Holeman – yes, Victor
Staley – yes, Chris Miller – yes, Vice Chair Amy von Hone - yes
VOTE: 6-yes 0-no
Respectfully Submitted by: Beth Devine
Action items:
Issue renewed Certificates for Committee signatures for: Pleasant Bay Health, Camp Mitton, Eldredge
Farm, and Brewster Recreation;
Re-issue renewal letters to those past due that have not yet responded;
Send letters to this year’s renewals due – Beth
Packet of additional documents available on the website for review