HomeMy Public PortalAboutBOH05.05.21packetMassachusetts Department of Environmental Protection
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1273540
4/16/2021:5:50:04 PM
2783.88K
SFARRENKOPF
Groundwater Discharge Monitoring Report Forms
In Process
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/1/2021 NOT APPLICABLE
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
BEA NSU PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Daily Log Sheet 2021 Mar Daily
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DAILY LOG SHEET
951
1. Permit Number
465405799
2. Tax identification Number
2021 MAR DAILY
3. Sampling Month & Frequency
C. Daily Readings/Analysis Information
Date Effluent
Flow GPD
Reuse
Flow GPD
Irrigation
Flow GPD
Turbidity Influent pH Effluent
pH
Chlorine
Residual
(mg/l)
UV
Intensity
(%)
1 224 6.9 7.1
2 175 6.9 7.0
3 613 6.8 7.1
4 4990 6.9 7.0
5 6032 6.9 7.0
6 6032
7 6032
8 5632 6.8 7.0
9 4623 6.9 7.0
10 5824 6.9 7.0
11 5487 6.9 7.1
12 5723 6.8 7.0
13 5723
14 5723
15 5334 6.8 6.9
16 7174 6.8 7.0
17 3994 6.9 7.0
18 6366 6.8 6.9
19 6625 6.8 7.0
20 6625
21 6625
22 5448 6.8 7.0
23 6525 6.8 6.9
24 5409 6.7 7.0
25 9911 6.7 6.9
26 5826 6.9 6.9
27 5826
28 5826
29 6560 6.9 6.9
30 4358 6.9 6.8
31 5697 6.8 6.9
gdpdls.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DAILY LOG SHEET
951
1. Permit Number
465405799
2. Tax identification Number
2021 MAR DAILY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/17/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Discharge Monitoring Report 2021 Mar Monthly
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
D. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
BOD 160 29 5.0
MG/L
TSS 79 25 14
MG/L
TOTAL SOLIDS 520
MG/L
AMMONIAN 12.8
MG/L
NITRATEN ND 0.10
MG/L
TOTAL NITROGEN(NO3+NO2+TKN)6.12 0.750
MG/L
OIL & GREASE ND 4.0
MG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/17/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Discharge Monitoring Report 2021 Quarterly 1
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
D. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
TOTAL PHOSPHORUS AS P 6.83 0.125
MG/L
ORTHO PHOSPHATE 5.23 0.125
MG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/17/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Discharge Monitoring Report 2021 Annual
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
E. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
ACETONE ND 25
UG/L
BENZENE ND 2.5
UG/L
1,1 DICHLOROETHANE ND 3.8
UG/L
1,2 DICHLOROETHANE ND 3.8
UG/L
1,1 DICHLOROETHYLENE ND 2.5
UG/L
CIS1,2DICHLOROETHYLENE ND 2.5
UG/L
TRANS 1,2 DICHLOROETHYLENE ND 3.8
UG/L
ETHYL BENZENE ND 2.5
UG/L
METHYLENECHLORIDE ND 2.5
UG/L
TOLUENE ND 2.5
UG/L
OXYLENE ND 2.5
UG/L
P/M XYLENE ND 5.0
UG/L
CARBON TETRACHLORIDE ND 2.5
UG/L
CHLOROFORM ND 2.5
UG/L
2BUTANONE (MEK)ND 25
UG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
E. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
4METHYL2PENTANONE (MIBK)ND 25
UG/L
TRICHLOROETHYLENE ND 2.5
UG/L
TETRACHLOROETHYLENE ND 2.5
UG/L
1,1,1 TRICHLOROETHANE ND 5.0
UG/L
VINYLCHLORIDE ND 2.5
UG/L
STYRENE ND 2.5
UG/L
CHLOROBENZENE ND 8.8
UG/L
METHYL TERTIARY BUTYL ETHER NS NS
UG/L
CHLOROETHANE ND 5.0
UG/L
1,2DICHLOROPROPANE ND 8.8
UG/L
DIBROMOCHLOROMETHANE ND 2.5
UG/L
1,1,2TRICHLOROETHANE ND 3.8
UG/L
2CHLOROETHYLVINYL ETHER ND 25
UG/L
BROMODICHLOROMETHANE ND 2.5
UG/L
BROMOFORM ND 2.5
UG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
E. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
1,1,2,2TETRACHLOROETHANE ND 2.5
UG/L
CHLOROMETHANE ND 12
UG/L
BROMOMETHANE ND 12
UG/L
CARBONDISULFIDE ND 12
UG/L
2HEXANONE ND 25
UG/L
ACROLEIN ND 20
UG/L
ACRYLONITRILE ND 25
UG/L
TRANS1,3DICHLOROPROPENE ND 3.8
UG/L
CIS1,3DICHLOROPROPENE ND 3.8
UG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/26/2021 NOT APPLICABLE
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
BEA NSU PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Monitoring Well Data Report 2021 Mar Monthly
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
C. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
DRY = Not enough water in well to sample.
<
Parameter/Contaminant MW1 MW2 MW3 MW4
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
PH 6.14 5.78 6.18 5.63
S.U.
STATIC WATER LEVEL 33.79 33.03 33.19 33.32
FEET
SPECIFIC CONDUCTANCE 87.6 190.2 342.6 91.5
UMHOS/C
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/26/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Monitoring Well Data Report 2021 Quarterly 1
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
C. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
DRY = Not enough water in well to sample.
<
Parameter/Contaminant MW1 MW2 MW3 MW4
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
NITRATEN 1.8 1.1 2.9 1.0
MG/L
TOTAL NITROGEN(NO3+NO2+TK 2.32 1.10 3.25 1.00
MG/L
TOTAL PHOSPHORUS AS P 0.052 ND 0.021 0.027
MG/L
ORTHO PHOSPHATE ND 0.010 0.008 ND
MG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/26/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Monitoring Well Data Report 2021 Annual
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
D. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
DRY = Not enough water in well to sample.
Parameter/Contaminant MW1 MW2 MW3 MW4
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
ACETONE ND ND ND ND
UG/L
BENZENE ND ND ND ND
UG/L
1,1 DICHLOROETHANE ND ND ND ND
UG/L
1,2 DICHLOROETHANE ND ND ND ND
UG/L
1,1 DICHLOROETHYLENE ND ND ND ND
UG/L
CIS1,2DICHLOROETHYLENE ND ND ND ND
UG/L
TRANS 1,2 DICHLOROETHYLENE ND ND ND ND
UG/L
ETHYL BENZENE ND ND ND ND
UG/L
METHYLENECHLORIDE ND ND ND ND
UG/L
TOLUENE ND ND ND ND
UG/L
OXYLENE ND ND ND ND
UG/L
P/M XYLENE ND ND ND ND
UG/L
CARBON TETRACHLORIDE ND ND ND ND
UG/L
CHLOROFORM 1.2 1.8 ND ND
UG/L
2BUTANONE (MEK)ND ND ND ND
UG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
D. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
DRY = Not enough water in well to sample.
Parameter/Contaminant MW1 MW2 MW3 MW4
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
4METHYL2PENTANONE (MIBK ND ND ND ND
UG/L
TRICHLOROETHYLENE ND ND ND ND
UG/L
TETRACHLOROETHYLENE ND ND ND ND
UG/L
1,1,1 TRICHLOROETHANE ND ND ND ND
UG/L
VINYLCHLORIDE ND ND ND ND
UG/L
STYRENE ND ND ND ND
UG/L
CHLOROBENZENE ND ND ND ND
UG/L
METHYL TERTIARY BUTYL ETHE NS NS NS NS
UG/L
CHLOROETHANE ND ND ND ND
UG/L
1,2DICHLOROPROPANE ND ND ND ND
UG/L
DIBROMOCHLOROMETHANE ND ND ND ND
UG/L
1,1,2TRICHLOROETHANE ND ND ND ND
UG/L
2CHLOROETHYLVINYL ETHER ND ND ND ND
UG/L
BROMODICHLOROMETHANE ND ND ND ND
UG/L
BROMOFORM ND ND ND ND
UG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
D. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
DRY = Not enough water in well to sample.
Parameter/Contaminant MW1 MW2 MW3 MW4
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
1,1,2,2TETRACHLOROETHANE ND ND ND ND
UG/L
CHLOROMETHANE ND ND ND ND
UG/L
BROMOMETHANE ND ND ND ND
UG/L
CARBONDISULFIDE ND ND ND ND
UG/L
2HEXANONE ND ND ND ND
UG/L
ACROLEIN ND ND ND ND
UG/L
ACRYLONITRILE ND ND ND ND
UG/L
TRANS1,3DICHLOROPROPENE ND ND ND ND
UG/L
CIS1,3DICHLOROPROPENE ND ND ND ND
UG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
951
1. Permit Number
465405799
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
Any person signing
a document under
314 CMR 5.14(1) or
(2) shall make the
following
certification
If you are filing
electronically and
want to attach
additional
comments, select
the check box.
Facility Information
MAPLEWOOD AT BREWSTER
a. Name
820 HARWICH ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
Certification
“I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.
Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware that the
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.”
SAMANTHA FARRENKOPF 4/16/2021
a. Signature b. Date (mm/dd/yyyy)
Reporting Package Comments
BENNETT ENVIRONMENTAL ASSOCIATES, LLC. (BEA) HAS COMPLETED THE MARCH 2021
MONTHLY INFLUENT AND EFFLUENT SAMPLING OF THE BIOCLERE WASTEWATER
TREATMENT SYSTEM. MONTHLY WASTEWATER SAMPLING WAS COMPLETED ON 3/17/21.
LABORATORY RESULTS REPORTED ALL PARAMETERS WITHIN DISCHARGE PERMIT
LIMITATIONS. EFFLUENT PH WAS REPORTED WITHIN THE 6.5 TO 8.5 RANGE THROUGHOUT
THE MONTH. FLOW VOLUME MEASUREMENTS WERE ASSESSED DURING THE MONTH
FROM THE SYSTEM’S EFFLUENT FLOW METER. DAILY FLOW REMAINED WITHIN THE
19,800GPD LIMITATION THROUGHOUT THE MONTH. THE MINIMUM, MAXIMUM AND AVERAGE
GPD FLOWS REPORTED OVER THE COURSE OF THE MONTH WERE 175 GPD, 9,911 GPD
AND 5,386 GPD, RESPECTIVELY.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
951
1. Permit Number
465405799
2. Tax identification Number
L2113382
Bennett Environmental Associates
K10842DA.S.WW.700
MAPLEWOOD AT BREWSTER
Client:
Project Name:
Project Number:
03/24/21
Eight Walkup Drive, Westborough, MA 01581-1019
Lab Number:
Report Date:
508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com
1573 Main Street
Brewster, MA 02631
Joe SmithATTN:
ANALYTICAL REPORT
Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148),
NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).
(508) 896-1706Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its
entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:03242112:37
Page 1 of 29
L2113382-01
L2113382-02
Alpha
Sample ID
INFLUENT
EFFLUENT
Client ID
BREWSTER, MA
BREWSTER, MA
Sample
Location
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2113382
03/24/21
03/17/21 11:30
03/17/21 11:00
Collection
Date/TimeMatrix Receive Date
WATER
WATER
03/17/21
03/17/21
Serial_No:03242112:37
Page 2 of 29
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2113382
03/24/21
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter
(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list
for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified
Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target
Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality
control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"
or "RE", respectively.
When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in
the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed
Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria
for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the
specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC
information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in
conjunction with the sample result, associated regulatory criteria and any associated data usability implications.
Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms
used in this report are provided in the Glossary located at the back of the report.
HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21
calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put
on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air
canisters will be disposed after 3 business days from the date the project is completed.
Please contact Project Management at 800-624-9220 with any questions.
Serial_No:03242112:37
Page 3 of 29
Case Narrative (continued)
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2113382
03/24/21
Volatile Organics by Method 624
L2113382-02D: The sample has elevated detection limits due to the dilution required by the sample matrix.
The sample is cloudy and has particles.
L2113382-02D: Due to the matrix of the sample (foam generation during purging/analysis), the laboratory used
Anti-Foam solution in the sample and associated QC.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 03/24/21
Serial_No:03242112:37
Page 4 of 29
ORGANICS
Serial_No:03242112:37
Page 5 of 29
VOLATILES
Serial_No:03242112:37
Page 6 of 29
FF
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
2.5
3.8
2.5
2.5
8.8
2.5
3.8
25
2.5
8.8
12
3.8
5.0
2.5
3.8
3.8
2.5
2.5
2.5
2.5
2.5
12
12
2.5
5.0
2.5
3.8
2.5
03/24/21
EFFLUENTClient ID:
03/17/21 11:00Date Collected:
03/17/21Date Received:
BREWSTER, MASample Location:
L2113382-02Lab ID:
Field Prep:Not Specified
D
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/18/21 19:13
GT
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03242112:37
Page 7 of 29
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
2.5
12
12
12
5.0
2.5
2.5
2.5
25
12
25
25
25
25
20
25
2.5
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
104
100
94
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
03/24/21
EFFLUENTClient ID:
03/17/21 11:00Date Collected:
03/17/21Date Received:
BREWSTER, MASample Location:
L2113382-02Lab ID:
Field Prep:Not Specified
D
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03242112:37
Page 8 of 29
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
03/18/21 17:06
128,624.1Analytical Method:
Analytical Date:
03/24/21
Analyst:GT
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 02 Batch: WG1477171-10
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03242112:37
Page 9 of 29
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
03/18/21 17:06
128,624.1Analytical Method:
Analytical Date:
03/24/21
Analyst:GT
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 02 Batch: WG1477171-10
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
99
100
98
60-140
60-140
60-140
Surrogate %Recovery Qualifier
Acceptance
Criteria
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03242112:37
Page 10 of 29
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
125
110
120
125
105
105
105
85
115
90
150
125
120
115
100
105
85
100
105
110
100
105
95
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
60-140
50-150
70-135
70-130
35-165
70-135
70-130
1-225
70-130
65-135
50-150
70-130
70-130
65-135
50-150
25-175
70-130
60-140
65-135
70-130
60-140
1-205
15-185
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
28
49
54
41
55
50
45
71
39
53
84
49
36
56
86
58
42
61
61
41
63
60
61
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 02 Batch: WG1477171-9
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
03/24/21
Qual Qual Qual
Serial_No:03242112:37
Page 11 of 29
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
115
120
120
110
110
105
95
95
100
100
95
95
120
100
112
132
108
112
130
112
100
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
5-195
40-160
50-150
70-130
60-140
65-135
65-135
70-130
65-135
60-140
60-140
60-140
40-160
60-140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
66
78
32
45
30
48
57
43
57
30
30
30
30
30
30
30
30
30
30
60
30
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 02 Batch: WG1477171-9
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
03/24/21
Qual Qual Qual
Serial_No:03242112:37
Page 12 of 29
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 02 Batch: WG1477171-9
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
105
102
92
60-140
60-140
60-140
Surrogate Qual%Recovery Qual%Recovery
LCS LCSD
03/24/21
Acceptance
Criteria
Qual Qual Qual
Serial_No:03242112:37
Page 13 of 29
INORGANICS
&
MISCELLANEOUS
Serial_No:03242112:37
Page 14 of 29
FF
INFLUENTClient ID:
03/17/21 11:30Date Collected:
03/17/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2113382-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Solids, Total
Solids, Total Suspended
Nitrogen, Ammonia
BOD, 5 day
520
79.
12.8
160
mg/l
mg/l
mg/l
mg/l
2
5
5
15
20
25
0.375
30
03/22/21 08:00
03/22/21 15:55
03/23/21 19:26
03/23/21 12:30
121,2540B
121,2540D
121,4500NH3-BH
121,5210B
DW
AC
AT
MT
Date
Prepared
-
-
03/19/21 17:30
03/18/21 16:10
03/24/21
MDL
NA
NA
--
NA
Sample Depth:
Serial_No:03242112:37
Page 15 of 29
FF
EFFLUENTClient ID:
03/17/21 11:00Date Collected:
03/17/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2113382-02Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Solids, Total Suspended
Nitrogen, Ammonia
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
BOD, 5 day
Oil & Grease, Hem-Grav
25.
1.04
ND
ND
6.12
6.83
5.23
29.
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
2.9
5
1
1
2
12.5
25
2.5
1
14
0.375
0.050
0.10
0.600
0.125
0.125
5.0
4.0
03/22/21 15:55
03/23/21 19:27
03/18/21 05:56
03/18/21 05:56
03/23/21 17:04
03/22/21 13:54
03/18/21 01:30
03/23/21 12:30
03/22/21 14:30
121,2540D
121,4500NH3-BH
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
121,5210B
74,1664A
AC
AT
MR
MR
AT
SD
AW
MT
TL
Date
Prepared
-
03/19/21 17:30
-
-
03/22/21 17:00
03/19/21 12:15
-
03/18/21 16:10
03/22/21 10:00
03/24/21
MDL
NA
--
--
--
--
--
--
NA
--
Sample Depth:
Serial_No:03242112:37
Page 16 of 29
FF
Parameter Result
Dilution
FactorQualifierUnitsRL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
03/24/21
Phosphorus, Orthophosphate
Nitrogen, Nitrite
Nitrogen, Nitrate
BOD, 5 day
Phosphorus, Total
Nitrogen, Ammonia
Solids, Total
Oil & Grease, Hem-Grav
Solids, Total Suspended
Nitrogen, Total Kjeldahl
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
0.005
0.050
0.10
2.0
0.010
0.075
10
4.0
5.0
0.300
03/18/21 01:24
03/18/21 05:41
03/18/21 05:38
03/23/21 12:30
03/22/21 13:04
03/23/21 19:22
03/22/21 08:00
03/22/21 14:30
03/22/21 15:55
03/23/21 16:59
121,4500P-E
44,353.2
44,353.2
121,5210B
121,4500P-E
121,4500NH3-BH
121,2540B
74,1664A
121,2540D
121,4500NH3-H
AW
MR
MR
MT
SD
AT
DW
TL
AC
AT
-
-
-
03/18/21 16:10
03/19/21 12:15
03/19/21 17:30
-
03/22/21 10:00
-
03/22/21 17:00
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1475701-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1475710-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1475711-1
General Chemistry - Westborough Lab for sample(s): 01-02 Batch: WG1475990-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1476331-1
General Chemistry - Westborough Lab for sample(s): 01-02 Batch: WG1476587-1
General Chemistry - Westborough Lab for sample(s): 01 Batch: WG1476998-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1477123-1
General Chemistry - Westborough Lab for sample(s): 01-02 Batch: WG1477225-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1477313-1
MDL
--
--
--
NA
--
--
NA
--
NA
--
Serial_No:03242112:37
Page 17 of 29
Phosphorus, Orthophosphate
Nitrogen, Nitrite
Nitrogen, Nitrate
BOD, 5 day
Phosphorus, Total
Nitrogen, Ammonia
Solids, Total
94
102
94
86
103
92
95
-
-
-
-
-
-
-
90-110
90-110
90-110
85-115
80-120
80-120
80-120
-
-
-
-
-
-
-
20
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1475701-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1475710-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1475711-2
General Chemistry - Westborough Lab Associated sample(s): 01-02 Batch: WG1475990-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1476331-2
General Chemistry - Westborough Lab Associated sample(s): 01-02 Batch: WG1476587-2
General Chemistry - Westborough Lab Associated sample(s): 01 Batch: WG1476998-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
03/24/21
Qual Qual Qual
Serial_No:03242112:37
Page 18 of 29
Oil & Grease, Hem-Grav
Solids, Total Suspended
Nitrogen, Total Kjeldahl
100
97
99
-
-
-
78-114
80-120
78-122
-
-
-
18
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1477123-2
General Chemistry - Westborough Lab Associated sample(s): 01-02 Batch: WG1477225-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1477313-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
03/24/21
Serial_No:03242112:37
Page 19 of 29
Phosphorus, Orthophosphate
Nitrogen, Nitrite
Nitrogen, Nitrate
BOD, 5 day
Phosphorus, Total
Nitrogen, Ammonia
Oil & Grease, Hem-Grav
Nitrogen, Total Kjeldahl
ND
0.24
17
2.7
0.189
0.076
ND
ND
0.487
4.8
21
130
0.706
3.44
36
7.07
97
114
100
128
103
84
94
88
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
80-120
80-120
83-113
50-145
75-125
80-120
78-114
77-111
-
-
-
-
-
-
-
-
20
20
6
35
20
20
18
24
Parameter
Native
Sample
MS
Found
MS
%Recovery
MSD
Found
MSD
%Recovery
Recovery
Limits RPD
RPD
Limits
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1475701-4 QC Sample: L2113186-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1475710-4 QC Sample: L2113308-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1475711-4 QC Sample: L2113308-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1475990-4 QC Sample: L2113380-03 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1476331-3 QC Sample: L2112897-02 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1476587-4 QC Sample: L2113323-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1477123-4 QC Sample: L2109826-140 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1477313-4 QC Sample: L2113323-01 Client ID: MS Sample
0.5
4
4
100
0.5
4
38.5
8
MS
Added
Matrix Spike Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2113382
03/24/21
Qual Qual Qual
Serial_No:03242112:37
Page 20 of 29
Phosphorus, Orthophosphate
Nitrogen, Nitrite
Nitrogen, Nitrate
BOD, 5 day
Phosphorus, Total
Nitrogen, Ammonia
Solids, Total
Oil & Grease, Hem-Grav
Solids, Total Suspended
ND
0.24
17
2.7
0.189
0.076
410
9.1
79
ND
0.24
17
ND
0.180
ND
400
23
84
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
NC
0
0
NC
5
NC
2
87
6
20
20
6
35
20
20
16
18
29
Units RPDParameterNative Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1475701-3 QC Sample: L2113186-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1475710-3 QC Sample: L2113308-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1475711-3 QC Sample: L2113308-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1475990-3 QC Sample: L2113380-03 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1476331-4 QC Sample: L2112897-02 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1476587-3 QC Sample: L2113323-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1476998-3 QC Sample: L2112984-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1477123-3 QC Sample: L2109826-139 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1477225-3 QC Sample: L2113382-01 Client ID: INFLUENT
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
L2113382Lab Number:
Report Date:
Lab Duplicate Analysis
Batch Quality Control
03/24/21
Qual
Q
Serial_No:03242112:37
Page 21 of 29
Nitrogen, Total Kjeldahl ND ND mg/l NC 24
Units RPDParameterNative Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1477313-3 QC Sample: L2113323-01 Client ID: DUP Sample
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
L2113382Lab Number:
Report Date:
Lab Duplicate Analysis
Batch Quality Control
03/24/21
Serial_No:03242112:37
Page 22 of 29
*Values in parentheses indicate holding time in days
L2113382-01A
L2113382-01B
L2113382-01C
L2113382-02A
L2113382-02B
L2113382-02C
L2113382-02D
L2113382-02E
L2113382-02F
L2113382-02G
L2113382-02H
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Plastic 950ml unpreserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 950ml H2SO4 preserved
Plastic 950ml unpreserved
Plastic 950ml unpreserved
Amber 1000ml HCl preserved
Amber 1000ml HCl preserved
A
A
A
A
A
A
A
A
A
A
A
<2
7
7
NA
NA
NA
<2
7
7
NA
NA
3.8
3.8
3.8
3.8
3.8
3.8
3.8
3.8
3.8
3.8
3.8
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
A Absent
Cooler Custody Seal
Cooler Information
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
NH3-4500(28)
TSC-2540(7),BOD-5210(2)
TSS-2540(7)
624.1(3)
624.1(3)
624.1(3)
TKN-4500(28),TPHOS-4500(28),NH3-4500(28)
OPHOS-4500(2),NO2-353(2),BOD-
5210(2),NO3-353(2)
TSS-2540(7)
OG-1664(28)
OG-1664(28)
Project Name:
Project Number:
L2113382Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
03/24/21
Were project specific reporting limits specified?YES
<2
7
7
<2
7
7
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:03242112:37
Page 23 of 29
Report Format:Data Usability Report
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L2113382MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700 03/24/21
Acronyms
DL
EDL
EMPC
EPA
LCS
LCSD
LFB
LOD
LOQ
MDL
MS
MSD
NA
NC
NDPA/DPA
NI
NP
NR
RL
RPD
SRM
STLP
TEF
TEQ
TIC
Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when
those target analyte concentrations are quantified below the limit of quantitation (LOQ). The DL includes any adjustments
from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)
Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction (SPME).
Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an
analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case
estimate of the concentration.
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Limit of Detection: This value represents the level to which a target analyte can reliably be detected for a specific analyte in a
specific matrix by a specific method. The LOD includes any adjustments from dilutions, concentrations or moisture content,
where applicable. (DoD report formats only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable.
Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available. For Method 332.0, the spike recovery is calculated
using the native concentration, including estimated values.
Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit.
N-Nitrosodiphenylamine/Diphenylamine.
Not Ignitable.
Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.
No Results: Term is utilized when 'No Target Compounds Requested' is reported for the analysis of Volatile or Semivolatile
Organic TIC only requests.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL
includes any adjustments from dilutions, concentrations or moisture content, where applicable.
Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less
than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values; although the RPD value will be provided in the report.
Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the
associated field samples.
Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.
Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF
and then summing the resulting values.
Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound
list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Serial_No:03242112:37
Page 24 of 29
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2113382MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700 03/24/21
Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is
shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Difference: With respect to Total Oxidizable Precursor (TOP) Assay analysis, the difference is defined as the Post-Treatment value minus the
Pre-Treatment value.
Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after
adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.
Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-
preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.
Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined upon
receipt, if applicable.
PAH Total: With respect to Alkylated PAH analyses, the 'PAHs, Total' result is defined as the summation of results for all or a subset of the
following compounds: Naphthalene, C1-C4 Naphthalenes, 2-Methylnaphthalene, 1-Methylnaphthalene, Biphenyl, Acenaphthylene,
Acenaphthene, Fluorene, C1-C3 Fluorenes, Phenanthrene, C1-C4 Phenanthrenes/Anthracenes, Anthracene, Fluoranthene, Pyrene, C1-C4
Fluoranthenes/Pyrenes, Benz(a)anthracene, Chrysene, C1-C4 Chrysenes, Benzo(b)fluoranthene, Benzo(j)+(k)fluoranthene, Benzo(e)pyrene,
Benzo(a)pyrene, Perylene, Indeno(1,2,3-cd)pyrene, Dibenz(ah)+(ac)anthracene, Benzo(g,h,i)perylene. If a 'Total' result is requested, the
results of its individual components will also be reported.
PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA,
PFNA and PFOS. In addition, the 'PFAS, Total (6)' result is defined as the summation of results at or above the RL for: PFHpA, PFHxS,
PFOA, PFNA, PFDA and PFOS. (Note: 'PFAS, Total (6)' is applicable to MassDEP DW compliance analysis only.). If a 'Total' result is
requested, the results of its individual components will also be reported.
The target compound Chlordane (CAS No. 57-74-9) is reported for GC ECD analyses. Per EPA,this compound "refers to a mixture of
chlordane isomers, other chlorinated hydrocarbons and numerous other components." (Reference: USEPA Toxicological Review of
Chlordane, In Support of Summary Information on the Integrated Risk Information System (IRIS), December 1997.)
Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total'
result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081
and 8082.
Data Qualifiers
A
B
C
D
E
F
G
H
I
J
M
ND
NJ
-
-
-
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensates" are byproducts of the extraction/concentration procedures when acetone is introduced in
the process.
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related
projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x)
the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above
one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-
Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable
concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone).
Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted
analyses.
Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations
of the analyte.
Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The ratio of quantifier ion response to qualifier ion response falls outside of the laboratory criteria. Results are considered to be an
estimated maximum concentration.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should
be considered estimated.
The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The lower value for the two columns has been reported due to obvious interference.
Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).
Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Not detected at the reporting limit (RL) for the sample.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
-
Footnotes
Serial_No:03242112:37
Page 25 of 29
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2113382MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700 03/24/21
Data Qualifiers
P
Q
R
RE
S
-
-
-
-
-
the identification is based on a mass spectral library search.
The RPD between the results for the two columns exceeds the method-specified criteria.
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than 5x the RL. (Metals only.)
Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
Analytical results are from modified screening analysis.
Serial_No:03242112:37
Page 26 of 29
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
44
74
121
128
Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
Method 1664,Revision A: N-Hexane Extractable Material (HEM; Oil & Grease) and
Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material) by
Extraction and Gravimetry, EPA-821-R-98-002, February 1999.
Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
Method 624.1: Purgeables by GC/MS, EPA 821-R-16-008, December 2016.
Project Name:
Project Number:
Lab Number:
Report Date:
L2113382MAPLEWOOD AT BREWSTER
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REFERENCES
03/24/21
Serial_No:03242112:37
Page 27 of 29
Alpha Analytical, Inc.ID No.:17873
Facility: Company-wide Revision 18
Department: Quality Assurance Published Date: 2/16/2021 5:32:02 PM
Title: Certificate/Approval Program Summary Page 1 of 1
Document Type: Form Pre-Qualtrax Document ID: 08-113
Certification Information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA 624/624.1: m/p-xylene, o-xylene, Naphthalene
EPA 8260C/8260D: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), 1,2,4,5-Tetramethylbenzene;
4-Ethyltoluene.
EPA 8270D/8270E: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.
SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.
Mansfield Facility
SM 2540D: TSS
EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.
EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene,
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene.
Biological Tissue Matrix: EPA 3050B
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE,
EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B, SM4500NO2-B
EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.
Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1:
Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E,
SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate.
EPA 624.1: Volatile Halocarbons & Aromatics,
EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II,
Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603, SM9222D.
Mansfield Facility:
Drinking Water
EPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.
EPA 522, EPA 537.1.
Non-Potable Water
EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn.
EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Serial_No:03242112:37
Page 28 of 29
Serial_No:03242112:37
Page 29 of 29
L2115333
Bennett Environmental Associates
K10842DA.S.WW.700
MAPLEWOOD AT BREWSTER
Client:
Project Name:
Project Number:
04/05/21
Eight Walkup Drive, Westborough, MA 01581-1019
Lab Number:
Report Date:
508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com
1573 Main Street
Brewster, MA 02631
Joe SmithATTN:
ANALYTICAL REPORT
Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148),
NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).
(508) 896-1706Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its
entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:04052113:37
Page 1 of 35
L2115333-01
L2115333-02
L2115333-03
L2115333-04
Alpha
Sample ID
MW-1
MW-2
MW-3
MW-4
Client ID
BREWSTER, MA
BREWSTER, MA
BREWSTER, MA
BREWSTER, MA
Sample
Location
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2115333
04/05/21
03/26/21 09:30
03/26/21 10:30
03/26/21 11:30
03/26/21 12:30
Collection
Date/TimeMatrix Receive Date
WATER
WATER
WATER
WATER
03/26/21
03/26/21
03/26/21
03/26/21
Serial_No:04052113:37
Page 2 of 35
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2115333
04/05/21
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter
(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list
for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified
Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target
Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality
control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"
or "RE", respectively.
When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in
the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed
Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria
for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the
specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC
information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in
conjunction with the sample result, associated regulatory criteria and any associated data usability implications.
Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms
used in this report are provided in the Glossary located at the back of the report.
HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21
calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put
on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air
canisters will be disposed after 3 business days from the date the project is completed.
Please contact Project Management at 800-624-9220 with any questions.
Serial_No:04052113:37
Page 3 of 35
Case Narrative (continued)
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2115333
04/05/21
Volatile Organics by Method 624
The WG1479948-3 LCS recoveries, associated with L2115333-01 through -04, are above the acceptance
criteria for bromoform (140%), 1,2-dichlorobenzene (155%), 1,3-dichlorobenzene (145%) and 1,4-
dichlorobenzene (150%); however, the associated samples are non-detect to the RL for these target analytes.
The results of the original analysis are reported.
Nitrogen, Nitrate
The WG1479468-4 MS recovery, performed on L2115333-01, is outside the acceptance criteria for nitrogen,
nitrate (128%); however, the associated LCS recovery is within criteria. No further action was taken.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 04/05/21
Serial_No:04052113:37
Page 4 of 35
ORGANICS
Serial_No:04052113:37
Page 5 of 35
VOLATILES
Serial_No:04052113:37
Page 6 of 35
FF
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
1.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
04/05/21
MW-1Client ID:
03/26/21 09:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-01Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/27/21 09:57
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 7 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
100
93
122
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
04/05/21
MW-1Client ID:
03/26/21 09:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-01Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 8 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
1.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
04/05/21
MW-2Client ID:
03/26/21 10:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-02Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/27/21 10:32
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 9 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
96
90
122
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
04/05/21
MW-2Client ID:
03/26/21 10:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-02Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 10 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
04/05/21
MW-3Client ID:
03/26/21 11:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-03Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/27/21 11:07
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 11 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
101
92
122
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
04/05/21
MW-3Client ID:
03/26/21 11:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-03Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 12 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
04/05/21
MW-4Client ID:
03/26/21 12:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-04Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/27/21 11:42
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 13 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
97
90
122
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
04/05/21
MW-4Client ID:
03/26/21 12:30Date Collected:
03/26/21Date Received:
BREWSTER, MASample Location:
L2115333-04Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 14 of 35
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
03/27/21 08:47
128,624.1Analytical Method:
Analytical Date:
04/05/21
Analyst:MKS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-04 Batch: WG1479948-4
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:04052113:37
Page 15 of 35
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
03/27/21 08:47
128,624.1Analytical Method:
Analytical Date:
04/05/21
Analyst:MKS
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-04 Batch: WG1479948-4
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
100
92
121
60-140
60-140
60-140
Surrogate %Recovery Qualifier
Acceptance
Criteria
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:04052113:37
Page 16 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
105
95
105
120
90
115
105
125
125
110
110
100
110
115
100
110
140
125
95
115
130
70
65
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
60-140
50-150
70-135
70-130
35-165
70-135
70-130
1-225
70-130
65-135
50-150
70-130
70-130
65-135
50-150
25-175
70-130
60-140
65-135
70-130
60-140
1-205
15-185
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
28
49
54
41
55
50
45
71
39
53
84
49
36
56
86
58
42
61
61
41
63
60
61
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-04 Batch: WG1479948-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
04/05/21
Qual Qual
Q
Qual
Serial_No:04052113:37
Page 17 of 35
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
85
90
100
100
110
100
155
145
150
130
125
120
64
100
64
78
80
68
75
78
95
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
5-195
40-160
50-150
70-130
60-140
65-135
65-135
70-130
65-135
60-140
60-140
60-140
40-160
60-140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
66
78
32
45
30
48
57
43
57
30
30
30
30
30
30
30
30
30
30
60
30
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-04 Batch: WG1479948-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
04/05/21
Qual Qual
Q
Q
Q
Qual
Serial_No:04052113:37
Page 18 of 35
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-04 Batch: WG1479948-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
103
93
121
60-140
60-140
60-140
Surrogate Qual%Recovery Qual%Recovery
LCS LCSD
04/05/21
Acceptance
Criteria
Qual Qual Qual
Serial_No:04052113:37
Page 19 of 35
INORGANICS
&
MISCELLANEOUS
Serial_No:04052113:37
Page 20 of 35
FF
MW-1Client ID:
03/26/21 09:30Date Collected:
03/26/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2115333-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
1.8
0.524
0.052
ND
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.300
0.010
0.005
03/27/21 07:07
03/27/21 07:07
04/05/21 11:39
03/30/21 13:28
03/27/21 05:26
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
JO
SD
AW
Date
Prepared
-
-
04/02/21 19:45
03/30/21 10:15
-
04/05/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 21 of 35
FF
MW-2Client ID:
03/26/21 10:30Date Collected:
03/26/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2115333-02Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
1.1
ND
ND
0.010
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.300
0.010
0.005
03/27/21 07:13
03/27/21 07:13
04/05/21 11:40
03/30/21 13:32
03/27/21 05:27
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
JO
SD
AW
Date
Prepared
-
-
04/02/21 19:45
03/30/21 10:15
-
04/05/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 22 of 35
FF
MW-3Client ID:
03/26/21 11:30Date Collected:
03/26/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2115333-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
2.9
0.353
0.021
0.008
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.300
0.010
0.005
03/27/21 07:15
03/27/21 07:15
04/05/21 11:41
03/30/21 13:35
03/27/21 05:27
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
JO
SD
AW
Date
Prepared
-
-
04/02/21 19:45
03/30/21 10:15
-
04/05/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 23 of 35
FF
MW-4Client ID:
03/26/21 12:30Date Collected:
03/26/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2115333-04Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
1.0
ND
0.027
ND
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.300
0.010
0.005
03/27/21 07:20
03/27/21 07:20
04/05/21 11:42
03/30/21 13:36
03/27/21 05:28
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
JO
SD
AW
Date
Prepared
-
-
04/02/21 19:45
03/30/21 10:15
-
04/05/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:04052113:37
Page 24 of 35
FF
Parameter Result
Dilution
FactorQualifierUnitsRL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
04/05/21
Nitrogen, Nitrite
Nitrogen, Nitrate
Phosphorus, Orthophosphate
Phosphorus, Total
Nitrogen, Total Kjeldahl
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.005
0.010
0.300
03/27/21 05:29
03/27/21 05:26
03/27/21 05:24
03/30/21 13:25
04/05/21 11:27
44,353.2
44,353.2
121,4500P-E
121,4500P-E
121,4500NH3-H
MR
MR
AW
SD
JO
-
-
-
03/30/21 10:15
04/02/21 19:45
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1479467-1
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1479468-1
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1479478-1
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1480356-1
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1482033-1
MDL
--
--
--
--
--
Serial_No:04052113:37
Page 25 of 35
Nitrogen, Nitrite
Nitrogen, Nitrate
Phosphorus, Orthophosphate
Phosphorus, Total
Nitrogen, Total Kjeldahl
106
100
94
105
100
-
-
-
-
-
90-110
90-110
90-110
80-120
78-122
-
-
-
-
-
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1479467-2
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1479468-2
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1479478-2
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1480356-2
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1482033-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
04/05/21
Qual Qual Qual
Serial_No:04052113:37
Page 26 of 35
Nitrogen, Nitrite
Nitrogen, Nitrate
Phosphorus, Orthophosphate
Phosphorus, Total
Nitrogen, Total Kjeldahl
ND
1.8
ND
0.052
ND
4.6
6.9
0.482
0.549
7.36
115
128
96
99
92
-
-
-
-
-
-
-
-
-
-
80-120
83-113
80-120
75-125
77-111
-
-
-
-
-
20
6
20
20
24
Parameter
Native
Sample
MS
Found
MS
%Recovery
MSD
Found
MSD
%Recovery
Recovery
Limits RPD
RPD
Limits
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1479467-4 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1479468-4 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1479478-4 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1480356-3 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1482033-4 QC Sample: L2115333-04 Client ID: MW-4
4
4
0.5
0.5
8
MS
Added
Matrix Spike Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
L2115333
04/05/21
Qual
Q
Qual Qual
Serial_No:04052113:37
Page 27 of 35
Nitrogen, Nitrite
Nitrogen, Nitrate
Phosphorus, Orthophosphate
Phosphorus, Total
Nitrogen, Total Kjeldahl
ND
1.8
ND
0.052
ND
ND
1.8
ND
0.048
ND
mg/l
mg/l
mg/l
mg/l
mg/l
NC
0
NC
8
NC
20
6
20
20
24
Units RPDParameterNative Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1479467-3 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1479468-3 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1479478-3 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1480356-4 QC Sample: L2115333-01 Client ID: MW-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1482033-3 QC Sample: L2115333-04 Client ID: MW-4
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
Project Name:
Project Number:
L2115333Lab Number:
Report Date:
Lab Duplicate Analysis
Batch Quality Control
04/05/21
Qual
Serial_No:04052113:37
Page 28 of 35
*Values in parentheses indicate holding time in days
L2115333-01A
L2115333-01B
L2115333-01C
L2115333-01D
L2115333-01E
L2115333-02A
L2115333-02B
L2115333-02C
L2115333-02D
L2115333-02E
L2115333-03A
L2115333-03B
L2115333-03C
L2115333-03D
L2115333-03E
L2115333-04A
L2115333-04B
L2115333-04C
L2115333-04D
L2115333-04E
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
NA
NA
NA
7
<2
NA
NA
NA
7
<2
NA
NA
NA
7
<2
NA
NA
NA
7
<2
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
B Absent
Cooler Custody Seal
Cooler Information
MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
Project Name:
Project Number:
L2115333Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
04/05/21
Were project specific reporting limits specified?YES
7
<2
7
<2
7
<2
7
<2
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:04052113:37
Page 29 of 35
Report Format:Data Usability Report
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L2115333MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700 04/05/21
Acronyms
DL
EDL
EMPC
EPA
LCS
LCSD
LFB
LOD
LOQ
MDL
MS
MSD
NA
NC
NDPA/DPA
NI
NP
NR
RL
RPD
SRM
STLP
TEF
TEQ
TIC
Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when
those target analyte concentrations are quantified below the limit of quantitation (LOQ). The DL includes any adjustments
from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)
Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction (SPME).
Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an
analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case
estimate of the concentration.
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Limit of Detection: This value represents the level to which a target analyte can reliably be detected for a specific analyte in a
specific matrix by a specific method. The LOD includes any adjustments from dilutions, concentrations or moisture content,
where applicable. (DoD report formats only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable.
Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available. For Method 332.0, the spike recovery is calculated
using the native concentration, including estimated values.
Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit.
N-Nitrosodiphenylamine/Diphenylamine.
Not Ignitable.
Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.
No Results: Term is utilized when 'No Target Compounds Requested' is reported for the analysis of Volatile or Semivolatile
Organic TIC only requests.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL
includes any adjustments from dilutions, concentrations or moisture content, where applicable.
Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less
than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values; although the RPD value will be provided in the report.
Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the
associated field samples.
Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.
Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF
and then summing the resulting values.
Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound
list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Serial_No:04052113:37
Page 30 of 35
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2115333MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700 04/05/21
Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is
shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Difference: With respect to Total Oxidizable Precursor (TOP) Assay analysis, the difference is defined as the Post-Treatment value minus the
Pre-Treatment value.
Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after
adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.
Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-
preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.
Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined upon
receipt, if applicable.
PAH Total: With respect to Alkylated PAH analyses, the 'PAHs, Total' result is defined as the summation of results for all or a subset of the
following compounds: Naphthalene, C1-C4 Naphthalenes, 2-Methylnaphthalene, 1-Methylnaphthalene, Biphenyl, Acenaphthylene,
Acenaphthene, Fluorene, C1-C3 Fluorenes, Phenanthrene, C1-C4 Phenanthrenes/Anthracenes, Anthracene, Fluoranthene, Pyrene, C1-C4
Fluoranthenes/Pyrenes, Benz(a)anthracene, Chrysene, C1-C4 Chrysenes, Benzo(b)fluoranthene, Benzo(j)+(k)fluoranthene, Benzo(e)pyrene,
Benzo(a)pyrene, Perylene, Indeno(1,2,3-cd)pyrene, Dibenz(ah)+(ac)anthracene, Benzo(g,h,i)perylene. If a 'Total' result is requested, the
results of its individual components will also be reported.
PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA,
PFNA and PFOS. In addition, the 'PFAS, Total (6)' result is defined as the summation of results at or above the RL for: PFHpA, PFHxS,
PFOA, PFNA, PFDA and PFOS. (Note: 'PFAS, Total (6)' is applicable to MassDEP DW compliance analysis only.). If a 'Total' result is
requested, the results of its individual components will also be reported.
The target compound Chlordane (CAS No. 57-74-9) is reported for GC ECD analyses. Per EPA,this compound "refers to a mixture of
chlordane isomers, other chlorinated hydrocarbons and numerous other components." (Reference: USEPA Toxicological Review of
Chlordane, In Support of Summary Information on the Integrated Risk Information System (IRIS), December 1997.)
Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total'
result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081
and 8082.
Data Qualifiers
A
B
C
D
E
F
G
H
I
J
M
ND
NJ
-
-
-
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensates" are byproducts of the extraction/concentration procedures when acetone is introduced in
the process.
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related
projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x)
the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above
one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-
Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable
concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone).
Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted
analyses.
Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations
of the analyte.
Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The ratio of quantifier ion response to qualifier ion response falls outside of the laboratory criteria. Results are considered to be an
estimated maximum concentration.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should
be considered estimated.
The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The lower value for the two columns has been reported due to obvious interference.
Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).
Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Not detected at the reporting limit (RL) for the sample.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
-
Footnotes
Serial_No:04052113:37
Page 31 of 35
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2115333MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700 04/05/21
Data Qualifiers
P
Q
R
RE
S
-
-
-
-
-
the identification is based on a mass spectral library search.
The RPD between the results for the two columns exceeds the method-specified criteria.
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than 5x the RL. (Metals only.)
Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
Analytical results are from modified screening analysis.
Serial_No:04052113:37
Page 32 of 35
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
44
121
128
Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
Method 624.1: Purgeables by GC/MS, EPA 821-R-16-008, December 2016.
Project Name:
Project Number:
Lab Number:
Report Date:
L2115333MAPLEWOOD AT BREWSTER
K10842DA.S.WW.700
REFERENCES
04/05/21
Serial_No:04052113:37
Page 33 of 35
Alpha Analytical, Inc.ID No.:17873
Facility: Company-wide Revision 19
Department: Quality Assurance Published Date: 4/2/2021 1:14:23 PM
Title: Certificate/Approval Program Summary Page 1 of 1
Document Type: Form Pre-Qualtrax Document ID: 08-113
Certification Information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA 624/624.1: m/p-xylene, o-xylene, Naphthalene
EPA 625/625.1: alpha-Terpineol
EPA 8260C/8260D: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), 1,2,4,5-Tetramethylbenzene;
4-Ethyltoluene.
EPA 8270D/8270E: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine, alpha-Terpineol; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.
SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.
Mansfield Facility
SM 2540D: TSS
EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.
EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene,
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene.
Biological Tissue Matrix: EPA 3050B
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE,
EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B, SM4500NO2-B
EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.
Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1:
Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E,
SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate.
EPA 624.1: Volatile Halocarbons & Aromatics,
EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II,
Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603, SM9222D.
Mansfield Facility:
Drinking Water
EPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.
EPA 522, EPA 537.1.
Non-Potable Water
EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn.
EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Serial_No:04052113:37
Page 34 of 35
Serial_No:04052113:37
Page 35 of 35
Massachusetts Department of Environmental Protection
eDEP Transaction Copy
Here is the file you requested for your records.
To retain a copy of this file you must save and/or print.
Username:
Transaction ID:
Document:
Size of File:
Status of Transaction:
Date and Time Created:
Note: This file only includes forms that were part of your
transaction as of the date and time indicated above. If you need
a more current copy of your transaction, return to eDEP and
select to “Download a Copy” from the Current Submittals page.
1273005
4/15/2021:1:38:28 PM
2773.87K
SFARRENKOPF
Groundwater Discharge Monitoring Report Forms
In Process
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/1/2021 NOT APPLICABLE
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
BEA NSU PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Daily Log Sheet 2021 Mar Daily
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DAILY LOG SHEET
746
1. Permit Number
200303120
2. Tax identification Number
2021 MAR DAILY
3. Sampling Month & Frequency
C. Daily Readings/Analysis Information
Date Effluent
Flow GPD
Reuse
Flow GPD
Irrigation
Flow GPD
Turbidity Influent pH Effluent
pH
Chlorine
Residual
(mg/l)
UV
Intensity
(%)
1 8278 7.5 74.3
2 14305 7.5 66.7
3 16615 7.7 66.6
4 12821 7.2 66.6
5 10265 8.0 7.3 66.7
6 10265
7 10265
8 10625 7.4 66.6
9 10164 7.6 66.7
10 8993 7.6 66.6
11 11278 7.6 66.7
12 7987 8.1 7.3 69.1
13 7987
14 7987
15 6918 7.8 69.1
16 10977 7.6 74.1
17 12580 7.4 69.1
18 8800 7.3 69.2
19 8716 7.9 7.8 56.3
20 8716
21 8716
22 4528 7.7 74.2
23 9267 7.4 74.1
24 8635 7.6 74.3
25 8478 7.4 74.1
26 9182 7.8 7.3 69.1
27 9182
28 9182
29 8674 7.4 66.7
30 4570 7.5 66.7
31 11264 7.5 66.6
gdpdls.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DAILY LOG SHEET
746
1. Permit Number
200303120
2. Tax identification Number
2021 MAR DAILY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/5/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Discharge Monitoring Report 2021 Mar Monthly
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
D. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
BOD 680 2.8 2.0
MG/L
TSS 460 ND 5.0
MG/L
TOTAL SOLIDS 1200 250 10
MG/L
AMMONIAN 9.66
MG/L
NITRATEN 4.6 0.10
MG/L
TOTAL NITROGEN(NO3+NO2+TKN)5.75 0.450
MG/L
OIL & GREASE ND 4.0
MG/L
FECAL COLIFORM ND 10
/100 ML
CHLORIDE 43 1.0
MG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/5/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Discharge Monitoring Report 2021 Quarterly 1
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
D. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
TOTAL PHOSPHORUS AS P 2.97 0.050
MG/L
ORTHO PHOSPHATE 2.43 0.125
MG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/5/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Discharge Monitoring Report 2021 Annual
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
E. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
ACETONE 71 ND 10
UG/L
BENZENE ND ND 1.0
UG/L
1,1 DICHLOROETHANE ND ND 1.5
UG/L
1,2 DICHLOROETHANE ND ND 1.5
UG/L
1,1 DICHLOROETHYLENE ND ND 1.0
UG/L
CIS1,2DICHLOROETHYLENE ND ND 1.0
UG/L
TRANS 1,2 DICHLOROETHYLENE ND ND 1.5
UG/L
ETHYL BENZENE ND ND 1.0
UG/L
METHYLENECHLORIDE ND ND 1.0
UG/L
TOLUENE 4.8 ND 1.0
UG/L
OXYLENE ND ND 1.0
UG/L
P/M XYLENE ND ND 2.0
UG/L
CARBON TETRACHLORIDE ND ND 1.0
UG/L
CHLOROFORM 2.2 ND 1.0
UG/L
2BUTANONE (MEK)ND ND 10
UG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
E. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
4METHYL2PENTANONE (MIBK)ND ND 10
UG/L
TRICHLOROETHYLENE ND ND 1.0
UG/L
TETRACHLOROETHYLENE ND ND 1.0
UG/L
1,1,1 TRICHLOROETHANE ND ND 2.0
UG/L
VINYLCHLORIDE ND ND 1.0
UG/L
STYRENE ND ND 1.0
UG/L
CHLOROBENZENE ND ND 3.5
UG/L
METHYL TERTIARY BUTYL ETHER NS NS NS
UG/L
CHLOROETHANE ND ND 2.0
UG/L
1,2DICHLOROPROPANE ND ND 3.5
UG/L
DIBROMOCHLOROMETHANE ND ND 1.0
UG/L
1,1,2TRICHLOROETHANE ND ND 1.5
UG/L
2CHLOROETHYLVINYL ETHER ND ND 10
UG/L
BROMODICHLOROMETHANE ND ND 1.0
UG/L
BROMOFORM ND ND 1.0
UG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
E. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
1,1,2,2TETRACHLOROETHANE ND ND 1.0
UG/L
CHLOROMETHANE ND ND 5.0
UG/L
BROMOMETHANE ND ND 5.0
UG/L
CARBONDISULFIDE ND ND 5.0
UG/L
2HEXANONE ND ND 10
UG/L
ACROLEIN ND ND 8.0
UG/L
ACRYLONITRILE ND ND 10
UG/L
TRANS1,3DICHLOROPROPENE ND ND 1.5
UG/L
CIS1,3DICHLOROPROPENE ND ND 1.5
UG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/5/2021 NOT APPLICABLE
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
BEA NSU PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Monitoring Well Data Report 2021 Mar Monthly
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
C. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
DRY = Not enough water in well to sample.
<
Parameter/Contaminant DG1 DG2 DG4 UG1
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
PH 6.08 6.63 6.77 6.49
S.U.
STATIC WATER LEVEL 11.81 11.86 11.82 12.36
FEET
SPECIFIC CONDUCTANCE 196 317.4 324 150.9
UMHOS/C
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 MAR MONTHLY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/5/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Monitoring Well Data Report 2021 Quarterly 1
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
C. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
DRY = Not enough water in well to sample.
<
Parameter/Contaminant DG1 DG2 DG4 UG1
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
NITRATEN 1.6 3.9 4.7 2.0
MG/L
TOTAL NITROGEN(NO3+NO2+TK 2.14 4.21 4.70 2.00
MG/L
TOTAL PHOSPHORUS AS P 0.016 0.035 1.13 0.021
MG/L
ORTHO PHOSPHATE ND 0.010 0.023 0.023
MG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 QUARTERLY 1
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JOSEPH SMITH
a. Name of Facility Contact Person
7742125005 jsmith@NSUWater.com
b. Telephone Number c. email address
3. Sampling information:
3/5/2021 ALPHA ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
ALPHA ANALYTICAL PERSONNEL
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Monitoring Well Data Report 2021 Annual
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
D. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
DRY = Not enough water in well to sample.
Parameter/Contaminant DG1 DG2 DG4 UG1
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
ACETONE ND ND ND ND
UG/L
BENZENE ND ND ND ND
UG/L
1,1 DICHLOROETHANE ND ND ND ND
UG/L
1,2 DICHLOROETHANE ND ND ND ND
UG/L
1,1 DICHLOROETHYLENE ND ND ND ND
UG/L
CIS1,2DICHLOROETHYLENE ND ND ND ND
UG/L
TRANS 1,2 DICHLOROETHYLENE ND ND ND ND
UG/L
ETHYL BENZENE ND ND ND ND
UG/L
METHYLENECHLORIDE ND ND ND ND
UG/L
TOLUENE ND ND ND ND
UG/L
OXYLENE ND ND ND ND
UG/L
P/M XYLENE ND ND ND ND
UG/L
CARBON TETRACHLORIDE ND ND ND ND
UG/L
CHLOROFORM 1.4 ND ND ND
UG/L
2BUTANONE (MEK)ND ND ND ND
UG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
D. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
DRY = Not enough water in well to sample.
Parameter/Contaminant DG1 DG2 DG4 UG1
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
4METHYL2PENTANONE (MIBK ND ND ND ND
UG/L
TRICHLOROETHYLENE ND ND ND ND
UG/L
TETRACHLOROETHYLENE ND ND ND ND
UG/L
1,1,1 TRICHLOROETHANE ND ND ND ND
UG/L
VINYLCHLORIDE ND ND ND ND
UG/L
STYRENE ND ND ND ND
UG/L
CHLOROBENZENE ND ND ND ND
UG/L
METHYL TERTIARY BUTYL ETHE NS NS NS NS
UG/L
CHLOROETHANE ND ND ND ND
UG/L
1,2DICHLOROPROPANE ND ND ND ND
UG/L
DIBROMOCHLOROMETHANE ND ND ND ND
UG/L
1,1,2TRICHLOROETHANE ND ND ND ND
UG/L
2CHLOROETHYLVINYL ETHER ND ND ND ND
UG/L
BROMODICHLOROMETHANE ND ND ND ND
UG/L
BROMOFORM ND ND ND ND
UG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
D. VOC Analysis Information
If VOCs are present, please indicate the amounts of the individual compounds in µg/l.
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
NS = Not Sampled
DRY = Not enough water in well to sample.
Parameter/Contaminant DG1 DG2 DG4 UG1
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
1,1,2,2TETRACHLOROETHANE ND ND ND ND
UG/L
CHLOROMETHANE ND ND ND ND
UG/L
BROMOMETHANE ND ND ND ND
UG/L
CARBONDISULFIDE ND ND ND ND
UG/L
2HEXANONE ND ND ND ND
UG/L
ACROLEIN ND ND ND ND
UG/L
ACRYLONITRILE ND ND ND ND
UG/L
TRANS1,3DICHLOROPROPENE ND ND ND ND
UG/L
CIS1,3DICHLOROPROPENE ND ND ND ND
UG/L
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
746
1. Permit Number
200303120
2. Tax identification Number
2021 ANNUAL
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
Any person signing
a document under
314 CMR 5.14(1) or
(2) shall make the
following
certification
If you are filing
electronically and
want to attach
additional
comments, select
the check box.
Facility Information
PLEASANT BAY HEALTH CTR
a. Name
383 SOUTH ORLEANS ROAD
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
Certification
“I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.
Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware that the
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.”
SAMANTHA FARRENKOPF 4/15/2021
a. Signature b. Date (mm/dd/yyyy)
Reporting Package Comments
BENNETT ENVIRONMENTAL ASSOCIATES, LLC. (BEA) HAS COMPLETED THE MARCH 2021
MONTHLY INFLUENT AND EFFLUENT SAMPLING OF THE AMPHIDROME WASTEWATER
TREATMENT SYSTEM. MONTHLY WASTEWATER SAMPLING WAS COMPLETED ON 3/5/21.
LABORATORY RESULTS REPORTED ALL PARAMETERS WITHIN DISCHARGE PERMIT
LIMITATIONS. EFFLUENT PH WAS REPORTED WITHIN THE 6.58.5 RANGE THROUGHOUT THE
MONTH. FLOW VOLUME MEASUREMENTS WERE ASSESSED DURING THE MONTH FROM
THE SYSTEM’S EFFLUENT FLOW METER. DAILY FLOW REMAINED WITHIN THE 26,500GPD
LIMITATION THROUGHOUT THE MONTH. THE MINIMUM, MAXIMUM AND AVERAGE GPD
FLOWS REPORTED OVER THE COURSE OF THE MONTH WERE 4,528 GPD, 16,615 GPD AND
9,555 GPD, RESPECTIVELY.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
746
1. Permit Number
200303120
2. Tax identification Number
L2111128
Bennett Environmental Associates
K47810DA.S.WW.700
PLEASANT BAY
Client:
Project Name:
Project Number:
03/12/21
Eight Walkup Drive, Westborough, MA 01581-1019
Lab Number:
Report Date:
508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com
1573 Main Street
Brewster, MA 02631
Joe SmithATTN:
ANALYTICAL REPORT
Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148),
NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).
(508) 896-1706Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its
entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:03122117:15
Page 1 of 37
L2111128-01
L2111128-02
L2111128-03
Alpha
Sample ID
INFLUENT
EFFLUENT
EFFLUENT
Client ID
BREWSTER, MA
BREWSTER, MA
BREWSTER, MA
Sample
Location
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2111128
03/12/21
03/05/21 13:55
03/05/21 14:15
03/05/21 14:15
Collection
Date/TimeMatrix Receive Date
WATER
WATER
WATER
03/05/21
03/05/21
03/05/21
Serial_No:03122117:15
Page 2 of 37
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2111128
03/12/21
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter
(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list
for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified
Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target
Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality
control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"
or "RE", respectively.
When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in
the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed
Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria
for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the
specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC
information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in
conjunction with the sample result, associated regulatory criteria and any associated data usability implications.
Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms
used in this report are provided in the Glossary located at the back of the report.
HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21
calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put
on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air
canisters will be disposed after 3 business days from the date the project is completed.
Please contact Project Management at 800-624-9220 with any questions.
Serial_No:03122117:15
Page 3 of 37
Case Narrative (continued)
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2111128
03/12/21
Volatile Organics by Method 624
The WG1471937-9 LCS recovery, associated with L2111128-02, is above the acceptance criteria for vinyl
acetate (145%); however, the associated sample is non-detect to the RL for this target analyte. The results of
the original analysis are reported.
Coliform, Fecal (MF)
L2111128-03: The sample has an elevated detection limit due to the dilution required by the sample matrix.
Oil & Grease, Hem-Grav
The WG1472943-4 MS recovery, performed on L2111128-02, is outside the acceptance criteria for oil &
grease, hem-grav (32%); however, the associated LCS recovery is within criteria. No further action was taken.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 03/12/21
Serial_No:03122117:15
Page 4 of 37
ORGANICS
Serial_No:03122117:15
Page 5 of 37
VOLATILES
Serial_No:03122117:15
Page 6 of 37
FF
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
2.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.8
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
03/12/21
INFLUENTClient ID:
03/05/21 13:55Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111128-01Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/06/21 10:18
MKS
MDL
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--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122117:15
Page 7 of 37
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
71
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
95
94
92
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
03/12/21
INFLUENTClient ID:
03/05/21 13:55Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111128-01Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122117:15
Page 8 of 37
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
03/12/21
EFFLUENTClient ID:
03/05/21 14:15Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111128-02Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/08/21 14:50
GT
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122117:15
Page 9 of 37
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
97
96
104
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
03/12/21
EFFLUENTClient ID:
03/05/21 14:15Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111128-02Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122117:15
Page 10 of 37
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/06/21 01:25
128,624.1Analytical Method:
Analytical Date:
03/12/21
Analyst:MKS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 01 Batch: WG1471521-4
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03122117:15
Page 11 of 37
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/06/21 01:25
128,624.1Analytical Method:
Analytical Date:
03/12/21
Analyst:MKS
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 01 Batch: WG1471521-4
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
98
95
100
60-140
60-140
60-140
Surrogate %Recovery Qualifier
Acceptance
Criteria
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03122117:15
Page 12 of 37
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/08/21 13:16
128,624.1Analytical Method:
Analytical Date:
03/12/21
Analyst:GT
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 02 Batch: WG1471937-10
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03122117:15
Page 13 of 37
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/08/21 13:16
128,624.1Analytical Method:
Analytical Date:
03/12/21
Analyst:GT
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 02 Batch: WG1471937-10
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
100
96
97
60-140
60-140
60-140
Surrogate %Recovery Qualifier
Acceptance
Criteria
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03122117:15
Page 14 of 37
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
110
110
125
125
115
110
110
46
130
110
95
110
125
130
110
115
100
115
115
120
115
125
80
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
60-140
50-150
70-135
70-130
35-165
70-135
70-130
1-225
70-130
65-135
50-150
70-130
70-130
65-135
50-150
25-175
70-130
60-140
65-135
70-130
60-140
1-205
15-185
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
28
49
54
41
55
50
45
71
39
53
84
49
36
56
86
58
42
61
61
41
63
60
61
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01 Batch: WG1471521-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/12/21
Qual Qual Qual
Serial_No:03122117:15
Page 15 of 37
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
80
100
95
110
110
110
105
105
105
115
110
100
84
105
102
125
106
118
105
100
90
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
5-195
40-160
50-150
70-130
60-140
65-135
65-135
70-130
65-135
60-140
60-140
60-140
40-160
60-140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
66
78
32
45
30
48
57
43
57
30
30
30
30
30
30
30
30
30
30
60
30
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01 Batch: WG1471521-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/12/21
Qual Qual Qual
Serial_No:03122117:15
Page 16 of 37
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01 Batch: WG1471521-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
100
97
100
60-140
60-140
60-140
Surrogate Qual%Recovery Qual%Recovery
LCS LCSD
03/12/21
Acceptance
Criteria
Qual Qual Qual
Serial_No:03122117:15
Page 17 of 37
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
105
115
115
125
110
110
105
65
120
95
90
110
120
125
105
110
100
105
110
115
100
110
75
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
60-140
50-150
70-135
70-130
35-165
70-135
70-130
1-225
70-130
65-135
50-150
70-130
70-130
65-135
50-150
25-175
70-130
60-140
65-135
70-130
60-140
1-205
15-185
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
28
49
54
41
55
50
45
71
39
53
84
49
36
56
86
58
42
61
61
41
63
60
61
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 02 Batch: WG1471937-9
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/12/21
Qual Qual Qual
Serial_No:03122117:15
Page 18 of 37
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
70
105
100
115
105
105
100
95
95
98
95
85
110
100
110
145
108
120
125
115
90
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
5-195
40-160
50-150
70-130
60-140
65-135
65-135
70-130
65-135
60-140
60-140
60-140
40-160
60-140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
66
78
32
45
30
48
57
43
57
30
30
30
30
30
30
30
30
30
30
60
30
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 02 Batch: WG1471937-9
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/12/21
Qual Qual
Q
Qual
Serial_No:03122117:15
Page 19 of 37
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 02 Batch: WG1471937-9
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
100
98
93
60-140
60-140
60-140
Surrogate Qual%Recovery Qual%Recovery
LCS LCSD
03/12/21
Acceptance
Criteria
Qual Qual Qual
Serial_No:03122117:15
Page 20 of 37
INORGANICS
&
MISCELLANEOUS
Serial_No:03122117:15
Page 21 of 37
FF
INFLUENTClient ID:
03/05/21 13:55Date Collected:
03/05/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2111128-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Solids, Total
Solids, Total Suspended
Nitrogen, Ammonia
BOD, 5 day
1200
460
9.66
680
mg/l
mg/l
mg/l
mg/l
2
10
5
60
20
50
0.375
120
03/09/21 07:10
03/10/21 15:55
03/11/21 18:20
03/10/21 18:45
121,2540B
121,2540D
121,4500NH3-BH
121,5210B
DW
AC
AT
JW
Date
Prepared
-
-
03/11/21 09:00
03/06/21 00:25
03/12/21
MDL
NA
NA
--
NA
Sample Depth:
Serial_No:03122117:15
Page 22 of 37
FF
EFFLUENTClient ID:
03/05/21 14:15Date Collected:
03/05/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2111128-02Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Solids, Total
Solids, Total Suspended
Chloride
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
BOD, 5 day
Oil & Grease, Hem-Grav
250
ND
43.
ND
4.6
1.15
2.97
2.43
2.8
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
5
25
1
1
10
5.0
1.0
0.050
0.10
0.300
0.050
0.125
2.0
4.0
03/09/21 07:10
03/10/21 15:55
03/09/21 00:13
03/06/21 06:16
03/06/21 06:16
03/11/21 17:20
03/12/21 15:37
03/06/21 02:06
03/10/21 18:45
03/10/21 22:00
121,2540B
121,2540D
121,4500CL-E
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
121,5210B
74,1664A
DW
AC
TL
MR
MR
AT
JB
AW
JW
IR
Date
Prepared
-
-
-
-
-
03/11/21 08:26
03/12/21 00:00
-
03/06/21 00:25
03/10/21 19:00
03/12/21
MDL
NA
NA
--
--
--
--
--
--
NA
--
Sample Depth:
Serial_No:03122117:15
Page 23 of 37
FF
EFFLUENTClient ID:
03/05/21 14:15Date Collected:
03/05/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2111128-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
Microbiological Analysis - Westborough Lab
Coliform, Fecal (MF)ND col/100ml 1010 03/05/21 20:15 121,9222D CC
Date
Prepared
-
03/12/21
MDL
NA
Sample Depth:
Serial_No:03122117:15
Page 24 of 37
FF
Parameter Result
Dilution
FactorQualifierUnitsRL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
03/12/21
Coliform, Fecal (MF)
BOD, 5 day
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Chloride
Solids, Total
Phosphorus, Total
Solids, Total Suspended
Oil & Grease, Hem-Grav
Nitrogen, Total Kjeldahl
Nitrogen, Ammonia
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
col/100ml
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1.0
2.0
0.005
0.10
0.050
1.0
10
0.010
5.0
4.0
0.300
0.075
03/05/21 20:15
03/10/21 18:45
03/06/21 02:02
03/06/21 05:04
03/06/21 05:07
03/08/21 22:34
03/09/21 07:10
03/12/21 15:06
03/10/21 15:55
03/10/21 22:00
03/11/21 17:05
03/11/21 18:00
121,9222D
121,5210B
121,4500P-E
44,353.2
44,353.2
121,4500CL-E
121,2540B
121,4500P-E
121,2540D
74,1664A
121,4500NH3-H
121,4500NH3-BH
CC
JW
AW
MR
MR
TL
DW
JB
AC
IR
AT
AT
-
03/06/21 00:25
-
-
-
-
-
03/12/21 00:00
-
03/10/21 19:00
03/11/21 08:26
03/11/21 09:00
Microbiological Analysis - Westborough Lab for sample(s): 03 Batch: WG1471332-1
General Chemistry - Westborough Lab for sample(s): 01-02 Batch: WG1471350-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1471366-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1471386-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1471387-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1472005-1
General Chemistry - Westborough Lab for sample(s): 01-02 Batch: WG1472142-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1472768-1
General Chemistry - Westborough Lab for sample(s): 01-02 Batch: WG1472825-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1472943-1
General Chemistry - Westborough Lab for sample(s): 02 Batch: WG1473107-1
General Chemistry - Westborough Lab for sample(s): 01 Batch: WG1473185-1
MDL
NA
NA
--
--
--
--
NA
--
NA
--
--
--
Serial_No:03122117:15
Page 25 of 37
BOD, 5 day
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Chloride
Solids, Total
Phosphorus, Total
107
97
104
98
100
101
105
-
-
-
-
-
-
-
85-115
90-110
90-110
90-110
90-110
80-120
80-120
-
-
-
-
-
-
-
20
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01-02 Batch: WG1471350-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1471366-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1471386-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1471387-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1472005-2
General Chemistry - Westborough Lab Associated sample(s): 01-02 Batch: WG1472142-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1472768-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/12/21
Qual Qual Qual
Serial_No:03122117:15
Page 26 of 37
Solids, Total Suspended
Oil & Grease, Hem-Grav
Nitrogen, Total Kjeldahl
Nitrogen, Ammonia
105
83
101
96
-
-
-
-
80-120
78-114
78-122
80-120
-
-
-
-
18
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01-02 Batch: WG1472825-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1472943-2
General Chemistry - Westborough Lab Associated sample(s): 02 Batch: WG1473107-2
General Chemistry - Westborough Lab Associated sample(s): 01 Batch: WG1473185-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/12/21
Serial_No:03122117:15
Page 27 of 37
BOD, 5 day
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Chloride
Phosphorus, Total
Oil & Grease, Hem-Grav
Nitrogen, Total Kjeldahl
Nitrogen, Ammonia
14
0.078
2.0
ND
500
4.86
ND
ND
0.169
130
0.575
5.8
4.5
510
3.55
12
6.24
3.77
117
99
95
112
50
0
32
78
90
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
50-145
80-120
83-113
80-120
58-140
75-125
78-114
77-111
80-120
-
-
-
-
-
-
-
-
-
35
20
6
20
7
20
18
24
20
Parameter
Native
Sample
MS
Found
MS
%Recovery
MSD
Found
MSD
%Recovery
Recovery
Limits RPD
RPD
Limits
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1471350-4 QC Sample: L2110960-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1471366-4 QC Sample: L2111121-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1471386-4 QC Sample: L2111119-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1471387-4 QC Sample: L2111119-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1472005-4 QC Sample: L2110173-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1472768-4 QC Sample: L2111124-02 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1472943-4 QC Sample: L2111128-02 Client ID: EFFLUENT
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1473107-4 QC Sample: L2111119-04 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1473185-4 QC Sample: L2111048-06 Client ID: MS Sample
100
0.5
4
4
20
0.5
37.7
8
4
MS
Added
Matrix Spike Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111128
03/12/21
Qual
Q
Q
Q
Qual Qual
Serial_No:03122117:15
Page 28 of 37
BOD, 5 day
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Chloride
Solids, Total
Phosphorus, Total
Solids, Total Suspended
Oil & Grease, Hem-Grav
14
0.078
2.0
ND
500
650
4.86
460
7.5
14
0.073
2.1
ND
520
630
5.15
440
6.7
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
0
7
5
NC
4
3
6
4
11
35
20
6
20
7
16
20
29
18
Units RPDParameterNative Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1471350-3 QC Sample: L2110960-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1471366-3 QC Sample: L2111121-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1471386-3 QC Sample: L2111119-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1471387-3 QC Sample: L2111119-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1472005-3 QC Sample: L2110173-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1472142-3 QC Sample: L2111048-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1472768-3 QC Sample: L2111124-02 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1472825-3 QC Sample: L2111128-01 Client ID: INFLUENT
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1472943-3 QC Sample: L2111087-01 Client ID: DUP Sample
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
L2111128Lab Number:
Report Date:
Lab Duplicate Analysis
Batch Quality Control
03/12/21
Qual
Serial_No:03122117:15
Page 29 of 37
Nitrogen, Total Kjeldahl
Nitrogen, Ammonia
ND
0.169
ND
0.118
mg/l
mg/l
NC
36
24
20
Units RPDParameterNative Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 02 QC Batch ID: WG1473107-3 QC Sample: L2111119-04 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1473185-3 QC Sample: L2111048-06 Client ID: DUP Sample
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
L2111128Lab Number:
Report Date:
Lab Duplicate Analysis
Batch Quality Control
03/12/21
Q
Serial_No:03122117:15
Page 30 of 37
*Values in parentheses indicate holding time in days
L2111128-01A
L2111128-01B
L2111128-01C
L2111128-01D
L2111128-01E
L2111128-01F
L2111128-02A
L2111128-02B
L2111128-02C
L2111128-02D
L2111128-02E
L2111128-02F
L2111128-02G
L2111128-02H
L2111128-02I
L2111128-03A
L2111128-03B
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Plastic 950ml unpreserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 60ml unpreserved
Plastic 500ml H2SO4 preserved
Plastic 950ml unpreserved
Plastic 950ml unpreserved
Amber 1000ml HCl preserved
Amber 1000ml HCl preserved
Bacteria Cup Na2S2O3 preserved
Bacteria Cup Na2S2O3 preserved
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
NA
NA
NA
<2
9
9
NA
NA
NA
7
<2
7
7
NA
NA
NA
NA
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
A Absent
Cooler Custody Seal
Cooler Information
PLEASANT BAY
K47810DA.S.WW.700
624.1(3)
624.1(3)
624.1(3)
NH3-4500(28)
TSC-2540(7),BOD-5210(2)
TSS-2540(7)
624.1(3)
624.1(3)
624.1(3)
CL-4500(28),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
OPHOS-4500(2),TSC-2540(7),BOD-5210(2)
TSS-2540(7)
OG-1664(28)
OG-1664(28)
F-COLI-MF(.33)
F-COLI-MF(.33)
Project Name:
Project Number:
L2111128Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
03/12/21
Were project specific reporting limits specified?YES
<2
9
9
7
<2
7
7
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:03122117:15
Page 31 of 37
Report Format:Data Usability Report
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L2111128PLEASANT BAY
K47810DA.S.WW.700 03/12/21
Acronyms
DL
EDL
EMPC
EPA
LCS
LCSD
LFB
LOD
LOQ
MDL
MS
MSD
NA
NC
NDPA/DPA
NI
NP
NR
RL
RPD
SRM
STLP
TEF
TEQ
TIC
Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when
those target analyte concentrations are quantified below the limit of quantitation (LOQ). The DL includes any adjustments
from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)
Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction (SPME).
Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an
analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case
estimate of the concentration.
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Limit of Detection: This value represents the level to which a target analyte can reliably be detected for a specific analyte in a
specific matrix by a specific method. The LOD includes any adjustments from dilutions, concentrations or moisture content,
where applicable. (DoD report formats only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable.
Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available. For Method 332.0, the spike recovery is calculated
using the native concentration, including estimated values.
Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit.
N-Nitrosodiphenylamine/Diphenylamine.
Not Ignitable.
Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.
No Results: Term is utilized when 'No Target Compounds Requested' is reported for the analysis of Volatile or Semivolatile
Organic TIC only requests.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL
includes any adjustments from dilutions, concentrations or moisture content, where applicable.
Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less
than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values; although the RPD value will be provided in the report.
Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the
associated field samples.
Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.
Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF
and then summing the resulting values.
Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound
list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Serial_No:03122117:15
Page 32 of 37
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2111128PLEASANT BAY
K47810DA.S.WW.700 03/12/21
Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is
shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Difference: With respect to Total Oxidizable Precursor (TOP) Assay analysis, the difference is defined as the Post-Treatment value minus the
Pre-Treatment value.
Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after
adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.
Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-
preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.
Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined upon
receipt, if applicable.
PAH Total: With respect to Alkylated PAH analyses, the 'PAHs, Total' result is defined as the summation of results for all or a subset of the
following compounds: Naphthalene, C1-C4 Naphthalenes, 2-Methylnaphthalene, 1-Methylnaphthalene, Biphenyl, Acenaphthylene,
Acenaphthene, Fluorene, C1-C3 Fluorenes, Phenanthrene, C1-C4 Phenanthrenes/Anthracenes, Anthracene, Fluoranthene, Pyrene, C1-C4
Fluoranthenes/Pyrenes, Benz(a)anthracene, Chrysene, C1-C4 Chrysenes, Benzo(b)fluoranthene, Benzo(j)+(k)fluoranthene, Benzo(e)pyrene,
Benzo(a)pyrene, Perylene, Indeno(1,2,3-cd)pyrene, Dibenz(ah)+(ac)anthracene, Benzo(g,h,i)perylene. If a 'Total' result is requested, the
results of its individual components will also be reported.
PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA,
PFNA and PFOS. In addition, the 'PFAS, Total (6)' result is defined as the summation of results at or above the RL for: PFHpA, PFHxS,
PFOA, PFNA, PFDA and PFOS. (Note: 'PFAS, Total (6)' is applicable to MassDEP DW compliance analysis only.). If a 'Total' result is
requested, the results of its individual components will also be reported.
The target compound Chlordane (CAS No. 57-74-9) is reported for GC ECD analyses. Per EPA,this compound "refers to a mixture of
chlordane isomers, other chlorinated hydrocarbons and numerous other components." (Reference: USEPA Toxicological Review of
Chlordane, In Support of Summary Information on the Integrated Risk Information System (IRIS), December 1997.)
Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total'
result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081
and 8082.
Data Qualifiers
A
B
C
D
E
F
G
H
I
J
M
ND
NJ
-
-
-
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensates" are byproducts of the extraction/concentration procedures when acetone is introduced in
the process.
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related
projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x)
the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above
one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-
Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable
concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone).
Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted
analyses.
Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations
of the analyte.
Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The ratio of quantifier ion response to qualifier ion response falls outside of the laboratory criteria. Results are considered to be an
estimated maximum concentration.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should
be considered estimated.
The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The lower value for the two columns has been reported due to obvious interference.
Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).
Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Not detected at the reporting limit (RL) for the sample.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
-
Footnotes
Serial_No:03122117:15
Page 33 of 37
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2111128PLEASANT BAY
K47810DA.S.WW.700 03/12/21
Data Qualifiers
P
Q
R
RE
S
-
-
-
-
-
the identification is based on a mass spectral library search.
The RPD between the results for the two columns exceeds the method-specified criteria.
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than 5x the RL. (Metals only.)
Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
Analytical results are from modified screening analysis.
Serial_No:03122117:15
Page 34 of 37
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
44
74
121
128
Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
Method 1664,Revision A: N-Hexane Extractable Material (HEM; Oil & Grease) and
Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material) by
Extraction and Gravimetry, EPA-821-R-98-002, February 1999.
Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
Method 624.1: Purgeables by GC/MS, EPA 821-R-16-008, December 2016.
Project Name:
Project Number:
Lab Number:
Report Date:
L2111128PLEASANT BAY
K47810DA.S.WW.700
REFERENCES
03/12/21
Serial_No:03122117:15
Page 35 of 37
Alpha Analytical, Inc.ID No.:17873
Facility: Company-wide Revision 18
Department: Quality Assurance Published Date: 2/16/2021 5:32:02 PM
Title: Certificate/Approval Program Summary Page 1 of 1
Document Type: Form Pre-Qualtrax Document ID: 08-113
Certification Information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA 624/624.1: m/p-xylene, o-xylene, Naphthalene
EPA 8260C/8260D: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), 1,2,4,5-Tetramethylbenzene;
4-Ethyltoluene.
EPA 8270D/8270E: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.
SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.
Mansfield Facility
SM 2540D: TSS
EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.
EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene,
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene.
Biological Tissue Matrix: EPA 3050B
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE,
EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B, SM4500NO2-B
EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.
Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1:
Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E,
SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate.
EPA 624.1: Volatile Halocarbons & Aromatics,
EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II,
Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603, SM9222D.
Mansfield Facility:
Drinking Water
EPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.
EPA 522, EPA 537.1.
Non-Potable Water
EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn.
EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Serial_No:03122117:15
Page 36 of 37
Serial_No:03122117:15
Page 37 of 37
L2111119
Bennett Environmental Associates
K47810DA.S.WW.700
PLEASANT BAY
Client:
Project Name:
Project Number:
03/12/21
Eight Walkup Drive, Westborough, MA 01581-1019
Lab Number:
Report Date:
508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com
1573 Main Street
Brewster, MA 02631
Joe SmithATTN:
ANALYTICAL REPORT
Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148),
NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).
(508) 896-1706Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its
entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:03122116:55
Page 1 of 35
L2111119-01
L2111119-02
L2111119-03
L2111119-04
Alpha
Sample ID
UG-1
DG-1
DG-2
DG-4
Client ID
BREWSTER, MA
BREWSTER, MA
BREWSTER, MA
BREWSTER, MA
Sample
Location
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2111119
03/12/21
03/05/21 09:00
03/05/21 10:00
03/05/21 11:00
03/05/21 12:00
Collection
Date/TimeMatrix Receive Date
WATER
WATER
WATER
WATER
03/05/21
03/05/21
03/05/21
03/05/21
Serial_No:03122116:55
Page 2 of 35
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2111119
03/12/21
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter
(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list
for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified
Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target
Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality
control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"
or "RE", respectively.
When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in
the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed
Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria
for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the
specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC
information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in
conjunction with the sample result, associated regulatory criteria and any associated data usability implications.
Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms
used in this report are provided in the Glossary located at the back of the report.
HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21
calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put
on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air
canisters will be disposed after 3 business days from the date the project is completed.
Please contact Project Management at 800-624-9220 with any questions.
Serial_No:03122116:55
Page 3 of 35
Case Narrative (continued)
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
Lab Number:
Report Date:
L2111119
03/12/21
Sample Receipt
L2111119-02: The sample was received above the appropriate pH for the Total Phosphorus - SM 4500 and
Total Kjeldahl Nitrogen - SM 4500 analysis. The laboratory added additional H2SO4 to a pH <2.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 03/12/21
Serial_No:03122116:55
Page 4 of 35
ORGANICS
Serial_No:03122116:55
Page 5 of 35
VOLATILES
Serial_No:03122116:55
Page 6 of 35
FF
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
03/12/21
UG-1Client ID:
03/05/21 09:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-01Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/06/21 04:35
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 7 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
95
95
100
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
03/12/21
UG-1Client ID:
03/05/21 09:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-01Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 8 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
1.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
03/12/21
DG-1Client ID:
03/05/21 10:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-02Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/06/21 05:13
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 9 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
94
93
101
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
03/12/21
DG-1Client ID:
03/05/21 10:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-02Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 10 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
03/12/21
DG-2Client ID:
03/05/21 11:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-03Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/06/21 05:51
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 11 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
92
92
101
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
03/12/21
DG-2Client ID:
03/05/21 11:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-03Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 12 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
03/12/21
DG-4Client ID:
03/05/21 12:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-04Lab ID:
Field Prep:Not Specified
Matrix:Water
Analytical Method:
Analytical Date:
Analyst:
128,624.1
03/06/21 06:28
MKS
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 13 of 35
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
1.0
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
94
94
100
60-140
60-140
60-140
Acceptance
CriteriaSurrogate % Recovery Qualifier
03/12/21
DG-4Client ID:
03/05/21 12:00Date Collected:
03/05/21Date Received:
BREWSTER, MASample Location:
L2111119-04Lab ID:
Field Prep:Not Specified
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 14 of 35
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
03/06/21 01:25
128,624.1Analytical Method:
Analytical Date:
03/12/21
Analyst:MKS
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.0
1.5
1.0
1.0
3.5
1.0
1.5
10
1.0
3.5
5.0
1.5
2.0
1.0
1.5
1.5
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.5
1.0
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-04 Batch: WG1471521-4
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03122116:55
Page 15 of 35
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
03/06/21 01:25
128,624.1Analytical Method:
Analytical Date:
03/12/21
Analyst:MKS
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Xylenes, Total
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
5.0
5.0
5.0
2.0
1.0
1.0
1.0
10
5.0
10
10
10
10
8.0
10
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-04 Batch: WG1471521-4
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
98
95
100
60-140
60-140
60-140
Surrogate %Recovery Qualifier
Acceptance
Criteria
MDL
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
--
Serial_No:03122116:55
Page 16 of 35
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
2-Chloroethylvinyl ether
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
110
110
125
125
115
110
110
46
130
110
95
110
125
130
110
115
100
115
115
120
115
125
80
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
60-140
50-150
70-135
70-130
35-165
70-135
70-130
1-225
70-130
65-135
50-150
70-130
70-130
65-135
50-150
25-175
70-130
60-140
65-135
70-130
60-140
1-205
15-185
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
28
49
54
41
55
50
45
71
39
53
84
49
36
56
86
58
42
61
61
41
63
60
61
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-04 Batch: WG1471521-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
03/12/21
Qual Qual Qual
Serial_No:03122116:55
Page 17 of 35
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
p/m-Xylene
o-xylene
Styrene
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Acrolein
Acrylonitrile
Dibromomethane
80
100
95
110
110
110
105
105
105
115
110
100
84
105
102
125
106
118
105
100
90
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
5-195
40-160
50-150
70-130
60-140
65-135
65-135
70-130
65-135
60-140
60-140
60-140
40-160
60-140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
66
78
32
45
30
48
57
43
57
30
30
30
30
30
30
30
30
30
30
60
30
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-04 Batch: WG1471521-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
03/12/21
Qual Qual Qual
Serial_No:03122116:55
Page 18 of 35
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD
RPD
Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-04 Batch: WG1471521-3
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
Pentafluorobenzene
Fluorobenzene
4-Bromofluorobenzene
100
97
100
60-140
60-140
60-140
Surrogate Qual%Recovery Qual%Recovery
LCS LCSD
03/12/21
Acceptance
Criteria
Qual Qual Qual
Serial_No:03122116:55
Page 19 of 35
INORGANICS
&
MISCELLANEOUS
Serial_No:03122116:55
Page 20 of 35
FF
UG-1Client ID:
03/05/21 09:00Date Collected:
03/05/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2111119-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
2.0
ND
0.021
0.023
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.300
0.010
0.005
03/06/21 06:18
03/06/21 06:18
03/11/21 18:43
03/11/21 12:43
03/06/21 02:00
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
AT
JB
AW
Date
Prepared
-
-
03/11/21 03:11
03/11/21 00:00
-
03/12/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 21 of 35
FF
DG-1Client ID:
03/05/21 10:00Date Collected:
03/05/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2111119-02Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
1.6
0.542
0.016
ND
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.300
0.010
0.005
03/06/21 06:28
03/06/21 06:28
03/11/21 18:44
03/11/21 12:44
03/06/21 02:00
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
AT
JB
AW
Date
Prepared
-
-
03/11/21 03:11
03/11/21 00:00
-
03/12/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 22 of 35
FF
DG-2Client ID:
03/05/21 11:00Date Collected:
03/05/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2111119-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
3.9
0.313
0.035
0.010
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
0.050
0.10
0.300
0.010
0.005
03/06/21 06:29
03/06/21 06:29
03/11/21 18:47
03/12/21 14:50
03/06/21 02:00
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
AT
JB
AW
Date
Prepared
-
-
03/11/21 03:11
03/12/21 00:00
-
03/12/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 23 of 35
FF
DG-4Client ID:
03/05/21 12:00Date Collected:
03/05/21Date Received:
Parameter Result
Dilution
Factor
Matrix:Water
BREWSTER, MASample Location:
L2111119-04Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
Field Prep:
Date
Analyzed
Analytical
Method Analyst
Not Specified
General Chemistry - Westborough Lab
Nitrogen, Nitrite
Nitrogen, Nitrate
Nitrogen, Total Kjeldahl
Phosphorus, Total
Phosphorus, Orthophosphate
ND
4.7
ND
1.13
1.00
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
5
2
0.050
0.10
0.300
0.050
0.010
03/06/21 06:31
03/06/21 06:31
03/11/21 17:08
03/12/21 15:36
03/06/21 02:01
44,353.2
44,353.2
121,4500NH3-H
121,4500P-E
121,4500P-E
MR
MR
AT
JB
AW
Date
Prepared
-
-
03/11/21 08:26
03/12/21 00:00
-
03/12/21
MDL
--
--
--
--
--
Sample Depth:
Serial_No:03122116:55
Page 24 of 35
FF
Parameter Result
Dilution
FactorQualifierUnitsRL
Method Blank Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
Date
Analyzed
Analytical
Method Analyst
Date
Prepared
03/12/21
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Phosphorus, Total
Phosphorus, Total
Nitrogen, Total Kjeldahl
Nitrogen, Total Kjeldahl
ND
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
0.005
0.10
0.050
0.010
0.010
0.300
0.300
03/06/21 01:53
03/06/21 05:04
03/06/21 05:07
03/11/21 15:12
03/12/21 14:48
03/11/21 18:40
03/11/21 17:05
121,4500P-E
44,353.2
44,353.2
121,4500P-E
121,4500P-E
121,4500NH3-H
121,4500NH3-H
AW
MR
MR
JB
JB
AT
AT
-
-
-
03/11/21 00:00
03/12/21 00:00
03/11/21 03:11
03/11/21 08:26
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1471365-1
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1471386-1
General Chemistry - Westborough Lab for sample(s): 01-04 Batch: WG1471387-1
General Chemistry - Westborough Lab for sample(s): 01-02 Batch: WG1472766-1
General Chemistry - Westborough Lab for sample(s): 03-04 Batch: WG1472767-1
General Chemistry - Westborough Lab for sample(s): 01-03 Batch: WG1473006-1
General Chemistry - Westborough Lab for sample(s): 04 Batch: WG1473107-1
MDL
--
--
--
--
--
--
--
Serial_No:03122116:55
Page 25 of 35
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Phosphorus, Total
Phosphorus, Total
Nitrogen, Total Kjeldahl
Nitrogen, Total Kjeldahl
98
104
98
104
101
102
101
-
-
-
-
-
-
-
90-110
90-110
90-110
80-120
80-120
78-122
78-122
-
-
-
-
-
-
-
20
Parameter
LCS
%Recovery
LCSD
%Recovery
%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1471365-2
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1471386-2
General Chemistry - Westborough Lab Associated sample(s): 01-04 Batch: WG1471387-2
General Chemistry - Westborough Lab Associated sample(s): 01-02 Batch: WG1472766-2
General Chemistry - Westborough Lab Associated sample(s): 03-04 Batch: WG1472767-2
General Chemistry - Westborough Lab Associated sample(s): 01-03 Batch: WG1473006-2
General Chemistry - Westborough Lab Associated sample(s): 04 Batch: WG1473107-2
Lab Control Sample Analysis
Batch Quality ControlProject Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
03/12/21
Qual Qual Qual
Serial_No:03122116:55
Page 26 of 35
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Phosphorus, Total
Phosphorus, Total
Nitrogen, Total Kjeldahl
Nitrogen, Total Kjeldahl
ND
2.0
ND
0.292
0.035
0.542
ND
0.501
5.8
4.5
0.821
0.573
7.16
6.24
100
95
112
106
108
83
78
-
-
-
-
-
-
-
-
-
-
-
-
-
-
80-120
83-113
80-120
75-125
75-125
77-111
77-111
-
-
-
-
-
-
-
20
6
20
20
20
24
24
Parameter
Native
Sample
MS
Found
MS
%Recovery
MSD
Found
MSD
%Recovery
Recovery
Limits RPD
RPD
Limits
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1471365-4 QC Sample: L2111097-01 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1471386-4 QC Sample: L2111119-01 Client ID: UG-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1471387-4 QC Sample: L2111119-01 Client ID: UG-1
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1472766-4 QC Sample: L2111097-07 Client ID: MS Sample
General Chemistry - Westborough Lab Associated sample(s): 03-04 QC Batch ID: WG1472767-4 QC Sample: L2111119-03 Client ID: DG-2
General Chemistry - Westborough Lab Associated sample(s): 01-03 QC Batch ID: WG1473006-4 QC Sample: L2111119-02 Client ID: DG-1
General Chemistry - Westborough Lab Associated sample(s): 04 QC Batch ID: WG1473107-4 QC Sample: L2111119-04 Client ID: DG-4
0.5
4
4
0.5
0.5
8
8
MS
Added
Matrix Spike Analysis
Batch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
PLEASANT BAY
K47810DA.S.WW.700
L2111119
03/12/21
Qual Qual Qual
Serial_No:03122116:55
Page 27 of 35
Phosphorus, Orthophosphate
Nitrogen, Nitrate
Nitrogen, Nitrite
Phosphorus, Total
Phosphorus, Total
Nitrogen, Total Kjeldahl
Nitrogen, Total Kjeldahl
ND
2.0
ND
0.292
0.035
0.542
ND
ND
2.1
ND
0.299
0.035
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
NC
5
NC
2
0
NC
NC
20
6
20
20
20
24
24
Units RPDParameterNative Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1471365-3 QC Sample: L2111097-01 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1471386-3 QC Sample: L2111119-01 Client ID: UG-1
General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1471387-3 QC Sample: L2111119-01 Client ID: UG-1
General Chemistry - Westborough Lab Associated sample(s): 01-02 QC Batch ID: WG1472766-3 QC Sample: L2111097-07 Client ID: DUP Sample
General Chemistry - Westborough Lab Associated sample(s): 03-04 QC Batch ID: WG1472767-3 QC Sample: L2111119-03 Client ID: DG-2
General Chemistry - Westborough Lab Associated sample(s): 01-03 QC Batch ID: WG1473006-3 QC Sample: L2111119-02 Client ID: DG-1
General Chemistry - Westborough Lab Associated sample(s): 04 QC Batch ID: WG1473107-3 QC Sample: L2111119-04 Client ID: DG-4
PLEASANT BAY
K47810DA.S.WW.700
Project Name:
Project Number:
L2111119Lab Number:
Report Date:
Lab Duplicate Analysis
Batch Quality Control
03/12/21
Qual
Serial_No:03122116:55
Page 28 of 35
*Values in parentheses indicate holding time in days
L2111119-01A
L2111119-01B
L2111119-01C
L2111119-01D
L2111119-01E
L2111119-02A
L2111119-02B
L2111119-02C
L2111119-02D
L2111119-02E
L2111119-03A
L2111119-03B
L2111119-03C
L2111119-03D
L2111119-03E
L2111119-04A
L2111119-04B
L2111119-04C
L2111119-04D
L2111119-04E
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Vial Na2S2O3 preserved
Plastic 250ml unpreserved
Plastic 500ml H2SO4 preserved
A
A
A
A
A
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
NA
NA
NA
7
<2
NA
NA
NA
7
6
NA
NA
NA
7
<2
NA
NA
NA
7
<2
4.1
4.1
4.1
4.1
4.1
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
Y
Y
Y
Y
Y
Y
Y
Y
Y
N
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
A
B
Absent
Absent
Cooler Custody Seal
Cooler Information
PLEASANT BAY
K47810DA.S.WW.700
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
624.1(3)
624.1(3)
624.1(3)
OPHOS-4500(2),NO2-353(2),NO3-353(2)
TKN-4500(28),TPHOS-4500(28)
Project Name:
Project Number:
L2111119Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler
Temp
deg C Pres Seal
Container Information
Analysis(*)
03/12/21
Were project specific reporting limits specified?YES
7
<2
7
<2
7
<2
7
<2
Frozen
Date/Time
Final
pH
Initial
pH
Serial_No:03122116:55
Page 29 of 35
Report Format:Data Usability Report
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L2111119PLEASANT BAY
K47810DA.S.WW.700 03/12/21
Acronyms
DL
EDL
EMPC
EPA
LCS
LCSD
LFB
LOD
LOQ
MDL
MS
MSD
NA
NC
NDPA/DPA
NI
NP
NR
RL
RPD
SRM
STLP
TEF
TEQ
TIC
Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when
those target analyte concentrations are quantified below the limit of quantitation (LOQ). The DL includes any adjustments
from dilutions, concentrations or moisture content, where applicable. (DoD report formats only.)
Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction (SPME).
Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an
analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case
estimate of the concentration.
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of
analytes or a material containing known and verified amounts of analytes.
Limit of Detection: This value represents the level to which a target analyte can reliably be detected for a specific analyte in a
specific matrix by a specific method. The LOD includes any adjustments from dilutions, concentrations or moisture content,
where applicable. (DoD report formats only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Limit of Quantitation: The value at which an instrument can accurately measure an analyte at a specific concentration. The
LOQ includes any adjustments from dilutions, concentrations or moisture content, where applicable. (DoD report formats
only.)
Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated
values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any
adjustments from dilutions, concentrations or moisture content, where applicable.
Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available. For Method 332.0, the spike recovery is calculated
using the native concentration, including estimated values.
Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit.
N-Nitrosodiphenylamine/Diphenylamine.
Not Ignitable.
Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.
No Results: Term is utilized when 'No Target Compounds Requested' is reported for the analysis of Volatile or Semivolatile
Organic TIC only requests.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL
includes any adjustments from dilutions, concentrations or moisture content, where applicable.
Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less
than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values; although the RPD value will be provided in the report.
Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the
associated field samples.
Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.
Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF
and then summing the resulting values.
Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound
list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Serial_No:03122116:55
Page 30 of 35
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2111119PLEASANT BAY
K47810DA.S.WW.700 03/12/21
Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is
shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Difference: With respect to Total Oxidizable Precursor (TOP) Assay analysis, the difference is defined as the Post-Treatment value minus the
Pre-Treatment value.
Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after
adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.
Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-
preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.
Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined upon
receipt, if applicable.
PAH Total: With respect to Alkylated PAH analyses, the 'PAHs, Total' result is defined as the summation of results for all or a subset of the
following compounds: Naphthalene, C1-C4 Naphthalenes, 2-Methylnaphthalene, 1-Methylnaphthalene, Biphenyl, Acenaphthylene,
Acenaphthene, Fluorene, C1-C3 Fluorenes, Phenanthrene, C1-C4 Phenanthrenes/Anthracenes, Anthracene, Fluoranthene, Pyrene, C1-C4
Fluoranthenes/Pyrenes, Benz(a)anthracene, Chrysene, C1-C4 Chrysenes, Benzo(b)fluoranthene, Benzo(j)+(k)fluoranthene, Benzo(e)pyrene,
Benzo(a)pyrene, Perylene, Indeno(1,2,3-cd)pyrene, Dibenz(ah)+(ac)anthracene, Benzo(g,h,i)perylene. If a 'Total' result is requested, the
results of its individual components will also be reported.
PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA,
PFNA and PFOS. In addition, the 'PFAS, Total (6)' result is defined as the summation of results at or above the RL for: PFHpA, PFHxS,
PFOA, PFNA, PFDA and PFOS. (Note: 'PFAS, Total (6)' is applicable to MassDEP DW compliance analysis only.). If a 'Total' result is
requested, the results of its individual components will also be reported.
The target compound Chlordane (CAS No. 57-74-9) is reported for GC ECD analyses. Per EPA,this compound "refers to a mixture of
chlordane isomers, other chlorinated hydrocarbons and numerous other components." (Reference: USEPA Toxicological Review of
Chlordane, In Support of Summary Information on the Integrated Risk Information System (IRIS), December 1997.)
Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total'
result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081
and 8082.
Data Qualifiers
A
B
C
D
E
F
G
H
I
J
M
ND
NJ
-
-
-
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensates" are byproducts of the extraction/concentration procedures when acetone is introduced in
the process.
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related
projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x)
the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above
one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-
Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable
concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone).
Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted
analyses.
Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations
of the analyte.
Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The ratio of quantifier ion response to qualifier ion response falls outside of the laboratory criteria. Results are considered to be an
estimated maximum concentration.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should
be considered estimated.
The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The lower value for the two columns has been reported due to obvious interference.
Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).
Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Not detected at the reporting limit (RL) for the sample.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
-
Footnotes
Serial_No:03122116:55
Page 31 of 35
Report Format:Data Usability Report
Project Name:
Project Number:
Lab Number:
Report Date:
L2111119PLEASANT BAY
K47810DA.S.WW.700 03/12/21
Data Qualifiers
P
Q
R
RE
S
-
-
-
-
-
the identification is based on a mass spectral library search.
The RPD between the results for the two columns exceeds the method-specified criteria.
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than 5x the RL. (Metals only.)
Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
Analytical results are from modified screening analysis.
Serial_No:03122116:55
Page 32 of 35
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
44
121
128
Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
Method 624.1: Purgeables by GC/MS, EPA 821-R-16-008, December 2016.
Project Name:
Project Number:
Lab Number:
Report Date:
L2111119PLEASANT BAY
K47810DA.S.WW.700
REFERENCES
03/12/21
Serial_No:03122116:55
Page 33 of 35
Alpha Analytical, Inc.ID No.:17873
Facility: Company-wide Revision 18
Department: Quality Assurance Published Date: 2/16/2021 5:32:02 PM
Title: Certificate/Approval Program Summary Page 1 of 1
Document Type: Form Pre-Qualtrax Document ID: 08-113
Certification Information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA 624/624.1: m/p-xylene, o-xylene, Naphthalene
EPA 8260C/8260D: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), 1,2,4,5-Tetramethylbenzene;
4-Ethyltoluene.
EPA 8270D/8270E: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.
SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.
Mansfield Facility
SM 2540D: TSS
EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.
EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene,
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene.
Biological Tissue Matrix: EPA 3050B
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE,
EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B, SM4500NO2-B
EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.
Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1:
Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E,
SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate.
EPA 624.1: Volatile Halocarbons & Aromatics,
EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II,
Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603, SM9222D.
Mansfield Facility:
Drinking Water
EPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.
EPA 522, EPA 537.1.
Non-Potable Water
EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn.
EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Serial_No:03122116:55
Page 34 of 35
Serial_No:03122116:55
Page 35 of 35
55 Walkers Brook Drive, Suite 100, Reading, MA 01867
Tel: 978.532.1900
Offices in: MA, CT, NH, VT, NY, NJ, PA, SC & FL
westonandsampson.com
March 17, 2021
Bryan Webb (via email)
Ocean Edge Resort
2907 Main Street
Brewster, MA 02631
RE: Ocean Edge Resort Wastewater Treatment Facility
Monthly Operations Report – February 2021
Dear Mr. Webb:
Enclosed please find the monthly Operations Reporting Package for the Ocean Edge Resort wastewater treatment
facility (WWTF) located at 832 Village Drive in Brewster, MA.
Weston & Sampson Services, Inc. would like to note the following:
• All regulated effluent parameters of samples collected on February 15, 2021 were reported to be within their
respective permissible limits.
• Data was filed with MassDEP electronically, via eDEP. A copy of the transaction is included in this package.
If you have any questions or concerns regarding this report, or the wastewater treatment facility, please feel free
to contact me at wsscompliance@wseinc.com.
Regards,
WESTON & SAMPSON SERVICES, INC.
James R. Tringale
Compliance Coordinator
cc: Brewster Board of Health (via email)
FR Mahony Associates (via email)
Massachusetts Department of Environmental Protection
eDEP Transaction Copy
Here is the file you requested for your records.
To retain a copy of this file you must save and/or print.
Username:
Transaction ID:
Document:
Size of File:
Status of Transaction:
Date and Time Created:
Note: This file only includes forms that were part of your
transaction as of the date and time indicated above. If you need
a more current copy of your transaction, return to eDEP and
select to “Download a Copy” from the Current Submittals page.
1265467
3/31/2021:1:11:31 PM
1023.10K
WSSINC
Groundwater Discharge Monitoring Report Forms
Submitted
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
OCEAN EDGE CONFERENCE CTR
a. Name
ROUTE 6A
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JAMES R. TRINGALE
a. Name of Facility Contact Person
9785321900 WSSCompliance@wseinc.com
b. Telephone Number c. email address
3. Sampling information:
2/1/2021 ONSITE MEASUREMENTS
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
CHRIS VIGNEAU
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Daily Log Sheet 2021 Feb Daily
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DAILY LOG SHEET
633
1. Permit Number
043395913
2. Tax identification Number
2021 FEB DAILY
3. Sampling Month & Frequency
C. Daily Readings/Analysis Information
Date Effluent
Flow GPD
Reuse
Flow GPD
Irrigation
Flow GPD
Turbidity Influent pH Effluent
pH
Chlorine
Residual
(mg/l)
UV
Intensity
(%)
1 5326 7.08 7.57
2 901 7.12 7.52
3 3212 7.17 7.74
4 3220 7.14 7.69
5 2259 7.18 7.78
6 4533
7 4533
8 4533 7.11 7.63
9 2450 7.17 7.65
10 3150 7.10 7.71
11 2714 7.18 7.62
12 6085 7.12 7.54
13 6752
14 6752
15 6752
16 6752 7.06 7.65
17 5173 7.03 7.72
18 7116 7.14 7.77
19 8086 7.18 7.70
20 7563
21 7563
22 7563 7.12 7.60
23 3045 7.19 7.62
24 3439 7.08 7.73
25 3783 7.04 7.58
26 3182 7.07 7.66
27 6496
28 6496
29
30
31
gdpdls.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DAILY LOG SHEET
633
1. Permit Number
043395913
2. Tax identification Number
2021 FEB DAILY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
OCEAN EDGE CONFERENCE CTR
a. Name
ROUTE 6A
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JAMES R. TRINGALE
a. Name of Facility Contact Person
9785321900 WSSCompliance@wseinc.com
b. Telephone Number c. email address
3. Sampling information:
2/15/2021 ONSITE MEASUREMENTS
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
CHRIS VIGNEAU
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Monitoring Well Data Report 2021 Feb Monthly
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
633
1. Permit Number
043395913
2. Tax identification Number
2021 FEB MONTHLY
3. Sampling Month & Frequency
C. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
DRY = Not enough water in well to sample.
<
Parameter/Contaminant DG2 DG3 DG4 DG5 UG1
Units Well #: 1 Well #: 2 Well #: 3 Well #: 4 Well #: 5 Well #: 6
PH 6.60 6.30 6.40 6.50 6.50
S.U.
STATIC WATER LEVEL 46 44.7 42.2 47.1 40.4
FEET
SPECIFIC CONDUCTANCE 390 370 480 290 310
UMHOS/C
mwdgwpblank.doc • rev. 09/15/15 Monitoring Well Data for Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
MONITORING WELL DATA REPORT
633
1. Permit Number
043395913
2. Tax identification Number
2021 FEB MONTHLY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
A. Facility Information
1. Facility name, address:
OCEAN EDGE CONFERENCE CTR
a. Name
ROUTE 6A
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
2. Contact information:
JAMES R. TRINGALE
a. Name of Facility Contact Person
9785321900 WSSCompliance@wseinc.com
b. Telephone Number c. email address
3. Sampling information:
2/15/2021 RI ANALYTICAL
a. Date Sampled (mm/dd/yyyy)b. Laboratory Name
VARIOUS ANALYSTS
c. Analysis Performed By (Name)
B. Form Selection
1. Please select Form Type and Sampling Month & Frequency
Discharge Monitoring Report 2021 Feb Monthly
All forms for submittal have been completed.
2.This is the last selection.
3.Delete the selected form.
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit Daily Log Sheet • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
633
1. Permit Number
043395913
2. Tax identification Number
2021 FEB MONTHLY
3. Sampling Month & Frequency
D. Contaminant Analysis Information
For "0", below detection limit, less than (<) value, or not detected, enter "ND"
TNTC = too numerous to count. (Fecal results only)
NS = Not Sampled
1. Parameter/Contaminant 2. Influent 3. Effluent 4. Effluent Method
Units Detection limit
BOD 170 7.9 3.0
MG/L
TSS 200 10 2.0
MG/L
TOTAL SOLIDS 510
MG/L
AMMONIAN 14
MG/L
NITRATEN 3.4 0.25
MG/L
TOTAL NITROGEN(NO3+NO2+TKN)6.9
MG/L
OIL & GREASE ND 0.5
MG/L
infeffrpblank.doc • rev. 09/15/15 Groundwater Permit Discharge Monitoring Report • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
DISCHARGE MONITORING REPORT
633
1. Permit Number
043395913
2. Tax identification Number
2021 FEB MONTHLY
3. Sampling Month & Frequency
Important:When
filling out forms on
the computer, use
only the tab key to
move your cursor
do not use the
return key.
Any person signing
a document under
314 CMR 5.14(1) or
(2) shall make the
following
certification
If you are filing
electronically and
want to attach
additional
comments, select
the check box.
Facility Information
OCEAN EDGE CONFERENCE CTR
a. Name
ROUTE 6A
b. Street Address
BREWSTER MA 02631
c. City d. State e. Zip Code
Certification
“I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.
Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware that the
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.”
JAMES R. TRINGALE 3/29/2021
a. Signature b. Date (mm/dd/yyyy)
Reporting Package Comments
gdpdls 20150915.doc • rev. 09/15/15 Groundwater Permit • Page 1 of 1
Massachusetts Department of Environmental Protection
Bureau of Resource Protection Groundwater Discharge Program
Groundwater Permit
633
1. Permit Number
043395913
2. Tax identification Number
Date Received:
Date Reported:
P.O. Number
Work Order #:
Project Name:
Enclosed are the analytical results and Chain of Custody for your project referenced above. The sample(s)
were analyzed by our Warwick, RI laboratory unless noted otherwise. When applicable, indication of
sample analysis at our Hudson, MA laboratory and/or subcontracted results are noted and subcontracted
reports are enclosed in their entirety.
All samples were analyzed within the established guidelines of US EPA approved methods with all
requirements met, unless otherwise noted at the end of a given sample's analytical results or in a case
narrative.
The Detection Limit is defined as the lowest level that can be reliably achieved during routine laboratory
conditions.
These results only pertain to the samples submitted for this Work Order # and this report shall not be
reproduced except in its entirety.
We certify that the following results are true and accurate to the best of our knowledge. If you have
questions or need further assistance, please contact our Customer Service Department.
Approved by:
WSS Inc.dba Weston & Sampson
Chris Vigneau
55 Walkers Brook Drive
Suite 100
Reading, MA 01867
2/16/2021
2/22/2021
2102-02509
PROJECT #25364 OCEAN EDGE RESORT MONTHLY
Attn:
Laboratory Certification Numbers (as applicable to sample's origin state):
Warwick RI * RI LAI00033, MA M-RI015, CT PH-0508
LABORATORY REPORT
Nicole Skyleson
Data Reporting Manager
Page 1 of 3
R.I. Analytical Laboratories, Inc.
Laboratory Report
Work Order #:
WSS Inc.dba Weston & Sampson
2102-02509
PROJECT #25364 OCEAN EDGE RESORT MONTHLYProject Name:
PARAMETER RESULTS
SAMPLE
LIMIT
DET.
UNITS METHOD ANALYZED
DATE/TIME
ANALYST
Sample Type :
2/15/2021 @ 16:15
COMPOSITE
INFLUENT
001
Sample Date / Time :
Sample Description:
Sample Number:
BOD 5 KAW2/16/2021SM5210B 21edmg/l60170 23:12
Total Suspended Solids AMO2/16/2021SM2540D 2011mg/l2.0200 15:40
Total Solids AMO2/18/2021SM2540B 18-21edmg/l10510.0 11:18
Ammonia (as N)BR2/17/2021EPA 350.1mg/l0.2014 11:20
PARAMETER RESULTS
SAMPLE
LIMIT
DET.
UNITS METHOD ANALYZED
DATE/TIME
ANALYST
Sample Type :
2/15/2021 @ 16:30
COMPOSITE
EFFLUENT
002
Sample Date / Time :
Sample Description:
Sample Number:
BOD 5 KAW2/16/2021SM5210B 21edmg/l3.07.9 23:31
Total Suspended Solids AMO2/16/2021SM2540D 2011mg/l2.010 15:40
Nitrite (as N)JMD2/16/2021EPA 300.0mg/l0.25<0.25 19:38
Nitrate (as N)JMD2/16/2021EPA 300.0mg/l0.253.4 19:38
TKN (as N)DDM2/17/2021SM4500NOrg-D 18-21edmg/l0.503.5 10:15
PARAMETER RESULTS
SAMPLE
LIMIT
DET.
UNITS METHOD ANALYZED
DATE/TIME
ANALYST
Sample Type :
2/15/2021 @ 16:45
GRAB
EFFLUENT
003
Sample Date / Time :
Sample Description:
Sample Number:
Oil & Grease Gravimetric AM2/19/2021EPA 1664Amg/l0.5<0.5 13:40
Page 2 of 3
Page 3 of 3